Why are temperatures between 95 and 100 degrees centigrade optimum for reduced graphene oxide synthesis by Hydrazine from Grephene oxide?

hello

I want to calculate the molar mass of polyvinyl alcool 10% weight coupled with imino di acetic acid

We want to perform Transient Photocurrent on the potentiostat. However, in the settings we could not find the option to perform this. Are there any supplementary softwares or hardwares needed other than the basics?

Generally, lattice constant increases if the doping atom has larger radius. But sometimes reverse phenomenon happens, that is lattice constant increases when doping atom has smaller radius. What are the probable reasons behind it?

Papers submitted to some journals are being openly accessible through research square even before acceptance. What does it mean from the scientific communication and ethics perspective?

Why the desorption points of Ag-based Coordination-Polymers stopped at 0.3 P/P0, it should come down to at least P/P0=0.1. some examples of the N2 adsorption/desorption isotherm which was reported in literature was listed below:

1) ACS omega 4.5 (2019): 8926-8934.

2) Materials Research Express, 6(12), 125071.

Hello,

I am wondering if using temperatures up to 65 C reduce graphene oxide at all. I currently fabricate graphene oxide membranes from a water dispersion (heat up to 40 C during sonication). I also dry the membranes under high vacuum at 65 C for about 30 minutes. My dispersions recently seem to get very bad (can visually see big paticles) that are stubborn to remove with sonication, which I think raises the possibility of partial GO reduction. Any help is appreciated.

I have synthesized N doped SnO₂ and want to calculate oxygen vacancies quantitatively using X-ray Photoelectron Spectroscopy (XPS).

Kindly tell me the equation with examples.

Recently, I am working on Li10GeP2S12(LGPS), and all the experiments are exerted in a glove box. Li2S, GeS2 and P2S5 were mixed according to the conventional proportion and get ball-milled, and pellets were cold-pressed with the mixed powder. Next, the cold-pressed pellets are put in a slicon tube(without sealing, only used as container ) for sintering for 8h at 550°C, the heating and cooling rate is 5 and 1°/min respectively.

All seems well till the sintering completed. The samples deformed and swelled, and there are small cracks on some of them. After grinding to get a flat surface, EIS are performed on these samples. No accidently, large impendance and low ionic conductivity(10^-4) are got from these samples. But there is only a semi arc in this EIS, without the straight line in low frequency as usual( from 0.1-10^6 Hz). I want to know

1. Why the samples swell and deform after sinterinig, the trouble arise from heating temperature, furnance, or other element?

2. Why there is only a semi arc in the EIS?

3. What leads to the failure in the experiment, or some tips could be noticed later?

Thank you very much