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LA-ICP-MS detrital zircon dating and its provenance significance in Yan'an Formation of the Early-Middle Jurassic in the northwestern margin of Ordos Basin

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Abstract

The Early-Middle Jurassic Yan'an Formation widely distributed in the northwestern margin of Ordos Basin, and the outcrops scattered limitedly with similar lithological features. Many disputes still exist about the source areas of Yan'an Formation due to the tremendous geological reformation since the Late Cretaceous. The zircon Laser-Ablation Inductively Coupled Plasma-Mass Spectrometry (LA-ICP-MS) U-Pb dating was used to determine the ages of the source areas of the Yan'an Formation in the region. There are three samples selected from the sandstone of Yan'an Formation in two areas, altogether 210 grains were dated, and 193 valid zircon ages were obtained. Most zircons from the samples of Helan Mountain showed circular belt images under the cathodoluminescence microscope and displayed the left-oblique distribution pattern of rare earth elements. Most of those zircons have the Th/U larger than 0.4 indicating the magmatic origin, and a few zircons were from the metamorphic rock in the area. Most zircon U-Pb dating ages are mainly of the Paleozoic with the major peak in the Permian. The secondary ages are of the Proterozoic. The zircons from Zhuozi Mountain area are with the similar characteristics both in the images under the cathodoluminescence microscope and in the rare earth element distribution pattern. There exists much difference in the zircon ages between the two areas. The old ages in Zhuozi Mountain possess great proportions; 66.7% are of the Late Archean-Proterozoic (mainly the Proterozoic); only 22.7% of the total ages belong to the Permian, and 10.6% are of the Early-Middle Triassic. Compared with the ages of surrounding ancient rocks, it is concluded that the main sources of the Early-Middle Jurassic in the northwest margin of Ordos Basin were the Proterozoic magmatic and metamorphic rocks in the Alashan Paleo-Block; for the north of Ordos Basin, the main source was the Hercynian granite in the Alashan Paleo-Block. The main provenance in Helan Mountain was the Hercynian magmatic rocks in the Alashan Paleo-Block, and the secondary source was the Proterozoic magmatic and metamorphic rocks(Helan Mountain complex)for its northwest. While the principal source area in the Zhuozi Mountain was Proterozoic magmatic and metamorphic rocks for the northwest and the Hercynian magmatic rocks and Early-Middle Triassic magmatic rocks acted as the minor source. There is difference in provenance ages among the two studied areas and the Ciyaobao area. More researches from the sedimentary and petrology need to be done to further describe the provenance attribute. ©, 2015, The Editorial Office of Earth Science Frontiers. All right reserved.

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Paleogene clastic sedimentary rocks in the Puna plateau of northwestern Argentina contain valuable information about the timing and location of early mountain building in the central Andes. Because these rocks generally lack tuffaceous facies, only paleontological ages have been available. We present U-Pb ages from detrital zircons in the conglomeratic Eocene Geste Formation of the central Puna plateau. The zircon ages indicate that the Geste Formation was derived from nearby high-relief ranges composed of Ordovician metasedimentary rocks. A small population of ca. 37 35 Ma grains also confirms the late Eocene stratigraphic age of the Geste Formation, and suggests that U-Pb detrital zircon ages may provide a new tool for determining depositional ages and provenance of widespread Paleogene deposits in the central Andes.
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The Helanshan Complex is located at the westernmost segment of the Khondalite Belt, a continent–continent collisional belt along which the Yinshan Block in the north collided with the Ordos Block in the south to form the Western Block of the North China Craton. The complex consists of S-type granites and high-grade pelitic granulite/gneiss, felsic paragneiss, quartzite, calc-silicate rock and marble, together called the Khondalite Series rocks. LA-Q-ICP-MS U–Pb geochronology and LA-MC-ICP-MS Lu–Hf isotopic data of zircons, combined with cathodoluminescence (CL) imaging, enable the resolution of magmatic and metamorphic events that can be directed towards understanding the formation and evolution of the Khondalite Belt in the Western Block of the North China Craton. CL images reveal the coexistence of magmatic-type detrital zircons and metamorphic zircons in most of the Khondalite Series rocks, of which the metamorphic zircons occur as either single grains or overgrowth rims surrounding and truncating magmatic-type detrital zircon cores. LA-Q-ICP-MS U–Pb analyses on magmatic-type detrital zircons reveal two distinct age populations, with one in the Archaean (2.85–2.53 Ga) and the other in the Palaeoproterozoic (2.2–2.0 Ga), suggesting that the sedimentary protoliths of the Khondalite Series rocks in the Helanshan Complex must have been deposited at some time after 2.0 Ga. The Hf analyses show that the Archaean detrital zircons possess negative εHf(t) values from − 7.64 to − 0.15 with depleted mantle model ages ranging from 3.34 to 3.10 Ga. This implies the existence of a Paleo-Mesoarchaean (3.34–3.10 Ga) crust in the Western Block, which underwent a recycling event in the period 2.85–2.53 Ga. Nearly all Palaeoproterozoic (2.2–2.0 Ga) detrital zircons possess positive εHf(t) values (0.86–9.38) with depleted mantle model ages of 2.45–2.15 Ga, suggesting a significant crustal growth event in the Western Block in the Palaeoproterozoic. Metamorphic zircons yield two groups of age, with one at ~ 1.95 Ga and the other at ~ 1.87 Ga, of which the former is considered as the timing of the collision between the Yinshan and Ordos Blocks to form the Western Block, whereas the latter is consistent with the age of ~ 1.86 Ga from two S-type granites which are considered to have formed by the partial melting of pelitic granulites/gneisses at the stage of the exhumation of the Helanshan Complex.
Article
Detrital zircons from the Wulashan khondalites in the Ordos Terrane, western block of the North China Craton, give U–Pb ages between 1.84 and 2.32 Ga, showing that their provenance was dominated by Paleoproterozoic rocks, much younger than those exposed in the Eastern Block. These zircons have oscillatory growth zoning and possess εHf values between − 8 and + 9, suggesting derivation of their precursor magmas from old crust and juvenile materials from the mantle. The lowest εHf values of zircons with different ages give a line that intersects the depleted mantle line at about 2.6 Ga in a εHf vs. time diagram. This may imply that the precursor magma source in the deep level of the crust was largely separated from the mantle ∼2.6 Ga ago and therefore 2.6 Ga may be an important crustal formation period for the terrane. One khondalite sample has detrital zircons with a single age population at ∼2.0 Ga and positive εHf values from + 1 to + 9, clearly recording the significant addition of juvenile materials at ∼2.0 Ga in the source region. This may inspire us to seek whether there was a connection between a mantle superevent and the formation of Columbia supercontinent. Data of this study exclusively demonstrate that the Ordos Terrane was developed independently from the Eastern Block until assembly of the Columbia supercontinent. Therefore, tectonic models involving that the whole North China Craton was cratonized 2.5 Ga ago should be dismissed.
Article
Although metasedimentary successions are widely distributed across the North China Craton, those of Palaeoproterozoic age are restricted to three orogenic belts, namely: the Trans-North China Orogen, the Khondalite Belt and the Jiao-Liao-Ji Belt. Prior to this work, some of those successions were considered to be Archaean in age. The Palaeoproterozoic metasedimentary rocks contain detrital igneous zircon grains with ages ranging from 3.0 to 2.1 Ga, with the majority recording an age between 2.3 and 2.0 Ga. This latter group define a series of magmatic events that occurred between formation of the Archaean basement and deposition of the metasedimentary rock protoliths. The metasedimentary rocks occur as two associations; older volcano-sedimentary units that formed between 2.37 and 2.0 Ma, and younger sedimentary units that formed mainly between 2.0 and 1.88 Ga. All these rock associations were then subjected to metamorphism during the Late Palaeoproterozoic (1.88 and 1.85 Ga) tectonothermal event, named the Lüliang Movement in early Chinese literature, which was a continent–continent collision that led to the amalgamation of the North China Craton.
Article
Clastic sedimentary rocks are samples of the exposed continental crust. In order to characterize the crustal growth history of North China and its possible regional variations, 479 concordant detrital zircons in three sand samples from the lower reach of the Yellow River (which drains the Tibet–Qinghai Plateau, the Western Qinling Orogen, the Qilian Orogen and the North China Craton) and two sand samples from the Luan River and the Yongding River (which run entirely within the North China Craton) were measured for U–Pb age and Lu–Hf isotopic compositions by excimer laser-ablation ICP-MS and MC-ICP-MS. Although regional variations exist, concordant detrital zircons from the Yellow River reveal three major age groups of 2.1–2.5 Ga, 1.6–2.0 Ga, and 150–500 Ma. Detrital zircons from the smaller Luan and Yongding Rivers show three broadly similar major age groups at 2.3–2.6 Ga, 1.6–2.0 Ga, and 140–350 Ma, but with narrower age ranges. Compared to the Luan and Yongding River zircons, the Yellow River zircons are characterized by a significant number of Neoproterozoic grains. Although Hf isotopic compositions show both juvenile crustal growth and crustal reworking for all age groups, much of the crustal growth of North China occurred in the Neoarchean and Mesoproterozoic. All three rivers are characterized by a common prominent group of Hf crust formation model ages at 2.4–2.9 Ga with a peak at 2.7–2.8 Ga. A less significant age group lies between 1.4 and 1.8 Ga for the Yellow River, and between 1.6 and 1.9 Ga for the Yongding River and Luan River. Crustal growth rates based on Hf continental crust formation model ages suggest 45% and 90% of the present crustal volume was formed by 2.5 Ga and 1.0 Ga, respectively, for the drainage area of the Yellow River. In comparison, 60% and 98% of the present crustal volume of the North China Craton was generated by 2.5 Ga and 1.0 Ga, respectively, for the Luan and Yongding Rivers. The 2.7–2.8 Ga age peak observed in all river samples agrees well with the coeval major peak for global crustal growth. However, the other suggested global peaks of crustal growth at 3.4 and 3.8 Ga are insignificant in North China. Taken together with our previous studies of the Yangtze Craton, which show insignificant crustal growth at 2.7–2.8 Ga, we suggest that these advocated worldwide crust formation peaks be re-examined and treated carefully. Our results also show that Phanerozoic zircons may have been derived from crustal sources separated from the mantle up to 2.0 Ga ago before the zircons crystallized, suggesting long-term preservation, reworking and recycling of the continental crust.
Article
Zircom U-Pb age and Hf isotope analyses were made on gneissic granite and garnet-mica two-feldspar gneiss from the Helanshan Group in the Bayan Ul-Helan Mountains area, the western block of the North China Craton (NCC). Zircons from the gneissic granite commonly show core-mantle-rim structures, with magmatic core, metamorphic mantle and rim having ages of 2323±20 Ma, 1923±28 Ma and 1856±12 Ma, respectively. The core, mantle and rim show similar Hf isotope compositions, with single-stage depleted mantle model ages (T DM1) of 2455 to 2655 Ma (19 analyses). Most of the detrital zircons from the garnet-mica two-feldspar paragneiss have a concentrated U-Pb age distribution, with a weighted mean 207Pb/206Pb age of 1978±17 Ma. A few detrital zircons are older (2871 to 2469 Ma). The age for metamorphic overgrown rim was not determined because of strong Pb loss due to their high U content. The zircons show large variation in Hf isotope composition, with T DM1 ages of 1999 to 3047 Ma. In combination with previous studies, the main conclusions are as follows: (1) protolith of the khondalite series in the Helanshan Group formed during Palaeoproterozoic rather than the Archaean as previously considered; (2) The results lend support to the contention that there is a huge Palaeoproterozoic Khondalite (metasedimentary) Belt between the Yinshan Mountains Block and the Ordos Block in the Western Block of NCC; (3) The widely-distributed bodies of early Palaeoproterozoic orthogneisses in the Khondalite Belt might be one of the important sources for detritus material in the khondalite series; (4) Collision between the Yinshan Block, the Ordos Block and the Eastern Block occurred in the same tectonothermal event of late Palaeoproterozoic, resulting in the final assembly of the NCC.
Article
The "Taihua Group" is a collective term for a series of old terranes scattered along the southern margin of the North China Craton. The timing of formation and thermal overprinting of the Taihua Group have long been contentious, and its relationship with the Qinling orogenic belt has been unclear. In this study, new data from integrated in-situ U–Pb dating and Hf isotope analysis of zircons from an amphibolite (from the Xiong’ershan terrane) and a biotite gneiss (from the Lantian-Xiaoqinling terrane) indicate that the Upper Taihua Group formed during the Paleoproterozoic (2.3–2.5Ga) and thus was originally part of the southern edge of North China Craton, detached during the Mesozoic Qinling orogeny and displaced about 100km north from its original location. This suggests that the Taihua Group became part of the tectonic terrane associated with the Qinling orogeny and now forms part of the overthrust basement section of the Qinling belt. Before the Qinling orogeny, the Taihua Group was metamorphosed at 2.1Ga. The initial Hf-isotope compositions of zircons, together with positive εNd(t) values for the whole-rocks, imply that the original magmas were derived from a juvenile source with some assimilation of an Archean crustal component.
Article
Analyses of zircon grains from the Queureuilh Quaternary tephras (pumice) provide new information about their pre-eruptive history. U–Pb dating was performed in situ using two methods: SHRIMP and LA-MC-ICPMS equipped with a multi-ion counting system. Both methods provided reliable 207Pb/206Pb and 206Pb/238U ratios as well as U and Th abundances required for U–Pb Concordia intercept age determination, after initial 230Th disequilibrium correction. The new LA-MC-ICPMS method was validated by dating a reference zircon (61.308B) and zircons from a phonolitic lava dated independently with the two techniques. A time resolution of about 20 kyr for 1 Ma zircon crystals was achieved for both methods.
Article
The Qianlishan Complex is located in the westernmost part of the Khondalite Belt, a continent–continent collisional belt along which the Yinshan Block in the north and the Ordos Block in the south amalgamated to form the Western Block, which then collided with the Eastern Block along the Trans-North China Orogen to form the North China Craton. The complex is dominated by high-grade supracrustal rocks and minor S-type granites, of which the supracrustals consist of graphite-bearing sillimanite-garnet gneiss, garnet quartzite, felsic paragneiss, calc-silicate rock and marble. CL images reveal the existence of detrital and metamorphic zircons in major rocks of the Qianlishan Complex. In most cases, detrital zircons occur as either single grains with oscillatory zoning or oscillatory zoning cores, typical of igneous origin, which are surrounded by metamorphic overgrowth rims that are structureless, high bright and low in Th/U ratio. Detrital zircons from the Qianlishan Complex yield nearly concordant 207Pb/206Pb ages ranging from 2.3 to 2.0 Ga, suggesting that the protoliths of the high-grade supracrustal rocks in the Qianlishan Complex were deposited at some time after 2.0 Ga. Metamorphic zircons yield two age populations with one at ∼1.95 Ga and another at ∼1.92 Ga, of which the former is interpreted as the timing of the collision between the Yinshan and Ordos Blocks to form the Western Block, whereas the later is considered to be the age of subsequent post-orogenic extensional event. Minor S-type granites were emplaced at ∼1.88 Ga, as a result of partial melting of supracrustals at the stage of the exhumation of the Qianlishan Complex. These new zircon ages, combined with structural and metamorphic considerations, enable resolution of the tectonothermal events involving the collision between the Yinshan and Ordos Blocks to form the Western Block, followed by the post-collisional extension and subsequent exhumation of the Khondalite Belt.
Article
LA-ICP-MS U–Pb zircon dating and cathodoluminescene (CL) image analysis were carried out to determine the protolith and metamorphic ages of high-grade Al-rich gneisses, named as “khondalites”, from the Jining Complex of the North China Craton (NCC). The analytical results of more than 200 detrital zircon grains from the khondalites show three main age populations: 2060 Ma, 1940 Ma and 1890 Ma. These data indicate that the provenance of the Jining khondalites is Paleoproterozoic in age, but not Archean as previously suggested, and the sediments were derived from a provenance different from the Eastern Block and the Yinshan Terrane of the NCC. The nearly concordant youngest age of 1842 ± 16 Ma (207Pb/206Pb age) for the detrital zircons is interpreted as the maximum depositional age of the khondalites. Overgrowth rims of detrital zircons yield an age of 1811 ± 23 Ma, which we interpret as the metamorphic age. The new age data are consistent with the recent three-fold tectonic subdivision of the NCC and support that the Eastern and Western Blocks collided at ∼1.8 Ga to form the coherent NCC.
Article
Provenance analysis of sediments is aimed at reconstructing the parent-rock assemblages of sediments and the climatic-physiographic conditions under which sediments formed. Inferring sediment provenance from the final product, a basin fill, is anything but straightforward because the detrital spectrum evolves as the sediment is transported along the pathway from source to basin. Successful provenance analysis requires that the nature and extent of compositional and textural modifications to the detrital spectrum be recognised, if not quantified. The history of quantification in sediment-provenance studies is summarised and illustrated by tracking two fundamental ideas: the concept of the sediment-petrological province or petrofacies, and the relation between sandstone composition and (plate) tectonic environment. Progress in sedimentary provenance analysis has been closely linked with advancements in measurement technology. A brief survey of modern data-acquisition tools illustrates the possibilities and limitations of modern provenance research. An operational definition of Quantitative Provenance Analysis (QPA) is presented in which the central role of mass balance is acknowledged. Extension of this definition to include quantitative predictions obtained by forward modelling (computer simulation) of sediment production, as well as methodological improvements in data acquisition and processing is needed to cover likely future developments in QPA. The contributions to the special issue "Quantitative Provenance Analysis of Sediments" illustrate the intrinsic multidisciplinarity and rapid expansion of QPA.