November 2024
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12 Reads
Journal of Alloys and Compounds
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November 2024
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12 Reads
Journal of Alloys and Compounds
October 2024
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73 Reads
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1 Citation
Applied Sciences
The intricate nanostructured surface of black silicon (BSi) has advanced photodetector technology by enhancing light absorption. Herein, we delve into the latest advancements in BSi surface modification techniques, specifically focusing on their profound impact on light trapping and resultant photodetector performance improvement. Established methods such as metal-assisted chemical etching, electrochemical etching, reactive ion etching, plasma etching, and laser ablation are comprehensively analyzed, delving into their mechanisms and highlighting their respective advantages and limitations. We also explore the impact of BSi on the emerging applications in silicon (Si)-based photodetectors, showcasing their potential for pushing the boundaries of light-trapping efficiency. Throughout this review, we critically evaluate the trade-offs between fabrication complexity and performance enhancement, providing valuable insights for future development in this rapidly evolving field. This knowledge on the BSi surface modification and its applications in photodetectors can play a crucial role in future implementations to substantially boost light trapping and the performance of Si-based optical detection devices consequently.
September 2024
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44 Reads
Materials
Two different microstructures of an Al-12Si (wt. %) alloy were produced, respectively, via a powder laser bed fusion (P-LBF) additive manufacturing and casting. Compared to casting, additive manufacturing of Al-based alloy requires extra care to minimize oxidation tendency. The role of the microstructure on the mechanical properties of Al-12Si (wt. %) alloy was investigated by in situ compression of the micro-pillars. The microstructure of additively manufactured specimens exhibited a sub-cellular (~700 nm) nature in the presence of melt-pool arrangements and grain boundaries. On the other hand, the microstructure of the cast alloy contains typical needle-like eutectic structures. This striking difference in microstructure had obvious effects on the plastic flow of the materials under compression. The yield and ultimate compressive strength of the additively manufactured alloy were 23.69–27.94 MPa and 75.43–81.21 MPa, respectively. The cast alloy exhibited similar yield strength (31.46 MPa); however, its ultimate compressive strength (34.95 MPa) was only half that of the additively manufactured alloy. The deformation mechanism, as unrevealed by SEM investigation on the surface as well as on the cross-section of the distorted micro-pillars, confirms the presence of ductile and quasi-ductile facture of the matrix and the Si needle, respectively, in the case of the cast alloy. In contrast, the additively manufactured alloy exhibits predominantly ductile fractures.
July 2024
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7 Reads
ACS Applied Materials & Interfaces
July 2024
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227 Reads
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3 Citations
Biosensors
The non-invasive brain sensing modulation technology field is experiencing rapid development, with new techniques constantly emerging. This study delves into the field of non-invasive brain neuromodulation, a safer and potentially effective approach for treating a spectrum of neurological and psychiatric disorders. Unlike traditional deep brain stimulation (DBS) surgery, non-invasive techniques employ ultrasound, electrical currents, and electromagnetic field stimulation to stimulate the brain from outside the skull, thereby eliminating surgery risks and enhancing patient comfort. This study explores the mechanisms of various modalities, including transcranial direct current stimulation (tDCS) and transcranial magnetic stimulation (TMS), highlighting their potential to address chronic pain, anxiety, Parkinson’s disease, and depression. We also probe into the concept of closed-loop neuromodulation, which personalizes stimulation based on real-time brain activity. While we acknowledge the limitations of current technologies, our study concludes by proposing future research avenues to advance this rapidly evolving field with its immense potential to revolutionize neurological and psychiatric care and lay the foundation for the continuing advancement of innovative non-invasive brain sensing technologies.
April 2024
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71 Reads
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1 Citation
Due to its tunable bandgap, anisotropic behavior, and superior thermoelectric properties, device applications using layered tellurene (Te) are becoming more attractive. Here, we report a thinning technique for exfoliated tellurene nanosheets using thermal annealing in an oxygen environment. We characterize different thinning parameters, including temperature and annealing time. Based on our measurements, we show that controlled layer thinning occurs in the narrow temperature range of 325–350 °C. We also show a reliable method to form β-tellurene oxide (β-TeO2), which is an emerging wide bandgap semiconductor with promising electronic and optoelectronic properties. This wide bandgap semiconductor exhibits a broad photoluminescence (PL) spectrum with multiple peaks covering the range of 1.76–2.08 eV. This PL emission, coupled with Raman spectra, is strong evidence of the formation of 2D β-TeO2. We discuss the results obtained and the mechanisms of Te thinning and β-TeO2 formation at different temperature regimes. We also discuss the optical bandgap of β-TeO2 and show the existence of pronounced excitonic effects evident by the large exciton binding energy in this 2D β-TeO2 system that reach 1.54–1.62 eV for bulk and monolayer, respectively. Our work can be utilized to have better control over the Te nanosheet thickness. It also sheds light on the formation of well-controlled β-TeO2 layered semiconductors for electronic and optoelectronic applications.
January 2024
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111 Reads
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2 Citations
Materials
The deformation aspects associated with the micro-mechanical properties of the powder laser bed fusion (P-LBF) additively manufactured stainless steel 316L were investigated in the present work. Toward that, micro-pillars were fabricated on different planes of the stainless steel 316L specimen with respect to build direction, and an in situ compression was carried out inside the chamber of the scanning electron microscope (SEM). The results were compared against the compositionally similar stainless steel 316L, which was fabricated by a conventional method, that is, casting. The post-deformed micro-pillars on the both materials were examined by electron microscopy. The P-LBF processed steel exhibits equiaxed as well as elongated grains of different orientation with the characteristics of the melt-pool type arrangements. In contrast, the cast alloy shows typical circular-type grains in the presence of micro-twins. The yield stress and ultimate compressive stress of P-LBF fabricated steel were about 431.02 ± 15.51 − 474.44 ± 23.49 MPa and 547.78 ± 29.58 − 682.59 ± 21.59 MPa, respectively. Whereas for the cast alloy, it was about 322.38 ± 19.78 MPa and 477.11 ± 25.31 MPa, respectively. Thus, the outcome of this study signifies that the AM-processed samples possess higher mechanical properties than conventionally processed alloy of similar composition. Irrespective of the processing method, both specimens exhibit ductile-type deformation, which is typical for metallic alloys.
September 2023
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76 Reads
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9 Citations
Materials Science and Engineering A
Inconel 718, a Ni-based superalloy, was prepared by powder laser bed fusion (P-LBF) additive manufacturing (AM) method. AM of the Inconel 718 is challenging, as this particular alloy possesses a higher melting point, as well as resistance to temperature, which induces ‘hot-cracking’. Thus, the selection of proper input parameters are essential, which was successfully achieved in this present study. The microstructure exhibits a hierarchical structure, that starts with equiaxed and sub-cellular (∼100–600 nm) grains, and ends up on the formation of melt-pool and grain boundaries. This structure is exceptional and completely dissimilar to that of wrought alloy, which is infested with twins and precipitates of different secondary phases. However, the effectiveness of such microstructure of L-PBF alloy towards material's strength was undermined, as it lacks the presence of abundant precipitates, which is the major contributor to the strength of such alloys. The strength of the L-PBF processed alloy was in the range of 413–491 MPa and 562–665 MPa respectively, for yield and ultimate compressive strength. This was marginally higher than that of wrought alloy (408 MPa of Yield and 656 MPa of compressive strength). This was attributed to the absence of abundant gamma/gamma double prime (γ'/γ'') phases, and the presence of laves and delta (δ) phases, that are inferior towards the overall strengthen of the Inconel 718. Cross-sectional SEM and TEM investigation of the deformed micro-pillars confirmed the prevailing deformation mechanism that can be attributed to the slip/share plane formation in the presence of dislocation loops.
August 2023
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230 Reads
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6 Citations
Materials
Additive manufacturing (AM) of stainless steel is more difficult than other metallic materials, as the major alloying elements of the stainless steel are prone to oxidation during the fabrication process. In the current work, specimens of the stainless steel 316L were made by the powder laser bed fusion (P-LBF) additive manufacturing process. These specimens were investigated by electron microscopy and micro-/nano-indentation techniques to investigate the microstructural aspects and the mechanical properties, respectively. Compositionally, a similar wrought stainless steel was subjected to identical investigation, and used as a benchmark material. The microstructure of the P-LBF-processed alloy shows both equiaxed and elongated grains, which are marginally smaller (3.2–3.4 μm) than that of the wrought counterpart (3.6 μm). Withstanding such marginal gain size refinement, the increase in shear stress and hardness of the L-PBF alloy was striking. The L-PBF-processed alloy possess about 1.92–2.12 GPa of hardness, which was about 1.5 times higher than that of wrought alloy (1.30 GPa), and about 1.15 times more resistant against plastic flow of material. Similarly, L-PBF-processed alloy possess higher maximum shear stress (274.5–294.4 MPa) than that of the wrought alloy (175.9 MPa).
March 2023
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126 Reads
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1 Citation
International Journal on Interactive Design and Manufacturing (IJIDeM)
Stents are usually used as an implant in the human bodies for the treatment of blocked coronary arteries, and hence supporting them. Stents have become a highly viable option in the present times for such treatments. While the use of stents has proved to be highly beneficial for such purposes, there are also concerns associated with the incidences of fractures in the structures, particularly after being implanted in human body. Such fractures of stents not only make the structure ineffective for treatment, but also impact the human health. The objective of this review has been focused on understanding the stents fracture, based on a failure analysis approach, and hence to realize the ideal properties of stent, the contribution of corrosion and fatigues to stent fractures, and overall role of fracture mechanics. Towards that, computer interactive design criteria, and simulation-based performance analysis was also taken into consideration.
... Techniques such as Extreme Ultraviolet Lithography (EUV) [31], Electron Beam Lithography (EBL) [31,32], and Nano Imprint Lithography (NIL) [33], combined with precise thin-film deposition methods, facilitate the fabrication of microelectronic devices at the nanometer scale. Many of these structures, produced using methods such as vapor-liquid-solid (VLS) growth or wet-chemical catalytic etching, are commonly referred to as "silicon nanowires", whereas structures created through dry etching are typically known as "black silicon" [19,20]. With advancements in these processes, etching techniques such as Inductively Coupled Plasma Reactive Ion Etching (ICP RIE) have also evolved, becoming essential for the precise construction and control of multilayer patterns [34]. ...
October 2024
Applied Sciences
... Brain stimulation methods have been an area of significant interest and development in both research and clinical practice for several decades [6]. These techniques, which involve the application of electrical or magnetic stimuli to the brain, aim to modulate neural activity in targeted regions [7]. The development and refinement of these methods have opened new avenues for understanding brain function and treating various neurological and psychiatric disorders [8]. ...
July 2024
Biosensors
... Similarly, when a laser beam is being used, the process is known as laser beam AM. One of the many developed AM techniques is laser powder bed fusion (L-PBF), which has grown in popularity [3], especially for fabrication of metallic materials [4]. At first, the process involves spreading a fine layer (~ 0.1-0.15 ...
January 2024
Materials
... Also, it is worth noting that the Si appears as a needle (and plates in three dimensions) in the cast alloy, which facilitates the movement of the slip/shear planes. This phenomenon is somewhat similar to that reported in the case of high-entropy alloy [46,47] and segregation of alloying elements in grain boundaries in additively manufactured Inconel alloys [48,49]. This physical evidence sheds light on the inherent deformation behavior of these two differently processed materials, which will be discussed in the next section. ...
September 2023
Materials Science and Engineering A
... Nanoindentation technology had been widely used in the field of micro-region testing, which can not only test the hardness and modulus of micro-regions [18,19], but can also test the fracture toughness, fatigue properties and friction [20][21][22][23]. Due to the convenience of indentation testing technology, it is considered as a fracture toughness test technology that can reduce defects [24][25][26]. Researchers have carried out a series of studies on monocrystalline materials by using nanoindentation. ...
August 2023
Materials
... Also, it is worth noting that the Si appears as a needle (and plates in three dimensions) in the cast alloy, which facilitates the movement of the slip/shear planes. This phenomenon is somewhat similar to that reported in the case of high-entropy alloy [46,47] and segregation of alloying elements in grain boundaries in additively manufactured Inconel alloys [48,49]. This physical evidence sheds light on the inherent deformation behavior of these two differently processed materials, which will be discussed in the next section. ...
March 2023
Materials
... Heat effected zone: the second layer is due to the conduction of heat to the successive layer and its thickness can be in the microns meter range; this layer also has different mechanical properties than bulk material. The last layer is known as bulk material; it is the part of the material that is not affected by the heat [31]. High output temperature of EDM is good for machining β-type titanium alloys because of their high melting temperature which increases the preparation difficulty of parts for other conventional machining techniques [32]. ...
January 2023
Materials
... These methods are limited by their high operating costs, area requirements, and expensive instruments, and they are timeconsuming [19]. Consequently, it is urgent to develop a new detection method based on fluorescent substance sensing with a fast response, low cost, and ease of operation for different pollutants [20]. ...
January 2023
Materials Today Chemistry
... 16 In addition, micro-pillars tests facilitate to study the plasticity accommodation in Austenitic stainless steel. 17 In this research, micro-pillars with orientation [100] and [110] are prepared via focused-ion-beam (FIB) methods, respectively, to investigate the effects of textures on mechanical responses of Mo-Re alloys. ...
November 2022
Materials Science and Engineering A
... The path of the laser tracks appears as a typical 'fish scale'-type appearance in the microstructure [33], as shown by the white arrows in Figure 1. In addition to that, the boundaries of successive laser tracks seem like melt-pool-type appearances [34,35], which are 100's of microns in width. ...
May 2022
Metals and Materials International