Shawn Moylan’s research while affiliated with National Institute of Standards and Technology and other places

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Publications (57)


Fig. 4 Example bare plate samples with different laser scan patterns and orientations. Laser-scanned traces can also be seen which are used to align and orient samples after cutting
Fig. 5 Schematics and images showing the source locations and sample IDs for cylindrical compression specimens extracted from nickel alloy 625 bridge specimens reserved from AM Bench 2018
Fig. 7 Measured cure depth as a function of photomask dimensions and exposure are shown for all four resins
Fig. 8 Schematic of the high-speed synchrotron radiography and laser absorption setup at the Advanced Photon Source (adapted from [32])
Primary measurements conducted as part of AMB2022-01

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Outcomes and Conclusions from the 2022 AM Bench Measurements, Challenge Problems, Modeling Submissions, and Conference
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July 2024

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86 Reads

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7 Citations

Integrating Materials and Manufacturing Innovation

Lyle Levine

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Brandon Lane

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Chandler Becker

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[...]

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Fan Zhang

The Additive Manufacturing Benchmark Test Series (AM Bench) provides rigorous measurement data for validating additive manufacturing (AM) simulations for a broad range of AM technologies and material systems. AM Bench includes extensive in situ and ex situ measurements, simulation challenges for the AM modeling community, and a corresponding conference series. In 2022, the second round of AM Bench measurements, challenge problems, and conference were completed, focusing primarily upon laser powder bed fusion (LPBF) processing of metals, and both material extrusion processing and vat photopolymerization of polymers. In all, more than 100 people from 10 National Institute of Standards and Technology (NIST) divisions and 21 additional organizations were directly involved in the AM Bench 2022 measurements, data management, and conference organization. The international AM community submitted 138 sets of blind modeling simulations for comparison with the in situ and ex situ measurements, up from 46 submissions for the first round of AM Bench in 2018. Analysis of these submissions provides valuable insight into current AM modeling capabilities. The AM Bench data are permanently archived and freely accessible online. The AM Bench conference also hosted an embedded workshop on qualification and certification of AM materials and components.

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Fig. 1. Collected from the work of Oropeza et al.[28]. A powder spreading testbed: (a) computer model showcasing major components with the roller as the powder spreading mechanism; (b) fabricated powder spreading testbed; (c) sectional side-view of the testbed highlighting moving components and motion trajectories ; (d) images from the powder spreading experiment using stainless steel 316L 15 µm-45 µm powder and 250 µm layer height (Permission to reproduce these images was obtained from the authors and the publisher).
Fig. 3. A triaxial accelerometer is mounted on the recoater bridge to measure vibration.
Fig. 7. Still image of recoater blade spreading stainless steel powder captured using the high-speed camera set up. The field of view measures 2.71 mm x 2.33 mm.
Fig. 10. Plot of the vector field with colors indicating velocity relative to the stationary camera. Since the baseplate of the PST is also stationary, this plot is especially informative near the baseplate, since it may indicate what frictional forces are likely between the particles and the baseplate.
Magnifications achievable with the commonly used lens systems.
Powder Spreading Testbed for Studying the Powder Spreading Process in Powder Bed Fusion Machines

November 2023

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224 Reads

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3 Citations

The spreading of powder is an integral part of powder bed fusion-based additive manufacturing technologies; however, due to the complex nature and the number of interactions between particles, studying the powder spreading process is difficult. In order to gain insight into how the metal powder is spread in powder bed fusion machines using a recoater, a spreading testbed is needed, which provides a method for investigating the powder spreading process and characterizing the powder spread layer. The objective of this testbed is to study and establish fundamental relationships between bulk metal powder characteristics and powder spreading performance. Here, fabrication of a powder spreading testbed (PST) is described. The minimum but necessary functionality of the PST is discussed and potential characterization methods for the powder spread layer are proposed. This document serves as a guideline for future enhancements to the present testbed.



Assessing the influence of non-uniform gas speed on the melt pool depth in laser powder bed fusion additive manufacturing

May 2023

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50 Reads

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3 Citations

Rapid Prototyping Journal

Purpose This paper aims to investigate the influence of nonuniform gas speed across the build area on the melt pool depth during laser powder bed fusion. This study focuses on whether a nonuniform gas speed is a source of process variation within an individual build. Design/methodology/approach Parts with many single-track laser scans were printed and characterized in different locations across the build area coupled with corresponding gas speed profile measurements. Cross-sectional melt pool depth, width and area are compared against build location/gas speed profiles, scan direction and laser scan speed. Findings This study shows that the melt pool depth of single-track laser scans produced on parts are highly variable. Despite this, trends were found showing a reduction in melt pool depth for slow laser scan speeds on the build platform near the inlet nozzle and when the laser scans are parallel to the gas flow direction. Originality/value A unique data set of single-track laser scan cross-sectional melt pool measurements and gas speed measurements was generated to assess process variation associated with nonuniform gas speed. Additionally, a novel sample design was used to increase the number of single-track tests per part, which is widely applicable to studying process variation across the build area.


Data related to the effect of specimen geometry and orientation on tensile properties of Ti-6Al-4V manufactured by electron beam powder bed fusion

November 2021

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82 Reads

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1 Citation

Data in Brief

Additive manufacturing quality assessment often relies on tensile testing as the preferred methodology to qualify builds and materials. The data included in this article provides additional supporting information on our manuscript (Shanbhag et al. [1]) on the effect of specimen geometry and orientation on tensile properties of Ti-6Al-4V manufactured by electron beam powder bed fusion. As such, the data in brief provides in-depth details on the tensile specimen specifications, the tensile specimen build layout and replicate notations, and the tensile testing datasets. The information presented herein complements the manuscript.


Geometric Performance Testing of Directed Energy Deposition Additive Manufacturing Machine Using Standard Tests for Machine Tools

November 2021

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11 Reads

While performance testing of additive manufacturing machines is still nascent, standard tests for performance of machine tools used in metal cutting are well established. Our hypothesis is that because directed energy deposition (DED) additive manufacturing machines physically resemble typical vertical machining centers, standard geometric performance tests for machine tools will directly apply to DED machines. Standard tests of positioning error motions and circular motion were successfully conducted on a commercially-available DED system. With all tests providing reasonable and expected results, there is nothing to falsify our hypothesis. One additional consideration is the need for testing of the Z-axis on additive manufacturing machines using target positioning intervals on the order of a typical layer thickness at several positions along the axis.


A comparison of particle size distribution and morphology data acquired using lab-based and commercially available techniques: Application to stainless steel powder

November 2021

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63 Reads

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25 Citations

Powder Technology

The particle size distribution (PSD) and particle morphology of metal powders undoubtedly affects the quality of parts produced by additive manufacturing (AM). It is, therefore, crucial to accurately know the PSD and morphology of these powders. There exist several measurement techniques for these quantities, but since each method is based on different physical phenomena, which are sensitive to different aspects of a particle's shape and size, it is unclear how the measured PSDs and morphology compare to one another. In this study, five different techniques are used: sieve analysis, dynamic imaging analysis, laser diffraction analysis, X-ray computed tomography (XCT), and scanning electron microscopy. The first three are commonly used in the powder metallurgy field while the last two are laboratory-based tools capable of providing robust size and shape data. Nominally identical samples of stainless-steel powders were produced via riffling, and each technique was employed to measure effectively the same PSD and in some cases the morphology. In this paper, the differences among these measurement techniques are explored by a comparison of the measured results. Besides the random variations of the various measurement processes, the difference in the results is partly due to the fact that the particles are not perfectly spherical and that there are many multi-particles present. Each of these affect the principle of each method differently. Three-dimensional particle morphology and size data collected via XCT is used to provide insight regarding the discrepancies among other sizing and morphology measurement techniques. (Official contribution of the National Institute of Standards and Technology; not subject to copyright in the United States.)


Effect of specimen geometry and orientation on tensile properties of Ti-6Al-4V manufactured by electron beam powder bed fusion

October 2021

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121 Reads

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16 Citations

Additive Manufacturing

Tensile testing is often proposed as the preferred methodology to qualify builds and materials produced through additive manufacturing. While there is already work demonstrating the difference in measured properties between tensile specimens produced in different build orientations, this does not extend to different specimen geometries. In addition, the body of knowledge in this domain is typically made up of studies that utilize custom combinations of specimen geometries, part finishing, and post-processing, making it challenging to compare results. To study the impact of geometry of tensile specimens on tensile testing results, a selection of standard specimen types provided in ASTM E8/E8M was prepared in Ti-6Al-4V using an electron beam powder-bed fusion additive manufacturing machine. These specimens were characterized to observe any porosity defects, dimensional deviations, and surface topography that could impact performance. It was found that changes in specimen geometry, specimen size, build orientation, and the internal porous defects; have significant effects on the tensile properties of the specimens. The horizontally built specimens had higher yield and tensile strengths, but lower elongation compared to vertically built specimens. With an increase in cross-sectional area, an increase in the yield, tensile strength, and elastic modulus was observed. With an increase in surface area to volume ratio, there was a decrease in the yield and tensile strength. The average solid fraction of the specimens had no influence on any measured tensile properties. Furthermore, with an increase in maximum pore size, the elongation of the specimen decreased.



Citations (43)


... The National Institute of Standards and Technology (NIST) established The Additive Manufacturing Benchmark Series (AM Bench) in 2016 to provide comprehensive validation measurement data to the AM modeling community [1][2][3]. Residual stress, strain, and corresponding part distortion measurements have been a prominent aspect of AM Bench from the beginning. An early collaboration that laid the foundation for later AM Bench residual strain measurements used energy dispersive synchrotron X-ray diffraction (EDD) and part distortion measurements for characterizing elastic strains in additively manufactured Ti-6Al-4V components [4]. ...

Reference:

Elastic Residual Strain Measurements of 3D Additively Manufactured Builds of Nickel Alloy 718 AM Bench 2022 Artifacts Using Energy Dispersive Synchrotron X-ray Diffraction
Outcomes and Conclusions from the 2022 AM Bench Measurements, Challenge Problems, Modeling Submissions, and Conference

Integrating Materials and Manufacturing Innovation

... where D crop is the diameter of the cropped image. 41,42 The CI is related to powder flowability as depicted in Table 2. A low CI value, representing low temporal fluctuations of the powder surface, corresponds to excellent flowability, while a high CI value, representing significant temporal fluctuations of the powder surface, corresponds to poor flowability. ...

An interlaboratory study for assessing repeatability and reproducibility of the data generated by rotating drum powder rheometers
  • Citing Article
  • May 2024

Powder Technology

... Finally, DEM simulations can generate data that is difficult or impossible to obtain experimentally, such as the powder bed's packing condition or the powder's velocity and deformation fields during spreading. Recently, particle image velocimetry has been employed to observe particle velocity and displacement during the powder spreading process [49,50]. However, it is crucial to note that this technique primarily offers observations at the surface region, limiting its ability to comprehensively explain particle flow in the inner region or describe the intensity of interparticle forces or the onset of concentrated force chains. ...

Powder Spreading Testbed for Studying the Powder Spreading Process in Powder Bed Fusion Machines

... The exit nozzle is located on the opposite side of the process table. Many researchers have studied the impact of inert gas flow on part quality and spatter behaviour [59][60][61][62][63]. The spatter distribution is closely linked to the direction of the gas flow, since the spatter accumulates preferentially downstream of the gas flow. ...

Assessing the influence of non-uniform gas speed on the melt pool depth in laser powder bed fusion additive manufacturing
  • Citing Article
  • May 2023

Rapid Prototyping Journal

... This area depends on the particle's orientation, which can vary, leading to differences in the measured size of the same particle when analyzed multiple times. The difference between the nominal and actual sizes of sieved solid particles has also been reported in previous studies [28,39,40]. For the convenience of this study, the different size ranges of the iron powder are based on the nominal sieving fractions. ...

A comparison of particle size distribution and morphology data acquired using lab-based and commercially available techniques: Application to stainless steel powder
  • Citing Article
  • November 2021

Powder Technology

... It was observed that lowering the scanning speed during fabrication while increasing input energy within the process window led to deeper melt pools and melt pool overlaps, which in turn led to fewer volumetric defects, notably LoF, in the material. Shanbhag et al. [32] also examined the impact of specimen geometry on the tensile properties of Ti-6Al-4 V fabricated by electron beam powder bed fusion. An increase in yield, tensile strength, and elastic modulus was seen with an increase in the cross-sectional area of specimens. ...

Effect of specimen geometry and orientation on tensile properties of Ti-6Al-4V manufactured by electron beam powder bed fusion
  • Citing Article
  • October 2021

Additive Manufacturing

... The possibility to print such small structures can find different applications in technology and research. In research, one of such applications is printing artificial defects to study crack initiation processes under fatigue load [5][6][7][8] in 'ideal' geometries, with the goal of separating different effects. In fact, the PBF-LB process has its own challenges, such as defects [9,10], pores [11] and lack of fusion (LoF) [12]. ...

Investigation of the Effect of Artificial Internal Defects on the Tensile Behavior of Laser Powder Bed Fusion 17–4 Stainless Steel Samples: Simultaneous Tensile Testing and X-Ray Computed Tomography
  • Citing Article
  • June 2020

Experimental Mechanics

... Complimentary efforts have studied actual asspread layer topography in the powder bed [6][7][8][9], revealing likely significant variability in the effective thickness of the powder layer -this area is a focus of active research. Laser positioning has also been investigated, most often through the inspection of etched patterns on artifacts [5,10]. Several varieties of in-situ camera-based laser positioning qualification have also been explored [11,12]. ...

Quasi-Static Position Calibration of the Galvanometer Scanner on the Additive Manufacturing Metrology Testbed

... As a result, precise temperature profiles around the melt pool remain elusive [141]. If calibration is not performed correctly, uncertainties and errors can arise, leading to inaccuracies in the monitored data [228]. ...

In-situ calibration of laser/galvo scanning system using dimensional reference artefacts
  • Citing Article
  • May 2020

CIRP Annals

... While the quantification of the POD presents valuable information regarding the reliability of the XCT examination in detecting a defect of a given size, it does not account for the errors in the measurements of their features, such as size 18,36 . Depending on the acquisition parameters used for the XCT inspection, the detected features may vary drastically for the same defects, resulting in large errors in the feature measurements 18 . ...

The Influence of X-Ray Computed Tomography Acquisition Parameters on Image Quality and Probability of Detection of Additive Manufacturing Defects
  • Citing Article
  • September 2019

Journal of Manufacturing Science and Engineering