Johannes Pernpeintner’s research while affiliated with German Aerospace Center (DLR) and other places

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Publications (55)


As-received LD chunk.
SEM microstructures of the as-received LD chunk cross-sections, revealing distinct morphologies (a,d) and granular core–shell-like (b,c) brighter needle-like crystals embedded in the darker matrix.
Chemical composition of the as-received LD chunks corresponding to SEM micrographs (Figure 2).
XRD diffractogram of the as-received LD powder.
SEM/EDS Mapping of as-received LD chunk.

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LiDonit—A Potential Secondary Raw Material for Ceramic Applications in Concentrated Solar Energy
  • Article
  • Full-text available

July 2024

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48 Reads

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Johannes Pernpeintner

Solid particles as heat absorptances and storage mediums promise enhanced energy storage densities in concentrated solar power/thermal (CSP/T) plants. Employment of metallurgical slags as a secondary precursor material for solid particle preparation is ecologically and economically beneficial. Although these processed wastes, comprised of several oxides, exhibit generally promising high-temperature properties, chemical scattering from batch to batch may result in distinct material and functional properties, which may be an obstacle for their utilization. In this study, a steelmaking slag, LiDonit (LD), produced using a unique controlled slag treatment with high reproducibility is investigated as a candidate material. The aforementioned subsequent unique slag treatment makes LD a very promising and distinguishable secondary raw material for high-temperature applications. The as-received microstructure, phase components, and chemical composition of the LD material were analyzed to understand its material properties and to assess its reproducibility. The as-received LD chunks were transferred into pellets by subsequent milling, gel-casting, and sintering stages to reveal the potential processing routes. The CSP/T-related properties of sintered pellets, such as high temperature stability, heat capacity, and solar absorptance, were also examined to reveal their potential use in CSP/T applications and expand application areas with high added value.

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Application of a combination of innovative non-destructive measurement techniques for structural, energetic and safety analysis of buildings

June 2024

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74 Reads

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2 Citations

Journal of Building Engineering

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Eckhard Lüpfert

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David Heuskin

Mapping and investigating the technical, energy, and safety properties of buildings can be effectively accomplished using Building Information Modelling (BIM) tools. However, detailed geometric and structural information, material properties, and complete BIM models are often unavailable for existing buildings. Renovations, conversions, and aging phenomena further complicate the assessment of a building’s condition over its lifetime, necessitating (re)surveying efforts. In a collaborative project focused on studying smoke and gas dispersion pathways in buildings, a multidisciplinary team at the German Aerospace Center (DLR) explored the application of innovative mobile and non-invasive measurement methods to characterize existing buildings, surpassing the capabilities of state-of-the-art techniques. This research entailed the development and testing of enhanced acoustic measurements and H2 tracer gas techniques for leakage detection. Furthermore, a novel radar system was designed to analyse walls for concealed interconnecting structures. All measurement systems and approaches were collectively demonstrated on an existing office building, with the integration and localization of measurement data achieved through an automated process into a unified 3D database. The information obtained from these comprehensive measurements was visualized within a single-building model. By employing these advanced measurement techniques, a more thorough understanding of existing building conditions was achieved, surpassing the limitations of conventional methods. The successful integration and visualization of the acquired information within a unified model provide valuable insights for future renovations, conversions, and safety analyses. This research contributes to bridging the gap between traditional surveying practices and modern, data-driven approaches, enabling more efficient and accurate assessments of existing buildings.


Using an Al-Incorporated Deep Black Pigment Coating to Enhance the Solar Absorptance of Iron Oxide-Rich Particles

November 2023

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38 Reads

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3 Citations

The use of solid particles as direct heat absorbance and storage media promises enhanced storage densities in concentrated solar power (CSP) technologies. The long-term optical performance of those particles, which aim to be operational over years, is crucial. Dry powder coating with a deep black Cu-Mn-oxide pigment in a resonant acoustic mixer and subsequent sintering was employed to improve the long-term optical performance of hematite-rich spherical particles, which aimed to replace the state-of-the-art bauxite proppants. Due to the specific reactivity of the hematite particles, a new strategy using an Al-modified composition of the initial deep black pigment was required. The Al modification diminishes cation diffusion into hematite, allowing the formation of spinel-type Fe-Mn-Cu-Al-oxide coatings with favorable long-term temperature and optical stability. The effect of chemical composition of the coating layer on the coating process mechanism was discussed and the need for an elongated sintering time was noticed to ensure the termination of stable spinel phase formation. The structural and optical measurements revealed the enhancement of the properties of hematite absorber particles through this new modified coating process.




Air leakage detection in building façades by combining lock-in thermography with blower excitation

April 2023

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15 Reads

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5 Citations

International Journal of Ventilation

Air leakage in building envelopes is responsible for a large portion of the building’s heating and cooling requirements. Therefore, fast and reliable detection of leaks is crucial for improving energy efficiency. This paper presents a new approach to determining air leakages in a building’s envelope from the outside, combining lock-in thermography and thermal excitation by a blower door system. The blower creates a periodic overpressure within the building, inducing periodic temperature variations of the surfaces near the leaks on the outside surface, the façade. With the temperature variations excited at a known frequency, Fourier transforms of the time-series of the thermal images at the excitation frequency result in amplitude and phase images highlighting the areas affected by leaks. Periodic excitation and detection by an IR camera is known as lock-in thermography and is widely used to characterise semiconductor devices and in non-destructive testing. Excitation is usually achieved by optical, electrical, or mechanical energy input. For this work, measurements of outside façades have been performed with three excitation cycles of a period of 40 s at a 75 Pa pressure difference, leading to a total measurement time of only 2 min. Measurements have been performed with air temperature differences of 5 to 7 K at highly variable conditions of irradiance, wind, and cloud cover. The measurements show higher detection quality and less impact from changing ambient conditions than the state-of-the-art differential infrared thermography measurements. With the method highlighting the variations in the amplitude image only at the excitation frequency, variations caused by environmental effects are filtered out. A temperature difference as low as a few Kelvin is therefore sufficient, and large façades can be examined from the outside. This amplitude image is already clearer than an image created with differential thermography. A further reduction of unwanted artefacts in the image is demonstrated using phase-weighing of the amplitude by scalar product.




Air Leakage Detection in Building Façades by Combining Lock-In Thermography with Blower Excitation

October 2022

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210 Reads

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4 Citations

Air leakage in building envelopes is responsible for a large portion of the building’s heating and cooling requirements. Therefore, fast and reliable detection of leaks is crucial for improving energy efficiency. This paper presents a new approach to determining air leakages in a building’s envelope from the outside, combining lock-in thermography and thermal excitation by a blower door system. The blower creates a periodic overpressure within the building, inducing periodic temperature variations of the surfaces near the leaks on the outside surface, the façade. With the temperature variations excited at a known frequency, Fourier transforms of the time-series of the thermal images at the excitation frequency result in amplitude and phase images highlighting the areas affected by leaks. Periodic excitation and detection by an IR camera is known as lock-in thermography and is widely used to characterize semiconductor devices and in non-destructive testing. Excitation is usually achieved by optical, electrical, or mechanical energy input. For this work, measurements of outside façades have been performed with three excitation cycles of a period of 40 seconds at a 75 Pa pressure difference, leading to a total measurement time of only 2 minutes. Measurements have been performed with air temperature differences of 5 to 7 K at highly variable conditions of irradiance, wind, and cloud cover. The measurements show higher detection quality and less impact from changing ambient conditions than the state-of-the-art differential infrared thermography measurements. With the method highlighting the variations in the amplitude image only at the excitation frequency, variations caused by environmental effects are filtered out. A temperature difference as low as a few Kelvin is therefore sufficient, and large façades can be examined from the outside. This amplitude image is already clearer than an image created with differential thermography. A further reduction of unwanted artefacts in the image is demonstrated using phase-weighing of the amplitude by scalar product.


Figure 4. Spectral (left) and solar-weighted absorptance with ASTM G173 direct AM1.5 solar spectrum (right) per evaluator and particle type. Θ is the incidence angle of the measurement.
Equipment utilized by each evaluator to measure absorptance (α) and emittance (ε) of the particles. PE stands for PerkinElmer Lambda, IS stands for integrating sphere, and AR stands for anti-reflective.
Average solar absorptance and thermal emittance values determined by the evaluators per particle type.
Round Robin Test of Absorptance and Emittance of Particles for CSP

September 2022

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42 Reads

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3 Citations

SolarPACES Conference Proceedings

Precise knowledge of particle optical properties is crucial to the advancement and success of directly-irradiated particle receiver technologies. This work presents the results of a Round Robin Test (RRT) that was conducted between seven laboratories, where each par- ticipant measured the absorptance and emittance for a set of five different particle types. This research was performed within the framework of the SolarPACES Task III group, and the re- sults helped establish a guideline for evaluating the optical properties of particles. The guide- line was published on the SolarPACES Task III website in May 2022.


Citations (28)


... Future research will concentrate on enhancing the properties essential for CSP applications, including high heat capacity, excellent wear resistance, long-term durability, and effective solar absorptivity 5,6 . The objective is to investigate a broader spectrum of cooling rates to further develop the fayalitic slag as a foundational material for subsequent modifications 1,7 . ...

Reference:

Study on slag design of fayalitic by-products as an oxide raw material for solar heat absorber and storage media
Using an Al-Incorporated Deep Black Pigment Coating to Enhance the Solar Absorptance of Iron Oxide-Rich Particles

... Recent advancements include the combination of thermography with pressurisation techniques. Kölsch et al. [23] demonstrated the effectiveness of using thermograms before and after thermal excitation and mathematical post-processing to locate infiltrations around windows. Hurel et al. [24]used thermography and PIV methods to characterise the air inlets and outlets in wall assemblies. ...

Air leakage detection in building façades by combining lock-in thermography with blower excitation
  • Citing Article
  • April 2023

International Journal of Ventilation

... Jeong et al. [27] found the spectrally averaged (380 nm to 1020 nm) absorptivity of individual bauxite particles as around 0.88 while forward and backward scattering are found as ~ 0.04 and ~ 0.08, respectively. Sutter et al. [28] measured the solar-weighted absorptivity (AM1.5) of 5 different bauxite fixed bed samples to be in the range of 0.835-0.944. Similarly, Siegel et al. [29] used packed bed pellets of 4 different sintered bauxite samples, and measured solar-weighted absorptivity (AM1.5) to be 0.895-0.931. ...

Round Robin Test of Absorptance and Emittance of Particles for CSP
  • Citing Conference Paper
  • January 2023

... Moreover, after a long time exposure to high temperatures, a significant loss of optical properties due to the instable surface structures are reported, which makes their long-term use inefficient [8,9]. Therefore, there are still many studies aiming to modify state-of-the-art proppants and develop new compositions [10][11][12][13]. ...

Improved Performance of Ceramic Solar Absorber Particles Coated with Black Oxide Pigment Deposited by Resonant Acoustic Mixing and Reaction Sintering

... Those technologies should mitigate the weather dependent behavior that characterizes solar based solutions. According to that, there is a strong research effort on different technological solutions that employ solar particle receivers applied to thermal energy storage [2][3][4], power generation [5][6][7][8][9] or heat for industry processes [10][11][12][13]. In this sense, beam-down solar towers are receiving much attention from the scientific and industry sectors [14]. ...

A particle receiver-driven thermochemical cycle employing elemental sulphur for solar thermochemical energy storage: Investigation of particles as concentrated sunlight harvesting media and sulphur trioxide splitting catalysts
  • Citing Article
  • March 2022

Solar Energy

... Concentrated Solar Power (CSP) and thermal technology has become a focus of research due to the general increase in demand for sustainable and resource-efficient energy production. 1 Furthermore a higher potential of generating energy with CSP technology was announced within the integration of thermal energy storage (TES) systems to compensate an off-sun condition and besides being able to produce energy independently from the weather or daytime conditions 2 . Therefore, several approaches are currently under research to find more environmentally friendly solar heat absorbers and storage media with better properties to be more efficient comparing to the currently used salt mixtures 3,4 . ...

Assessment of Metallurgical Slags as Solar Heat Absorber Particles

... The findings indicate that lower cooling rates lead to increased crystallinity, thereby facilitating the formation of more stable iron-rich phases, specifically in the transition from fayalite to magnetite and ultimately to haematite. Furthermore, previous studies conducted by Alkan et al. 1,2 have demonstrated that the phases characterized by reduced amorphous content and elevated crystallinity are advantageous for application as ceramic particles in solar heat absorbers and storage media. The observed increase correlates with enhanced abrasion resistance of the particles within the CSP plant, highlighting their potential utility in this context. ...

Evaluation of Ceramic Proppants as Heat Transfer and Storage Medium

AIP Conference Proceedings

... There are variety of techniques which have been employed to gauge the thermal losses of the absorber component considering its operating mode. Field measurements and laboratory setups for assessing receiver heat losses that are derived the balances of the energy from the heated interior of the absorber to the surrounding environment were conducted by [5][6]. Rojas et al. and have examined the implementation of the absorber tube's capillary system in direct steam generation which can be applied to various applications. ...

Parabolic trough receiver heat loss measurement – Correction of absorber temperature over-prediction
  • Citing Conference Paper
  • July 2019

AIP Conference Proceedings

... Heat loss and optical efficiency of a parabolic trough receiver are essential elements of the efficiency of a parabolic trough solar field. First described by E. Lüpfert et al. [1] heat loss testing was adopted by several laboratories [2], [3], [4], and [5]. Goal of the measurement is to determine heat loss of a parabolic trough receiver as a function of absorber temperature. ...

Parabolic Trough Receiver Heat Loss and Optical Efficiency Round Robin 2015/2016
  • Citing Article
  • July 2017

AIP Conference Proceedings

... While the last sections describe "standard" solar field instrumentation, this section is dedicated to advanced approaches. An overview about recent research is given in [62]. Some of these monitoring approaches are leaving the sector of research and are gaining influence in industrial practice. ...

New methods and Instruments for Performance and Durability Assessment
  • Citing Chapter
  • December 2017