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October 2016
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53 Reads
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3 Citations
Organic & Biomolecular Chemistry
An efficient metal-free procedure for the formal α-carboxylation of primary alcohols has been developed. The method involves a one-pot oxidation/Passerini/hydrolysis sequence and provides access to α-hydroxy acids bearing a broad range of functional groups. A minor modification to the reaction conditions extends the range of accessible products to α-hydroxy esters.
September 2014
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37 Reads
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28 Citations
We report the palladium(II)‐catalyzed aerobic oxidative coupling of isocyanides with various (2‐aminophenyl)azoles using air as the stoichiometric oxidant. A diverse range of medicinally valuable azolo[ c ]quinazolines was obtained by this new approach. magnified image
... SCHEME 19 | Reaction of 2-amino-benzophenones with methylarenes catalyzed by potassium iodide. significant azole fused quinazolines 44 by using air as oxidant at 75 • C in 2-methyltetrahydrofuran (Vlaar et al., 2014). An ample spectrum of triazole starting materials was reacted well and furnished annulated products in moderate to excellent isolated yields (11-83%) (Scheme 20A). ...
September 2014
