Anirban Tewari’s scientific contributions

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Publications (1)


Figure 1. Structure of Ibuprofen. 
Figure 2. UV Spectra for pure Ibuprofen Ibuprofen showed maximum peak at 222 nm (solvent: 0.1N HCl/ 1N HCl) so the analytical wavelength was selected at 222 nm. 
Table 2 (a). Results of accuracy calculation
Figure 3. Standard Curve of pure Ibuprofen: (a) (SOLVENT-0.01 N HCl) (b) (SOLVENT-1 N HCl) Results for determination of validation parameters Specificity (Solvent-0.01 N HCl) 
Figure 4 : (a) Linearity Curve (Solvent-0.01 N HCl) (b) (Solvent1 N HCl) 

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Preparation, Estimation and Validation of the parameters of the standard curve of Ibuprofen by comparative study
  • Article
  • Full-text available

July 2017

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10,432 Reads

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4 Citations

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Anusree Raha

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Prosenjit Mukherjee

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Anirban Tewari

Objective: The objective of present study was to study and validation of different parameters for Ibuprofen. Material and methods: UV spectrophotometric method for the comparative quantitative determination of Ibuprofen was developed for the validation of the prepared standard curve of the drug in two different conc. of same solvent (HCl). The parameters like linearity, accuracy, precision, limit of detection, limit of quantization, range, Robustness & Ruggedness were studied according to International Conference on Harmonization guidelines (ICH). The absorbance values were measured at 222 nm. Results and conclusion: Results of the analysis were validated statistically and also by recovery studies. The proposed method can also be used for the reliable quantization of Ibuprofen in pharmaceutical formulation. In the UV spectroscopic method linearity over the concentration range of (100-600) ug/ml with a correlation coefficient 0.9972 (Solvent is 0.1N HCl) and 0.9937 (Solvent is 1N HCl) for (50-100) ug/ml were found out.

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Citations (1)


... Among the tested pH, the results highlighted pH 5 and 230 nm as the optimal condition for attaining both the highest absorbance values and the most substantial peak of activity (results not shown). The findings were corroborated with the other Ibuprofen studies conducted by Marchlewicz et al. (2017) and Tewari et al. (2017). Employing sodium acetate buffer, Marchlewicz et al. (2019) selected an optimal wavelength of 230 nm for their analysis. ...

Reference:

Leveraging the Pharmaceutical Area Through Multidisciplinary Synergy: From Prescription to Disintegration
Preparation, Estimation and Validation of the parameters of the standard curve of Ibuprofen by comparative study