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The principles of microwave heating as applied to industrial processing are outlined and the basic design of applicators for material processing is described. Industrial applications range from food tempering to rubber vulcanisation and from vacuum drying to sintering of ceramics. The most promising applications to date are summarised
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Microwave heating
The principles of microwave heating as applied to industrial processing are outlined and the basic
design of applicators for material processing is described. Industrial applications range from food
tempering to rubber vulcanisation and from vacuum drying to sintering of ceramics. Established
applications to date are summarised.
By A.C. Metaxas
Microwave heating is a process within a family of electroheat techniques, such as induction, radio
frequency, direct resistance or infra-red heating, all of which utilise specific parts of the
electromagnetic spectrum. These processes supplement, and in specific cases totally replace,
conventional heating or drying systems used in industry. This is because some conventional
systems are very bulky, not easy to operate, can pollute the environment due to harmful
omissions and above all can be very inefficient.
The major advantages of using microwaves for industrial processing are rapid heat transfer,
volumetric and selective heating, compactness of equipment, speed of switching on and off and
pollution-free environment as there are no products of combustion. Microwave leakage can
certainly be kept well below government recommended levels.
Fundamentals of microwave heating
Dielectric loss
It has long been established that a dielectric material can be processed with energy in the form of
high-frequency electromagnetic waves. There are many distinct frequency bands which have
been allocated for industrial, scientific and medical (ISM) use, as shown in Table 1, with the
principal frequencies centred at 896 MHz (915 MHz in the USA) and 2450 MHz for which
equipment can be readily purchased.
In this frequency regime there are primarily two physical mechanisms through which energy can
be transferred to a non-metallic material. At the lower microwave frequencies conductive currents
flowing within the material due to the movement of ionic constituents, such as salts for example,
can transfer energy from the microwave field to the material. This loss mechanism is
characterised by an equivalent dielectric conductivity term σ, giving effectively a loss parameter of
σ/ωεο.
At the other end of the microwave heating spectrum, around 3000 MHz, the energy absorption is
primarily due to the existence of permanent dipole molecules which tend to re-orientate under the
influence of a microwave electric field, as shown in the inset of Fig. 1. This re-orientation loss
mechanism originates from the inability of the polarisation to follow extremely rapid reversals of
the electric field. At such high frequencies therefore the resulting polarisation phasor lags the
applied electric field. This ensures that the resulting current density has a component in phase
with the field, and therefore power is dissipated in the dielectric material.
Table 1 Frequency allocation for industrial, medical and scientific (ISM) purposes in the
range 433.92 MHz to 40 GHz
Frequency Frequency Area permitted
MHz tolerance + or -
433.92 0-2% Austria, The Netherlands, Portugal,
West Germany, Switzerland
896 10 MHz UK
915 13 MHz North and South America
2375 50 MHz Albania, Bulgaria, Hungary, Romania
Czechoslovakia, USSR
2450 50 MHz worldwide except where 2375 MHz is used
3390 0-6% The Netherlands
5800 75 MHz worldwide
6780 0-6% The Netherlands
24150 125 MHz worldwide
40680 UK
Source adapted from Ref. 2
The loss mechanism is characterised by the relative loss factor term ε˝, which is part of the
complex relative permittivity, whereas absolute permittivity is given by ε = εοε*. The two
components of the complex relative permittivity shown plotted as a function of the frequency in
Fig. 1, for a dipolar liquid or for a wet dielectric, where the losses at microwave frequencies are
due to re-orientation polarisation. The conductivity effects of ionic species, shown by the light blue
response, dominate at radio frequencies, while the combined loss is shown by the red response.
ε"
ε"e
ε"
e
Effective loss factor as a function of the frequency due to dipolar
relaxation and Maxwell-Wagner or ionic conduction mechanisms.
σ
εο
log ƒ
789 10
13.56
MHz 27.12
MHz 896
MHz 2450
MHz
Industrial
allocated
frequencies }
+
dipolar
re-orientation
E
e/m
field
ionic
conduction
material
boundary
t
ω
+
-
+
-
+
-
+
-
+
-
+
-
+
+
+
+
+
+
+
+
+
+
+
+
+
+
+
+
+
+
+
+
+
+
+
+
Fig. 1. Effective loss factor as a function of the frequency. The inserts
show the dipolar re-orientation and conductive loss mechanisms
Wave equation
The basic equations in microwave heating, through which a number of fundamental parameters
are derived, are the total current density established in the dielectric material and the modified
wave equation1. The total current density includes the contributions of conductive and
displacement current densities and is given by the curl of the magnetic field phasor, H:
X H = σE + D/t [1]
where the first term on the right hand side of eqn [1] is the conductive contribution due to ionic
constituents and the second term is due to the displacement current density, where D = εE, where
E being the applied electric field phasor. The analysis proceeds by considering eqn [1] together
with Faraday’s equation
X E = B/t [2]
to derive a differential equation in E or H. Using the inter-relationship between E, E/t and
2E/t2, and assuming that E=ReEejωt, the following modified wave equation is derived for a
dielectric slab where the induced electric field is predominantly constant in the z-direction and the
magnetic field lies in the x -direction:
2EZly2 = µεοKω2Ez = γ2Ez [3]
The propagation constant γ is given by
γ = jω√Kεοµ = α + jβ [4]
where α and β are the attenuation and phase constant, respectively, and the parameter K is given
be K = ε′−j(ε″+σ/ωεο) = (ε′−jεe), where εe is the effective loss factor shown in red in Fig. 1.
Semi-infinite slab analysis: The simplest case to consider is a horn applicator emanating
microwave energy to a relatively thin semi-infinite dielectric slab of high dielectric loss factor as
shown in Fig. 2a. The electric field within the dielectric is substantially constant along the x-
direction and it decays in the y-direction as it traverses the material as depicted in Fig. 2b.
Solution of eqn.[3], including time variations and assuming that when y , Ez must be finite,
yields
Ez=Re Eoe-γyejωt=Eoe-α y cos(ωt-by) [5]
where Eο is the maximum value of the electric field intensity at the material/air interface. Such a
simplistic approach to the problem, resulting in an exponential decay, does also have some
(a)
+ + + + +
Dielectric
material
E-field
(b)
z
E
x
0
x
z
y
D
0.37
Electric field
Power density
p δ
(c)
0.14
0Ž/2 Ž
P or E
0y
Eo
P
o
Fig. 2(a) Semi-infinite slab analysis (b) the direction of the E-field along the
waveguide face and (c) the electric field and power density distribution
relevance in practice as it relates approximately to the treatment of foodstuffs with microwaves.
This is because most foodstuffs have a relatively high effective loss factor εe, which results in a
rapidly decaying electric field and justifying the assumption made above which is inherent in the
derivation of eqn.[5] Whether a finite slab or a semi-finite slab is considered, the electric field has
decayed to a very small value within a very short distance of the air/dielectric interface.
Finite slab: Unless the dielectric properties of the processed material are very high, the
assumptions made in the previous paragraph do not hold for a finite slab and the electric field is
given by the general solution of eqn. 3:
Ez=Re {[Ae-γy+ Be+γy]ejωt} [6]
where A and B are constants that fit the appropriate boundary conditions. It is not justifiable now
to set B = O in this case because the slab has medium to low loss factor value and the second
term may be of the same order as the first term in eqn.[6]. The electric field in this case does not
decay exponentially and more elaborate solutions ought to be found when y is set equal to the
slab width.
Heating in the standing wave electric field: The analysis of the semi-infinite slab has been
applied to a dielectric material placed inside a multimode oven applicator for approximate
calculations of the electric field and other parameters. This is justified only if the dielectric loss
factor is fairly high, as is the case with most foodstuffs, resulting in a rapidly decaying field. With a
medium to low loss dielectric the electric field no longer decays exponentially and more rigorous
methods of calculation should be deployed.
Power dissipation within the dielectric
It is often required to estimate the amount of power that can safely be dissipated in a dielectric
given that the effective loss factor is known. This can be obtained from considering the Poynting
vector EXH, which leads to the following expression for the power dissipated per unit volume2:
Pv=(1/2)[σ+ωεοε”)|Ez|2=(1/2)σe|Ez|2 [7]
where ω = 2πf, with f being the applied frequency in Hz, σe the effective dielectric conductivity and
Ez being given by the appropriate expressions above. The total power dissipated P in a volume V
is obtained by integration, therefore
P = VpvdV [8]
In a multimode cavity applicator fitted with distributed energy sources and mode stirrers, the
electric field may be assumed to have been randomised to an approximately constant value,
resulting in a volumetric power density pv=σ eERMS
2, where ERMS is the RMS value of the electric
field established in the processing zone. For example, for a power dissipation of 107 W/m3 and
εe = 0.1, the required electric field at 2450 MHz is 27 kV/m.
The effective loss factor varies as a function of the moisture content and temperature.
Such data, typically shown in Fig. 3, are very useful when assessing the type of applicator and
frequency of operation for drying or for other heating applications. For example, the response at a
frequency of 27.12 MHz is more suitable for moisture levelling than that at 2450 MHz, while the
εe against T response, typically of a high-temperature ceramic material, shows that there is a
high probability of thermal runaway above some critical temperature Tc.
wet paper
27.12 MHz
2450 MHz
M%
EÆ
e
(b)
ε"ceramics
T
cT
critical temperature
e
(d)
ε"
(a) (b)
Fig. 3 Loss factor as a function of (a) the moisture content M and (b) temperature T
Skin and power penetration depths
Returning to the simplistic approach of a semi-infinite slab system, as the electromagnetic energy
penetrates into the interior of the material it attenuates to an extent depending on the effective loss
factor εe. The inverse of the attenuation constant is defined as the skin depth, δ=1/α, which is the
depth at which the magnitude of the electric field drops to 1/e of the value at the surface. Fig.2c
shows schematically the decay of the electric field and power. As pv is proportional to Ez 2, the
power dissipated per unit volume decays as the energy traverses the semi-infinite dielectric slab.
pv(y)=Poe-2y/δ=Poe-y/Dp [9]
where PΟ is the incident power density and Dp is the power penetration depth at which the power
drops to 1/e from its value at the surface At y=δ, eqn.[9] yields pv(δ)=0.14Po giving 86%
dissipation (note that Dp =1/2α=δ/2-see figure 2c). At the frequencies allocated for industrial use in
the microwave regime, the penetration depths could be very small indeed and often the size of
the dielectric to be treated, particularly when it is fairly lossy, is many times larger than Dp, which
may result in temperature non-uniformities. Rough estimates of Dp can be determined by
consulting the literature on dielectric properties.
Temperature distribution
Microwave heating entails the conversion of electrical energy to heat either to raise the material
temperature to a critical level or for material drying or for material melting, to cite but a few well
known examples.
A generalised hear flow equation can be formulated, to describe the temperature or moisture
distribution for these processes, containing the following terms: rate of rise of temperature
ρcT/t; temperature distribution, .q, through Fourier’s law q=keT; volumetric power density
generation pv; as well as an additional convective heat flow term due to any appreciable
surrounding gas/solid energy exchange and specific heat and enthalpy of evaporation terms due
to the components of a moist dispersed system. Here, ρ and c are the density and specific heat,
while ke refers to the effective thermal conductivity of the material. In the case of unit operations,
use is also made of the relevant mass transfer equations of the bound materials3, where now ke is
a tensor and c is an effective specific heat, both parameters containing contributions of the
various components in the heterogeneous mixture.
By taking specific simple cases, solutions can be obtained, say, for the temperature distribution
within a heated dry dielectric material after a steady-state condition has been reached or for the
moisture levelling in planar dielectrics where, for example, the microwave energy is applied when
T/
t = 0 and where the contributing effect of the Fourier-derived term is ignored.
Numerical modelling
A concerted effort has recently been made to determine the temperature and moisture distribution
theoretically during microwave processing4. The power density term p, contains the electric field
established in the material and strictly speaking the wave equation has to be solved in order to
determine the field’s distribution5. Exact analytical solutions can only be obtained for the most
simple cases, in which it is still necessary to assume constant εe, σ e, ke, ρ and c parameters6.
Numerical methods based on finite differences, finite elements, the method of moments or
transmission line matrix methods have been used with varying degrees of success. Metallic sheet
insert and shields specially used in microwaveable food packages can now routinely be modelled
using finite elements7.
Industrial systems
Typical industrial microwave heating or drying equipment is shown in Fig. 4. Basically there are
three major components. The first component is the power unit where microwaves are generated
at the required frequency band. The second component forms the applicator, where the material
is subjected to intense microwave fields, and to which any additional ancillary process equipment
such as pumps for operation under moderate vacuum conditions, steam or hot air injection, must
be connected. Often the applicator forms the last part of a conventional processor.
Power
Unit Control and
automation
Power
supply
Vacuum
tube
Conventional
equipment
Microwave or
radio frequency
applicator
Hybrid
system
Circulator or
matching
circuit
Fig. 4. Typical microwave hearting set-up
Finally, the third major component is the control circuitry to optimise and regulate the overall
performance of the microwave heater. Magnetron tubes are used primarily to generate the
microwave power. It is by now usual and prudent practice to incorporate a ferrite iso-circulator
protection between the magnetron source and the applicator.
Microwave applicators
The most common form of an applicator, comprising well over 50% of industrial systems, is the
multimode type. In principle, it is an extension of the domestic microwave oven but built for large
scale material processing. However, industry uses many other types, with a brief description of
some of the most popular ones given below2.
Multimode applicators
Basic application: Multimode resonant applicators consist of a metallic enclosure into which a
microwave signal is coupled through a slot and suffers multiple reflections as shown in Fig. 5a.
The superposition of the incident and reflected waves gives rise to a standing wave pattern or
mode. In a given frequency range such an applicator will support a number of resonant modes.
(a) (b)
Fig. 5 Multimode oven applicators (a) basic multimode applicator with four
magnetrons (b) modular system
For any empty applicator each of these modes exhibits a sharp resonant response. However, for
an applicator partially filled with a dielectric material which couples reasonably to the microwave
electromagnetic fields, the resonant responses of the modes will overlap in frequency to give a
continuous coupling with the dielectric load. This applicator is very versatile in that it can accept a
wide range of material loads of different effective loss factors and sizes.
Coupling systems: The energy is coupled into the applicator through a slot, an array of resonant
slots, a radiating horn or by other means. To improve the uniformity of heating within the
multimode applicator a number of methods are used, such as a mode stirrer. With multiple
generators the opportunity exists to distribute the power so as to give a better excitation of the
modes and better uniformity of heating than can be achieved with a single feed, by distributing the
feed points around the walls of the oven and by feeding at different polarisations. The magnetrons
may be mounted directly or through a launching waveguide.
In common with all oscillators the impedance of the load connected to the output affects the
performance of the magnetron in both generated power and output frequency. The reactive
component of the load impedance causes a small change in the output frequency, whereas the
resistive component affects the output power.
These characteristics are displayed in the Rieke diagram, shown typically in Fig. 6, in which
contours of frequency and power output ate plotted on an impedance circle diagram. Usually
within the permitted load impedance range of the magnetron, frequency and power changes do
not exceed ± 0.2% of nominal frequency and ± 15% of nominal output power, respectively.
Material
Conveyor
modular multioven system
Absorbing
load
Chokes
Magnetrons
Processed
material
Conveyor supports
To extractin
g
fans
Conveyor
Mode stirrers
-5 MHz
0 Hz
+5MHz
Restricted
region
Towards
load
P
4
P3
P2
P1
x
Waveguide
short circuit
backing plate
Magnetron
antenna
Variable
mismatch
load
(a)
(b) (c)
Po
x
Fig. 6 (a) Waveguide launcher (b) power distribution and (c) Rieke diagram
The position of the back plate of the waveguide is determined by experiment following a set of
well documented guidelines whereby the magnetron is substituted by a probe and using a
variable mismatch load at the end of the waveguide as shown in Fig. 6a. The power distribution
shown in Fig. 6b follows.
In the case where the magnetron is connected to the oven applicator via a waveguide one can
fine match the magnetron to the loaded applicator, by substituting the magnetron with a suitable
probe and carrying out impedance measurements using a network analyser. Matching
adjustments are then made to ensure that operation is kept within the manufacturer’s
recommended region, shown shaded on the Rieke diagram of Fig. 6c.
The region where the frequency contours converge, called the sink, should be avoided. This is
because when the Voltage Standing Wave Ratio (VSWR- a measure of reflections) exceeds the
specified maximum in the sink, unstable operation, including moding and frequency jumping, may
occur. However, operation in the region of convergent frequency lines outside the sink is
desirable to obtain mode shifts in the multimode applicator.
Multimode processing systems: A typical online multimode oven applicator for industrial
processing of irregular loads is shown in Fig. 5a. Leakage of electromagnetic energy is minimised
by the use of protective devices such as absorbing loads or reflective devices. In Fig. 5a four
magnetrons are shown to feed power to the applicator, however, industrial systems with many
tens of magnetrons feeding one applicator cavity have been designed.
Fig. 7 Continuous microwave meat tempering system
(Courtesy of Selo-Bollans Ltd)
Fig. 7 shows a multi-feed processor for meat tempering at 896 MHz, while Fig. 8 shows a
prototype puffing or rapid drying for snack foods. In this latter system a relatively small volume
Fig. 8 Microwave puffing system for snack foods
(Courtesy of APV Baker Ltd)
applicator is used capable of being able to handle large amount of power without arcing occurring.
Consequently, the high power density produced in the applicator is used for dry-frying of snack
foods such as pellets. By bringing the pellets rapidly to 100oC it boils off the moisture and
expands them in less than ten seconds. The product is healthier compared to when using oil
baths although for organoleptic reasons some oil may be added afterwards for optimising the
recipe for microwave processing.
Modular microwave systems have been very popular in that a large microwave processor can be
constructed by placing a number of units shown in Fig. 5b in series and running the material on a
conveyor which passes through all the units. Fig. 9 shows such a system comprising two modules
for preheating rubber composite extrusions, including metallic spines, prior to vulcanisation in a
hot air tunnel. Each module offers the facility of connecting up to 12 kW of microwave power at
2450 MHz in 2 kW steps according to the specific requirement of throughput and type of rubber.
Fig. 9 Modular microwave pre-heater for rubber vulcanisation
(Courtesy of Microwave Heating Ltd)
Horn applicator
Horns can be used effectively to beam the energy into a conveyor tunnel which carries foodstuffs
to be processed. In a specific application the energy from the magnetron is split equally four ways
as shown in Fig.10a and radiated sequentially from the four sides as shown in Fig. 10b towards
blocks of foodstuffs, such as meat or butter, for tempering. In such a process the frozen foodstuff
is elevated from the cold store temperature to just a few degrees below zero. This avoids
defrosting the product, which might lead to thermal runaway on account of the much higher εe of
water compared with that of ice.
3 dB couplers
Source
horns (a) (b)
Fig.10 (a) Microwave splitter using 3 dB couplers and (b) continuous microwave
butter tempering lines (Courtesy of Anchor Foods Ltd)
In the particular application shown in Fig. 10b three separate lines operating at 896 MHz are used
to temper 25 kg blocks of butter from -14ºC to about -2ºC, which facilitates further mechanical
processing such as blending and portioning 250 g retail packs.
Single-mode resonant applicators
In single (fundamental or higher order) mode resonant cavities the superposition of the incident
and reflected waves gives a standing wave pattern which is very well defined in space. This
enables the dielectric material to be placed in the position of maximum electric field for optimum
transfer of the electromagnetic energy.
A most versatile single mode resonant applicator is shown in Fig. 11, which operates in the TE10n
mode. It consists of a rectangular waveguide, into which a co-sinusoidal electric field distribution
of n half-wavelengths is established, connected to a flange with a coupling iris on one side and a
non-contacting short-circuit plunger on the other side.
M/wave
source
Dielectric
material
Slot
tuning
plunger
Matching
Aperture
S/C
E-field distribution
(a)
(b)
E
Z
Iso-circulator
Fig. 11 TE10n single mode resonant applicator
The dielectric material to be processed is inserted into the applicator through a slot in the broad
dimension of the waveguide. The dielectric experiences the maximum electric field of the standing
wave set up within the applicator, which is in the range 1<E<2 kV/cm with moderate output power
from the source, say a few kW. Larger electric fields, say up to 10 kV/cm, can also be achieved
resulting in a very high rate of heating, typically exceeding 30ºC/s.
For optimum performance of such an applicator both the position of the plunger, which
determines the operating frequency, and size of the iris, which establishes how much of the
energy is in fact transferred to the applicator, are dependent upon the dielectric properties of the
material under consideration. Optimisation procedures much be carried out at low power using a
network analyser which measures, among other parameters, the reflection coefficient and hence
the VSWR and the cavity impedance.
The versatility of such an applicator is unquestioned because a variable plunger and a variable
aperture enable this applicator to treat a wide range of dielectrics of different effective loss factors
simply by choosing the right dimensions. The system in Fig.11 shows the cavity, with its variable
aperture, connected to the power source via an iso-circulator. Infra-red pyrometry measures the
surface temperature of a heated sample through a small hole at the side of the waveguide cavity.
Single-mode resonant applicators suffer from the limitation that relatively small size material
throughputs can be treated at any one time, even at the 896/915 MHz frequency band, and
consequently their adoption in industry has been limited. Furthermore, when processing low loss
materials, automatic feedback control systems are necessary to operate within the required
resonant frequency band and hence maintain high heating rates. Other less versatile resonant
cavities have been used for industrial processing of liquid foodstuffs, for example the TM010 or the
higher order TM020 and TM11n cavities2.
Special applicators
The use of microwave frequencies has given rise to the possibility of designing applicators to suit
every requirement and material configuration. This range from corrugated to periodic applicators
and from meander to slow wave or radiator applicators. Moreover, the use of small power
magnetrons enables the designer to concentrate the power at specific regions of the processing
zone2.
Review of industrial microwave heating applications
Microwave heating has been established in some key industries. The brief description below
highlights the most important applications to date, making reference to Fig.13 where
appropriate1,2. This review does not include chemical applications where great strides have
already been made, particular in organic synthesis8.
Food tempering
Meat, fish, fruit, butter and other foodstuffs can be tempered for cold store temperature to around
-3ºC for ease of further processing such as grinding the meat in the production of burgers or
blending and portioning butter packs. The industrial customer cannot eradicate waste from errors
in long-term forecasting demand where, for example, too much or too little meat tempered
resulted in either wasted meat or lost custom. A typical continuous system is shown in Fig. 7.
Pre-heating for rubber vulcanisation
The temperature of rubber extrusions can rapidly and uniformly be brought up using microwave
energy to the required level, for cross-linking of the bonds to commence. The latter process is
then carried out using hot air or infra-red energy, as shown by route 1 in Fig.12.
Apart from continuous vulcanisation using modular systems, as shown in Fig. 9, microwaves have
been used in batch systems either on a small scale or in multi-magnetron systems to heat blocks
of rubber of up to several hundred kg in weight.
Drying
Atmospheric pressure: A host of materials from textiles to ceramics and from coated paper to
leather have been dried using microwaves, usually in combination with conventional systems as
shown by route 2 in Fig. 13. The drying of pasta is an established application comprising three
stages involving microwaves and hot air in various combinations, to give improved sanitation and
better control as well as quality. Other examples include the drying of onions, parsnips, snack
foods (with subsequent expansion as described above in puffing of pellets), fabrics, leather,
ceramic cores and moulds and ceramic wares.
Vacuum drying: Some materials are heat sensitive and cannot be dried at atmospheric pressure.
It is necessary to reduce the pressure to reduce the boiling point and effect drying at a reduced
temperature. A modest vacuum around 100-200 mm Hg is necessary where the formation of a
microwave plasma or arc can still be avoided. Notable examples are the drying of fruit juices,
beverages, drugs and pharmaceutical pellets.
Fig.12 Combined mixing, granulating and vacuum drying system
(Courtesy of Niro T.K. Fielder Ltd)
Fig. 12 shows an integrated processor for mixing, granulating and drying under vacuum a wide
range of pharmaceutical products using a 27 kW, 2450 MHz microwave unit. This hybrid
processor is highlighted by route 4 in Fig. 13.
Heating and cooking
Many foodstuffs have been cooked by microwaves for various stages of processing. Examples
include bacon cooking in a combination system, meat coagulation to upgrade scrap and doughnut
cooking for frying.
Pasteurisation and sterilisation
Food products, such as bread, precooked foods and animal feedstuffs have been processed
using microwaves for pasteurisation or sterilisation or simply to improve their digestibility. Specific
examples include the sterilisation of bonemeal and the processing of barley to achieve starch to
gelatine conversion. Food pasteurisation of sealed packs under pressure can be effected by
microwave energy, however, as with most pasteurisation processes the product after treatment
needs rapid cooling to avoid infestation, as shown by route 3 in Fig. 13.
Potential applications
There are a host of potential microwave applications awaiting better economic conditions to either
e revived or be developed further. These include the following areas: food processing, asphalt
hole patcher, vitrification of nuclear wastes, treatment of highly toxic substances, waster recover
of plastics, pyrolysis, heating of resins, polymerisation, heating of oil sands and the processing of
minerals.
Apart from drying other areas of interest in ceramic processing with microwaves include slip
casting, sintering of a wide range of ceramics and composites, joining and calcining of
superconductors or electroceramics. Microwave energy is presently being used for providing
additional heating to the plasma used in thermonuclear fusion reactors and for etching
semiconductor products1.
OTHER ELECTRICAL
ENERGY IR etc
INFRARED
HOT AIR
or
STEAM
or
AIR JETS
HOT AIR OR STEAM
HEAT RECOVERY
VACUUM
RF OR MICROWAVE
APPLICATOR
CHOKE
COOLER
PRESSURE
3 1
2
1
2 3
4
4
Fig.13 Hybrid systems
Economics
Current industrial equipment capital costs vary between 2000 Euro and 5000 Euro per kW
installed, depending on the power range and the level of sophistication of auxiliary equipment
required such as backing/diffusion tests sets for the production of a moderate vacuum, injection of
hot air or steam, microprocessor control and automation. The overall efficiency, from mains to
power dissipated in the product, lies in the range 50-70%. Ultimately, some heat recovery on the
conventional hot air unit, as shown in Fig. 13, as well as a careful mix of the various sources of
energy available, would enhance the overall system performance.
Conclusions
Microwave heating has been established in a number of industrial sectors. Undoubtedly the food
industry with its diverse operations such as tempering, blanching, sterilising, cooking, puffing and
vacuum drying offers the biggest opportunity for microwave processing, but the formidable
challenge of other competitive techniques must be seriously addressed. Recent developments in
the ceramics industries point to major applications which may come on stream involving large
microwave power the near future.
References
1 METAXAS, A. C.:Foundations of electroheat: a unified approach, John Wiley and
Sons 1996
2 METAXAS, A. C. and MEREDITH, R. J.: Industrial microwave heating (IEE, 1983,
reprinted 1988 and 1993)
3 FULFORD, G. D.: ‘A survey of recent Soviet research on drying of solids’, Can. J. Chem.
Eng., 1969, 47, pp. 378-391
4 LORENSON, C.: ‘The why’s and how’s of mathematical modelling for microwave heating’,
Microwave World, 1990, 2, (1) pp. 14-22
5 Dibben D.C and Metaxas A C., 'Finite Element Time Domain Analysis of Multimode
Applicators Using Edge Elements', Journal of Microwave Power and Electromagnetic
Energy, 29(4), pp.242-251, 1994
6 HILL, J. M.: ‘Simple exact solutions applicable to microwave heating’, J. Appl. Math.,
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AMPERE Newsletter, ISSN 1361-8598, Issue number 45 June 2005
Based on an article first published in the IEE Power Engineering Journal 5(5) in September 1991
Dr A C (Ricky) Metaxas is a Fellow and Tutor at St John’s College, Cambridge, England, UK.
From 1995 until 2005 he was President of AMPERE, the European based organisation which
promotes the use of microwave and radio frequency energy in industry and commerce. He is an
IEE Fellow.
... These powders were mechanically alloyed using a planetary ball mill: Pulverisette 4, manufactured by Fritch (Idar-Oberstein, Germany, 2010). The technological parameters of the mechanical alloying process are presented in Table 2. Microwave sintering of metal-based composite materials cannot be performed due to the high reflection of microwaves by metals [20]. Therefore, indirect microwave heating or hybrid microwave heating can be applied, but only after a simulation of temperature distribution to establish the lowest level of microwave power. ...
... Microwave sintering of metal-based composite materials cannot be performed due to the high reflection of microwaves by metals [20]. Therefore, indirect microwave heating or hybrid microwave heating can be applied, but only after a simulation of temperature distribution to establish the lowest level of microwave power. ...
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Over 60% of reported failures for reactive power compensation systems are given for damage to electrical circuit breaker contacts. This paper presents a study on the development of microwave technology for sintering of W–Cu–Cr alloys at 1012 °C for 65 min using 623.38 W microwave power, as well as microwave joining at 231 °C of the W–Cu–Cr composite material on body contact using 475 W microwave power for 55 s. The joined components were subjected to mechanical and electrical tests in accordance with ICE standards to validate the applied technology. Tests of connection–disconnection of the electrical contacts were carried out in accordance with the maximum number of disconnections allowed by the manufacturer (2 cycles/min): 25 s rest time and 5 s operating time under load. The components of the electrical contact after 111237 switches were analyzed under a microscope revealing a reduction of the damaged area by 27% compared with the original contact.
... Additional research in the field of microwave sintering of ceramics has been performed by Wang et al. as well as Hao et al. [12,13]. Other research related to microwave heating has focused mainly on process stability, rate of conversion and thermal runaway, in order to optimize the MHH process or to improve its stability [14][15][16][17][18][19]. ...
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Featured Application Sintered Barium Ferrite W-type materials can be used for the manufacturing of permanent magnets for the automotive industry in order to increase the performance of electric engines. Microwave hybrid heating (MHH) is a sustainable and efficient process with a small carbon footprint that can be applied for sintering. However, the MHH process is unstable for ceramic material, with a high potential for the conversion of microwaves into heat due to the possible occurrence of the thermal runaway phenomenon. Abstract Thermal runaway in microwave hybrid heating of ceramics is an unwanted phenomenon which damages the sintered products. The aim of the present study is to establish to what extent the pressing forces of 100, 200 and 300 MPa used in the compaction process and the optimization of the microwave heating mechanism can reduce the occurrence of thermal runaway. Modeling and simulation of temperature distributions alongside defects created by the compaction process are performed in order to evaluate their influence on the stability of MHH. Based on CT scanning, defects with dimensions from 110 to 515 μm are studied in terms of local overheating and how the thermal runaway can lead to internal arc discharge. The results show that samples compacted at 100 MPa and exposed at 600 W injected power reach temperatures peaks around 1010 °C and are affected by major cracks and large melted areas. The samples compacted at 200 and 300 MPa present similar behavior, without arc discharge, but are also affected by cracks. Based on these findings, the MHH process can be applied to sintering processes but with a reduced injected power below 300 W for samples compacted with pressing forces higher than 300 MPa.
... Many techniques have been proposed to address not only the efficiency of the process but also the quality and safety of end products. Among these novel techniques, thermal processing, encompassing microwave heating, radiofrequency heating, ohmic heating, pulsed electric field, and ultrasound treatment, has emerged as up-and-coming areas of research [20][21][22][23][24][25][26][27][28][29][30]. ...
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Featured Application Ultrasonic treatment at 24 kHz enhances fermentation dynamics and boosts ethanol yield by up to 20%, especially in high-density worts. This approach can improve the efficiency and profitability of industrial ethanol production. Abstract This study investigates the effect of ultrasonic treatment on the fermentation of molasses wort with a density range of 18–24 °Blg, using two high-performance Saccharomyces cerevisiae yeast strains: Thermosacc Dry and Ethanol Red. The primary objective was to determine if ultrasound could accelerate fermentation and increase ethanol yield. The research showed that ultrasonic treatment at 24 kHz significantly increased fermentation dynamics and ethanol yield by 5 to 20%, depending on the yeast strain and wort density. Higher wort densities (22–24 °Blg) showed more pronounced positive effects. Ultrasound treatment caused visible indentations in the yeast cell walls and promoted cell aggregation. In addition, the study investigated the influence of different ultrasound amplitudes on fermentation efficiency and showed that higher amplitudes further improved ethanol production in 22–24 °Blg worts. These results suggest that ultrasound can improve the efficiency and profitability of ethanol production, highlighting the potential for further research to optimise industrial fermentation processes. The application of ultrasound in biotechnology, particularly in fuel ethanol production, could lead to significant economic benefits on a global scale.
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Utilizing direct microwave- (MW)-induced heating in solid-state synthesis yields the clear benefits of greatly reduced reaction times and lower energy requirements as compared with conventional methods. Here, we describe a bespoke single-mode cavity (SMC) MW reactor designed to operate within a neutron beamline that allowed powder diffraction data to be collected from materials in situ as they were heated using MWs. The unique set-up was used to investigate the rapid solid-state synthesis of the binary metal chalcogenide thermoelectric (TE) materials Bi2Se3, Bi2Te3, Sb2Se3 and Sb2Te3. The resultant time-resolved diffraction data from each synthesis were time-sliced post-reaction into segments covering periods of tens of seconds, enabling the reaction progression to be visualized as colourmap plots. This technique enabled the accurate tracking of polycrystalline structure formation and a quantitative analysis of phase fractions during the accelerated heating and subsequent cooling stages of each reaction. Our investigations have also revealed some of the present limitations of rapid in situ neutron diffraction techniques and how these might be remedied. This article is part of the discussion meeting issue ‘Microwave science in sustainability’.
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Nanomaterials have garnered significant interest across industries such as energy, engineering, agriculture, and textiles due to their versatile applications. Microwave (MW)-assisted synthesis has emerged as a cost-effective, eco-friendly, and efficient method for producing high-quality nanomaterials. This technique enables precise control over size, shape, growth kinetics, and crystalline structure while reducing energy consumption and improving chemical yield. In this review, we explore the mechanisms of MW-assisted synthesis, focusing on its ability to modulate structural and morphological attributes. We also discuss challenges, prospects, and sustainable approaches for synthesizing nanostructured composites using MW technology. Finally, we highlight promising directions for advancing MW-assisted methodologies, offering novel insights into the high-yield production of premium-quality nanomaterials for industrial applications.
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Nowadays, microwelding processes have been developed for various technologies, mainly for electronic applications. Resistive bonding is usually used, but electrical energy consumption represents a challenge due to energy crisis in terms of lack of energy supply and prices. This paper aims to evaluate the carbon footprint and economic issues related to microwave welding of aluminum plates against conventional resistive bonding. The research performed has shown that for different levels of microwave injected power from 600 up to 1200 W, the calculated footprint based on energy consumption has shown the sustainability of the microwave welding process. The total energy consumed for microwelding process was less than 360 Wh meaning a total cost up 0,2 euro/100 joints.
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In this work the reasons for the occurrence of the temperature runaway effect in radio-frequency thawing are examined and the importance of the polarization of the electric field is clarified. In particular it is observed that the polarization of the electric field normal to the food surface generally counteracts the temperature runaway effect by reducing the food loss in portions at higher temperature. One exception was found to be beef fat. An efficient simulation technique is proposed for the design of food thawing equipment that considers circuit simulations, electromagnetic simulations and thermal calculations. By assuming a uniform food temperature, the simulation time for the whole thawing process is in the order of one second. It is very convenient for the design of the matching circuit and of the overall system, because the variation with time of average temperature, electrode impedance, voltage, efficiency and power balance can be obtained.
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The importance of internal moisture migration in the drying of solids and the various approaches to the study of this phenomenon are outlined briefly. The extensive Soviet work in this field, particularly by Lykov's school, is reviewed, and the advantages, disadvantages and practical applications of this approach are discussed. Some of the more interesting practical Soviet studies of drying plant and processes are also mentioned briefly. On expose brièvement l'importance de la migration de l'humidité interne dans le séchage des solides ainsi que les diverges voies d'accès à l'étude de ce phénomène. On passe en revue le travail intensif qu'ont fait les Russes dans ce domaine (particulièrement les, disciples de Lykov) et discute les avantages, inconvénients et applications pratiques de leur méthode d'étude. On souligne aussi quelques-unes des études leg plus intéressantes el pratiques que les Russes ont faites en ce qui a trait aux usines et procédés de séchage.
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There is presently considerable interest in the utilization of microwave heating to novel industrial applications. Mathematically such problems involve Maxwell''s equations coupled with the heat equation and for which all thermal, electrical and magnetic properties of the material are nonlinearly dependent upon temperature. Accordingly such problems are highly complex and very little theoretical work has been undertaken. The purpose of this paper is to obtain simple exact solutions applicable to microwave heating in the simplest situation, involving only one spatial dimension and assuming that all thermal, electrical and magnetic properties exhibit a power law dependence on temperature. Similarity solutions and other special solutions are examined. These generally result in highly nonlinear coupled systems of ordinary differential equations and although some new closed results are obtained in special cases, in general, such complex systems of ordinary differential equations need to be solved numerically. Roughly speaking, we show that stretching similarity solutions exist only if the power law electrical and thermal conductivities and magnetic permeability with indicesl, m andn respectively are such thatl+m+n=0. Similar constraints on the indices apply for the existence of other simple solutions.
Based on an article first published in the
Based on an article first published in the IEE Power Engineering Journal 5(5) in September 1991