A side compound sharp crested weir is a flow diversion structure provided in one or both side walls of a channel to spill/divert water from the main channel Experimental programme for this study were conducted in Advance Hydraulic Laboratory of Department of Civil Engineering, Aligarh Muslim University, India. Dimensional analysis is carried out to estimate the functional relationship for the coefficient of discharge for
side compound weir. It is found that the coefficient of discharge depends on the approach flow Froude number, the ratio of the weighted crest height of the side weir to the length of the side weir and the ratio of the upstream depth in the channel to the length of side weir. On the basis of F-test, it is observed that P / Lis the most significant parameter for the prediction of Cd. The developed relationship using regression approach for the coefficient of discharge for side compound weir gives root means square error is 0.0634. The performance of the present model is based on the coefficient of correlation of the non-linear regression line between predicted values from the present model and desired output (R=0.8609), average percentage error (APE=-2.356), Absolute average deviation (AAD=13.406), Standard deviation (STDV=10.13) and scattering index (SI=0.1675).