Article

Effects of ECAP on the mechanical properties of Mg-Al2O3 nanocomposites

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Abstract

The purpose of this paper is the study of the effect of equal channel angular pressing (ECAP) on the mechanical properties of the Mg-Al2O3 nanocomposites. Magnesium and its alloys have excellent physical and mechanical properties for a number of applications. In particular its high strength: weight ratio makes it an ideal metal for automotive and aerospace applications, where weight reduction is of significant concern. Design/methodology/approach: Severe plastic deformation is a useful methodology to refine the grain size to the submicron or even nanometer size Findings: In the present work the influence of number of passes of ECAP by grain size, evolution of microstructure, mechanical properties and fracture of magnesium composites with different volume fraction of Al2O3 particles has been investigated by means of optical microscopy, tensile tests and scanning electron microscopy. Research limitations/implications: It has been found, that the grain size decreases with increasing number of passes. The mechanical properties of magnesium alloys are significantly influenced by the testing temperature leading to a decrease in the strength, by reinforcement and/or grain reinforcement leading to an increase in the strength. Originality/value: From previous studies, it was found that the MMCs using different size particles and different ECAP passes can improved the mechanical properties. But the research of Mg MMCs reinforcement with different wt.% nanoscale Al2O3 particles is not adequate.

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... Such limitations can be overcome with the incorporation of proper, harder, and stiffer ceramic particles such as SiC [4], Al 2 O 3 [7], CNT [8], etc., to fabricate a reinforced Mg metal matrix composite (MMC). The addition of single reinforcement particles can improve the specific strength, specific stiffness, creep, wear, and corrosion properties and provide enhanced wettability [4,9]. ...
Article
Magnesium is a low-density metal which is used in extensive structural applications such as load-bearing components in the automobile industry. To improve the strength and ductility of the magnesium alloys, method of production of metal matrix composites have been developed. In this study, AZ61 magnesium alloy was reinforced with hybrid particles (2 wt% Al2O3 and 1 wt% SiC) fabricated by the stir casting method. Then, the casted samples were homogenized at 410 °C for 24 h, aged at 200 °C for 10 h followed by severe plastic deformation (SPD) processing using equal channel angular pressing (ECAP). The obtained microstructure observation showed that the hybrid reinforcement particles were uniformly distributed in the metal matrix. After the ECAP process, the grain size was significantly reduced from 148.79±79 μm to 12.2±8 μm due to the dynamic recrystallization (DRX) mechanism during the plastic deformation. The mechanical properties of hardness, yield strength (YS), ultimate tensile strength (UTS), and elongation are effectively improved after each ECAP pass; the maximum values achieved were 61.2±4.6 HV, 110.3 MPa, 250.1 MPa, and 19.3%, respectively on the ECAP-2P AZ61/Al2O3/SiC hybrid composite. The enhancement of the mechanical properties of the AZ61 hybrid composites was mainly attributed to the Hall-Petch strengthening mechanism.
... Usually, light-weight materials reinforced using ceramic particles, such as SiC, Al 2 O 3 , TiB 2 , carbon nanotubes (CNT), and others, are used to produce MMCs [8][9][10][11][12][13]. Among these particles, SiC is the most applicable reinforcement for aluminum and magnesium alloys due to its high strength and hardness, low cost, and good compatibility with the metallic matrix. ...
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The work presents the results of the investigation of the influence of a submicrocrystalline structure, texture, and phase composition conditioned by different types of deformation–heat treatment (rolling, torsion strain on Bridgman anvils, lateral extrusion, and subsequent annealing) of copper, CuAlFe bronze and CuZnPb brass on wear resistance at dry sliding under the following conditions: sliding velocity 0.78 m s−1, pressure 0.2 to 10 MPa, and sliding distance 0.5 to 10 km. The results indicate an essential effect of some structural parameters (grain size, phase composition, texture) on wear resistance of this materials. Scanning electron microscopy observations were used to confirm the well-known mechanisms of `mild' wear of copper and bronze with submicrocrystalline structure and delamination of brass with microcrystalline structure under given conditions.
Wear Analysis for Engineers
  • R G Bayer
Bayer, R.G. (2002) Wear Analysis for Engineers, HNB Publishing, New York.
Verfestigung von aluminium mit metallischen dispersoiden (strengthening of aluminum with metallic dispersoids
  • G Jangg
  • F Kutner
  • G Korb
  • F Feher
Jangg, G., Kutner, F., Korb, G. and Feher F. (1975) 'Verfestigung von aluminium mit metallischen dispersoiden (strengthening of aluminum with metallic dispersoids)', Metall, Vol. 29, No. 10, pp.1014-1019.