Article

Effect of Drying Methods on Chemical Composition, Color and Antioxidant Properties of Thai Red Curry Powder

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Abstract

Thai red curry pastes were transformed into powder by two different drying methods: microwave and hot-air drying. The microwave drying was carried out in a microwave oven with output powers of 180, 360 and 540 W and the hot-air drying was carried out at air temperatures of 60, 70 and 80°C. The quality attributes of Thai red curry powder were evaluated for proximate composition, color (Hunter L, a and b) and antioxidant properties (total phenolic content and antioxidant activities). The Folin-Ciocalteu method was used to determine total phenolic content, while 2,2-diphenyl-1-picrylhydrazyl (DPPH) radical scavenging and ferric reducing antioxidative power (FRAP) assays were used to elucidate antioxidant activities. The drying methods showed no significant effects on the chemical compositions of the red curry powder, whereas color and antioxidant properties were all affected by the two methods to different extents. Microwave drying resulted in darker and less yellow color than the hot-air drying. Almost all red curry powder in the microwave-dried samples had a greater phenolic content and antioxidant activity than hot-air dried samples.

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... The highest contents of polyphenols in microwave-dried sage plants could be explained by the fact that the intense heat generated from the microwaves creates a high vapor pressure and temperature inside plant tissue, resulting in the disruption of plant cell wall polymers. Consequently, in certain cases, cell wall phenolics or bond phenolics could be released, thus causing more phenolics to be extracted (Inchuen et al. 2010). Among microwave-dried sage plants, augmenting microwave power from 600 to 800 W per 30 g of fresh plant significantly (p<0.05) ...
... However, the antioxidant activity of plant extracts cannot be evaluated using only one method, due to the complex composition of the phytochemical and oxidative processes (Inchuen et al. 2010). In fact, the antioxidant activity may be due to different mechanisms, such as prevention of chain initiation, decomposition of peroxides, prevention of continued hydrogen abstraction, free radical scavenging, reducing capacity, and binding of transition-metal ion catalysts (Mao et al. 2006). ...
... In fact, the antioxidant activity may be due to different mechanisms, such as prevention of chain initiation, decomposition of peroxides, prevention of continued hydrogen abstraction, free radical scavenging, reducing capacity, and binding of transition-metal ion catalysts (Mao et al. 2006). Therefore, at least two methods should be employed in order to evaluate the total antioxidant activity (Inchuen et al. 2010). ...
Article
In the current study, we determined the effects of seven drying methods on total phenolics, flavonoids, individual phenolics, and antioxidant activity of the methanol extract of Salvia officinalis L. As compared with total phenolic content (TPC) of fresh plants, results showed that the highest TPC was recorded in plants dried by microwave (MW) at a power of 800 W/30 g of fresh plant and was 4.2 times higher than that of fresh plants whereas the lowest content was found in the case of plants dried by far-infrared (FIR) at 45 °C. The analysis of the different extracts by RP-HPLC showed a predominance of phenolic acids particularly in fresh plants and those dried by MW (600 W/30 g of fresh plant) whereas flavonoids predominate in the case of plants dried by FIR (65 °C). The assessment of the radical scavenging activity (RSA) against the stable radical 1,1-diphenyl-1-picrylhydrazyl (DPPH) showed an increase in the scavenging effect particularly in MW (800 W/30 g of fresh plant) dried plants with an IC50 = 13.49 μg ml−1 (IC50 is the concentration required to cause 50 % DPPH inhibition). The complementary assessment of the RSA using the β-carotene/linoleic acid system showed an increase of this activity for all extracts and particularly for the extract derived from MW (600 W/30 g of fresh plant) dried plants as compared to fresh ones. Finally, all the plant extracts showed moderate reducing power as assessed by the ferric-reducing antioxidant potential. These results suggested that MW drying could be applied to retain phenolic contents and to enhance antioxidant activity of sage plant materials.
... The highest contents of polyphenols in microwave-dried sage plants could be explained by the fact that the intense heat generated from the microwaves creates a high vapor pressure and temperature inside plant tissue, resulting in the disruption of plant cell wall polymers. Consequently, in certain cases, cell wall phenolics or bond phenolics could be released, thus causing more phenolics to be extracted (Inchuen et al. 2010 Cluster analysis was carried out to determine the relationship between the different drying methods on the basis of their TPC (Fig. 2). Results obtained showed the existence of one well-defined group represented by the methods MW (600 W/ 30 g of fresh plant), ambient air, oven (45 °C), oven (65 °C), IR (45 °C), and IR (65 °C) together with fresh plants suggesting similar compositions. ...
... Several analytical methods have been developed to determine the antioxidant capacity of natural substances in vitro. However, the antioxidant activity of plant extracts cannot be evaluated using only one method, due to the complex composition of the phytochemical and oxidative processes (Inchuen et al. 2010). In fact, the antioxidant activity may be due to different mechanisms, such as prevention of chain initiation, decomposition of peroxides, prevention of continued hydrogen abstraction, free radical scavenging, reducing capacity, and binding of transition-metal ion catalysts (Mao et al. 2006). ...
... In fact, the antioxidant activity may be due to different mechanisms, such as prevention of chain initiation, decomposition of peroxides, prevention of continued hydrogen abstraction, free radical scavenging, reducing capacity, and binding of transition-metal ion catalysts (Mao et al. 2006). Therefore, at least two methods should be employed in order to evaluate the total antioxidant activity (Inchuen et al. 2010). In our study, DPPH radical scavenging, β-carotene bleaching , and ferric-reducing antioxidant potential (FRAP) methods were used to evaluate the antioxidant activity and results were summarized inTable 3. We noticed that all the studied extracts (from fresh and dried plants) were able to scavenge the DPPH free radical to different degrees. ...
... This activity of the extract is related to its high phenolic content (phenols, flavonoids and flavonols) found in this part of the plant compared to other extracts. Antioxidant activity of polyphenols from natural origin occurs in various mechanisms such as the prevention of chain initiation, peroxide decomposition, the prevention of further hydrogen abstraction, trapping free radicals, reducing ability, and the binding of transition metal ions [45]. Phenolic compounds have the ability to transfer hydrogen atoms which are generally associated with the presence of reducing agents [45,46]. ...
... Antioxidant activity of polyphenols from natural origin occurs in various mechanisms such as the prevention of chain initiation, peroxide decomposition, the prevention of further hydrogen abstraction, trapping free radicals, reducing ability, and the binding of transition metal ions [45]. Phenolic compounds have the ability to transfer hydrogen atoms which are generally associated with the presence of reducing agents [45,46]. In addition, the number and position of the hydroxyl groups of phenolic compounds also regulate their antioxidant activity [45]. ...
... Phenolic compounds have the ability to transfer hydrogen atoms which are generally associated with the presence of reducing agents [45,46]. In addition, the number and position of the hydroxyl groups of phenolic compounds also regulate their antioxidant activity [45]. The determination of antioxidant properties of the extract through radical scavenging (DPPH, ABTS, OH and NO) is considered to be a good indication of the ability of antioxidants to divest hydrogen even though they are not biologically relevant [47]. ...
Article
Full-text available
The aim of this study was to determine the in vitro antioxidant activity, free radical scavenging property and the beneficial effects of extracts of various parts of Syzygium guineense in reducing oxidative stress damage in the liver. The effects of extracts on free radicals were determined on radicals DPPH, ABTS, NO and OH followed by the antioxidant properties using Ferric Reducing Antioxidant Power assay (FRAP) and hosphomolybdenum (PPMB). The phytochemical screening of these extracts was performed by determination of the phenolic content. The oxidative damage inhibition in the liver was determined by measuring malondialdehyde (MDA) as well as the activity of the antioxidant enzymes superoxide dismutase (SOD), catalase (CAT) and peroxidase. Overall, the bark extract of the ethanol/water or methanol showed the highest radical scavenging activities against DPPH, ABTS and OH radicals compared to the other extracts. This extract also contained the highest phenolic content implying the potential contribution of phenolic compounds towards the antioxidant activities. However, the methanol extract of the root demonstrated the highest protective effects of SOD and CAT against ferric chloride while the hydro-ethanol extract of the leaves exhibited the highest inhibitory effects on lipid peroxidation. These findings suggest that antioxidant properties of S. guineense extracts could be attributed to phenolic compounds revealed by phytochemical studies. Thus, the present results indicate clearly that the extracts of S. guineense possess antioxidant properties and could serve as free radical inhibitors or scavengers, acting possibly as primary antioxidants. The antioxidant properties of the bark extract may thus sustain its various biological activities. Keywords: antioxidant activity; phenolic content; Syzygium guineense; radical scavenging activity; lipid peroxidation
... This activity of the extract is related to its high phenolic content (phenols, flavonoids and flavonols) found in this part of the plant compared to other extracts. Antioxidant activity of polyphenols from natural origin occurs in various mechanisms such as the prevention of chain initiation, peroxide decomposition, the prevention of further hydrogen abstraction, trapping free radicals, reducing ability, and the binding of transition metal ions [45]. Phenolic compounds have the ability to transfer hydrogen atoms which are generally associated with the presence of reducing agents [45,46]. ...
... Antioxidant activity of polyphenols from natural origin occurs in various mechanisms such as the prevention of chain initiation, peroxide decomposition, the prevention of further hydrogen abstraction, trapping free radicals, reducing ability, and the binding of transition metal ions [45]. Phenolic compounds have the ability to transfer hydrogen atoms which are generally associated with the presence of reducing agents [45,46]. In addition, the number and position of the hydroxyl groups of phenolic compounds also regulate their antioxidant activity [45]. ...
... Phenolic compounds have the ability to transfer hydrogen atoms which are generally associated with the presence of reducing agents [45,46]. In addition, the number and position of the hydroxyl groups of phenolic compounds also regulate their antioxidant activity [45]. The determination of antioxidant properties of the extract through radical scavenging (DPPH, ABTS, OH and NO) is considered to be a good indication of the ability of antioxidants to divest hydrogen even though they are not biologically relevant [47]. ...
Article
Full-text available
The aim of this study was to determine the in vitro antioxidant activity, free radical scavenging property and the beneficial effects of extracts of various parts of Syzygium guineense in reducing oxidative stress damage in the liver. The effects of extracts on free radicals were determined on radicals DPPH, ABTS, NO and OH followed by the antioxidant properties using Ferric Reducing Antioxidant Power assay (FRAP) and hosphomolybdenum (PPMB). The phytochemical screening of these extracts was performed by determination of the phenolic content. The oxidative damage inhibition in the liver was determined by measuring malondialdehyde (MDA) as well as the activity of the antioxidant enzymes superoxide dismutase (SOD), catalase (CAT) and peroxidase. Overall, the bark extract of the ethanol/water or methanol showed the highest radical scavenging activities against DPPH, ABTS and OH radicals compared to the other extracts. This extract also contained the highest phenolic content implying the potential contribution of phenolic compounds towards the antioxidant activities. However, the methanol extract of the root demonstrated the highest protective effects of SOD and CAT against ferric chloride while the hydro-ethanol extract of the leaves exhibited the highest inhibitory effects on lipid peroxidation. These findings suggest that antioxidant properties of S. guineense extracts could be attributed to phenolic compounds revealed by phytochemical studies. Thus, the present results indicate clearly that the extracts of S. guineense possess antioxidant properties and could serve as free radical inhibitors or scavengers, acting possibly as primary antioxidants. The antioxidant properties of the bark extract may thus sustain its various biological activities.
... Total phenolics increased to 2.83 mg/g d.m. from 1.08 mg/g d.m. when the microwave power increased to 600 W from 90 W at the same thickness value (Figure 2). This result is consistent with the other studies related with Thai red curry powder (Inchuen et al., 2010) and dried sage plants (Sellami et al., 2013). Another research about extraction of phenolic compounds in dried mushrooms by using oven and microwave, total phenolics increased with microwave power (Celebi Sezer et al., 2017). ...
... It is reported that plant cell wall polymers can deteriorate when intense heat formed from the microwaves leads a high vapor pressure and temperature in the tissue. So, cell wall phenolics or bond phenolics could be released and more phenolics could be extracted (Inchuen et al., 2010;Sellami et al., 2013). ...
... This increment could be explained that the deterioration of plant tissue increased with a rise in the power of microwave, causing more phenolic compounds to be released. So antioxidant activity increases (Inchuen et al., 2010). Similar results observed compared to the other studies related with dried asparagus (Nindo et al., 2003), strawberry (Wojdylo et al., 2009), Thai red curry powder (Inchuen et al., 2010) and sour cherry (Wojdylo et al., 2014). ...
Article
This study was conducted to investigate hot-air and microwave dryings on phenolics and antioxidant activity of dried white button mushroom slices (Agaricus bisporus) using the response surface methodology. It was also aimed to determine optimized drying conditions. In hot-air drying, total phenolics content reduced with corresponding increase in drying temperature and slice thickness, whereas in microwave drying, the total phenolics content increased with microwave power. Although the effect of drying temperature on antioxidant activity is not significant, there is a decrease in antioxidant activity as the slice thickness of the samples increases. Microwave power had also a significant linear effect on antioxidant activity of dried samples (p<0.01). Both increases and decreases in individual phenolic compounds were detected with the change of drying conditions and sample thickness. A quadratic model was well fitted to all responses. As a result of numerical optimization, optimum conditions for hot-air drier and microwave oven were suggested as 50 °C and 600 Watt having mushroom slices of 2 mm thickness, respectively. Our results show that the quality of dried mushroom depends on the drying method and conditions. Also, microwave drying is suitable method for drying of mushroom slices within a shorter time compared with hot-air drying.
... Consequently, in certain cases, cell wall phenolics or bound phenolics could be released, thus causing more phenolics to be extracted [68]. These results are in agreement with those of Inchuen et al. [69] who reported that increasing microwave power from 180 to 540 W resulted in an increase of the TPC of Thai red curry powder. Besides, according to Inchuen et al. [69], the highest content of phenols in microwave-dried samples could be attributed to the formation of new products by Maillard reaction and intermediate products of non-enzymatic browning; some compounds were undesirable from a nutritional point of view. ...
... These results are in agreement with those of Inchuen et al. [69] who reported that increasing microwave power from 180 to 540 W resulted in an increase of the TPC of Thai red curry powder. Besides, according to Inchuen et al. [69], the highest content of phenols in microwave-dried samples could be attributed to the formation of new products by Maillard reaction and intermediate products of non-enzymatic browning; some compounds were undesirable from a nutritional point of view. The increase of TPC of infrared dried lemon peel at high temperature could also be explained by the formation of antioxidant compounds by Maillard reaction and intermediate products of non-enzymatic browning. ...
Article
Full-text available
The aim of this work is to establish a comparative investigation of the effect of different drying processes: microwave dehydration (100–600 W), air drying (40–60 °C) and infrared drying (40–60 °C) on drying kinetics and on the main quality attributes (color, total phenols and flavonoids contents, water and oil retention capacities) kinetics’ of lemon (Citrus limon. v. lunari) peels. The experimental drying kinetics’ of lemon peels were fitted to nine thin layer drying models. The Midilli and Kucuk model showed a better fit to experimental drying data for the three drying processes. Microwave drying at 450W preserved the maximum phenols (1.855 ± 0.016 g CAE/100 g DM) and flavonoids (0.802 ± 0.072 g RE/100 g DM) contents respectively. An increase of phenol content was noticed after 9, 13 and 14 min of microwave drying at 600, 450 and 300 W and after 156, 102 and 54 min of infrared drying at 40, 50 and 60 °C. A first-order kinetic model adequately fitted, at the beginning of drying processes, the change of total phenols and flavonoids contents. Total color difference (ΔE) increased progressively with increasing drying time and temperature or microwave power level. ΔE showed a zero-order model whatever the applied drying process. Water retention capacity (WRC) of dried lemon peels decreased during drying processes. However, infrared and microwave drying increased the oil retention capacity (ORC) of lemon peels. The WRC and ORC followed first-order kinetics during air drying and a second order polynomial model during microwave and infrared drying processes.
... Antioxidant activity of tomato slices increased with increasing drying temperature from 50 to 70°C but decreased as drying time progressed from 30 to 300 min. The trend in our results is similar to previously published results obtained for tomato (Dewanto et al., 2002;Kamiloglu et al., 2014;Kamiloglu et al., 2016), Kappaphycus alvarezii (Ling et al., 2015), Thai red curry powder (Inchuen et al., 2010), red guava (Nora et al., 2014) and fruit plum powder (Michalska ...
... The increase was related to the increase in the release of bound phenolics from the cell wall as a result of heat treatment that breaks down the ester between phenolic and cell wall. Decrease in total phenolic with increasing drying time at all temperatures could be due to the long drying time which has been reported to destroy some phenolic compounds (Li et al., 2007;Garau et al., 2007;Inchuen et al., 2010;Gupta et al., 2011;Ling et al., 2015). ...
Article
Full-text available
This study investigated the influence of drying temperature, and time on antioxidant activity, phenolic, flavonoid, lycopene and β – carotene contents of tomato slices. It also evaluated the influence of drying process on drying kinetics, moisture diffusivity and activation energy. Oven processed tomato slices had temperature-dependent significant increase in antioxidant activity at 30 and 60 min, phenolic from 30 - 120 min and lycopene contents from 120 - 300 min. Significantly decreased contents of flavonoid and β – carotene were obtained for oven processed tomato slices with increasing drying temperature and time. Page model accurately predicted the drying process of tomato slices. Similarity between experimentally determined moisture ratio and Page predicted moisture ratio was obtained with high correlation (R² = 0.9986). Effective moisture diffusivities indicated that drying process of tomato slices was temperature dependent while Arrhenius equation explained the relationship between activation energy and temperature.
... tek bir yöntem yoktur ve en iyi çözüm tek boyutlu bir yaklaşım yerine çeşitli yöntemler kullanmaktır [186]. Bitki ekstraktların antioksidan aktivitesi fitokimyasal ve oksidasyon işlemlerin karmaşık kompozisyonuna bağlı olarak sadece bir yöntem kullanarak değerlendirilemeyeceğini ileri sürülmüştür [187]. Çünkü her yöntemin kendine ait avantajı ve dezavantajı bulunmaktadır. ...
... Mikrodalga-vakum kurutma işlemi esnasında fiber optik termometre (sıcaklık probları) Yapmış olduğumuz çalışma, Inchuen vd. [187], Tay kırmızı köri tozunun 180 ila 540 W arasında artan mikrodalga gücünde artan TPC ile sonuçlandığını bildiren çalışma ile benzerlik göstermektedir. Ayrıca literatürde benzerlik gösteren birçok çalışma daha mevcuttur. ...
Thesis
Drying is a preservation process commonly used in the food industry. Today, hot-air drying is commonly used to preserve products that do not have a long shelf life such as fruit and vegetables. However, considering the quality losses and long drying times of the final products dried by this method, new drying techniques have started to be used recently. In this study, it was aimed to investigate the effect of microwave-vacuum drying (<10% moisture content) on the drying time characteristic and some quality properties of rosehip. In accordance with this purpose, the drying process was performed under different microwave power (50, 100, and 150 W) and absolute pressures (40, 75 and 110 mbar). Power and pressure effects on quality characteristics were determined. Freeze drying and hot air drying (60 ° C-1.5 m / s) methods were also investigated. The effect of three drying methods on some chemical and physical quality characteristics of dried rose hip was determined and compared. The drying time to the target moisture content by microwave-vacuum method is 75-195 minutes. The shortest drying time was observed under high power and low absolute pressure conditions. In all chemical analysis results (total phenolic content, total antioxidant activity amount and ascorbic acid amount), the lowest value was found in hot-air dried samples. Dried samples with hot-air were found to have the lowest value in all chemical analysis results (Total phenolic content, total antioxidant activity amount and ascorbic acid amount). Total phenolic content was highest in all microwave-vacuum dried samples. Most of the microwave vacuum dried samples had higher total antioxidant activity amount than freeze-dried samples. However, the highest amount of ascorbic acid (vitamin C) was obtained in freeze-dried samples after fresh sample. While the dried samples with Microwave-vacum and freeze drying had a similar open and porous microstructure, the dried samples with hot-air had a completely closed and non-porous structure. Therefore, the rehydration rate values of microwave-vacuum and freeze drying samples were higher than those of hot-air samples. At high microwave powers (150 W) and freze drying dried samples were found rehydration rate was highest and there was no statistically significant difference between them.
... (Nimse & Pal, 2015) and phenolic compounds (Huyut, Beydemir, & Gülçin, 2017;Loganayaki, Siddhuraju, & Manian, 2013). At least two methods should be employed to evaluate the total antioxidant activity due to different mechanisms of antioxidants, such as prevention of chain initiation, decomposition of peroxides, prevention of continued hydrogen abstraction, free radical scavenging, reducing capacity, and binding of transition metal ion catalysts (Inchuen, Narkrugsa, & Pornchaloempong, 2010). Therefore, DPPH and FRAP assays were used to determine the antioxidant activity of the samples under various drying conditions (Mao, Pan, Que, & Fang, 2006). ...
... The highest DPPH radical scavenging and TPC values were also found in the samples dried at 25°C indicating that DPPH free radical scavenging was direct correlations to TPC. Correlations between TPCs and DPPH radical scavenging activity were also reported in other studies about the drying of fruits and vegetables (Inchuen et al., 2010;İzli, Yıldız, Ünal, Işık, & Uylaşer, 2014;Sultana, Anwar, Ashraf, & Saari, 2012). In this study, it was found that the DPPH radical scavenging ability and TPC had a positive correlation with high R-squared value (0.94). ...
Article
Full-text available
Bitter melon (Momordica charantia L.) is a fruit that brings health benefits to consumers because the fruit is rich in bioactive compounds. In this work, a combination of low‐temperature convective drying and microwave radiation was used to dehydrate sliced bitter melon. One‐factor‐at‐a‐time design was performed to evaluate the influence of microwave power density (1.5, 3.0, 4.5 W/g), drying temperatures (20, 25, and 30°C), and air velocity (1.0, 1.2 and 1.4 m/s) on the change of moisture content, nutrient levels (vitamin C and total phenolics), and the antioxidant activities (DPPH and FRAP assays) of the bitter melon. The obtained results showed that all investigated factors affected the rate of moisture removal. Microwave power density output and air‐drying temperature strongly participated in the retention of nutrients. In this study, the drying process was driven by both heat and mass transfer processes, so the increase of air velocity prolonged the drying time causing more loss of nutrient levels and antioxidant activities. It was found that DPPH free radical scavenging ability directly correlated with total phenolic content, but the ferric‐reducing antioxidant power was related to the presence of reductants including phenolic compounds, vitamin C, and other phytochemicals in bitter melons. This work determined that microwave power density and the air‐drying temperature are the main two factors that should be used for further investigations. The effects of drying conditions in the convective low‐temperature microwave‐assisted drying of bitter melon were investigated. The results were used to develop an understanding of how the microwave power density, drying temperature, and air velocity affect the final quality of the dried fruit product.
... However, the antioxidant activity of plant extracts cannot be evaluated using one method due to the complex composition of the phytochemical and oxidative processes. [39] In fact, the antioxidant activity may be attributed to different mechanisms, such as prevention of chain initiation, decomposition of peroxides, prevention of continued hydrogen abstraction, free radical scavenging, reducing capacity, and binding of transition-metal ion catalysts. [40] Therefore, at least two methods should be employed to evaluate the total antioxidant activity. ...
... [40] Therefore, at least two methods should be employed to evaluate the total antioxidant activity. [39] In our study, DPPH radical scavenging and FRAP methods were used to evaluate the antioxidant activity (results summarized in Table 3). All the studied extracts (from fresh and dried onion samples) were able to scavenge the DPPH free radical to different extents. ...
Article
The effects of four drying treatments (freeze-drying, hot air-drying, oven drying and vacuum oven drying) on the bioactive compounds (total phenolics, total flavonoids and quercetins), colour and antioxidant capacity of organic and non-organic onions of two varieties (Red Baron and Hyfort) subjected to two agronomic treatments (OSOP and CSCP) were investigated. The average final dry weight of the samples was 9.82 ±0.41 %. After drying, there was a significant increase in total phenolics, total flavonoids, total quercetin and antioxidant capacity in comparison with fresh onion samples, which suggested that drying can improve the extractability of phenols and accordingly the antioxidant activity of onions. Different drying techniques also resulted in different fractions of individual quercetins. Dried organic onions had higher levels of bioactive compounds and antioxidant capacity than dried non-organic onions for a same variety. The highest antioxidant capacity displayed by freeze-dried and hot air-dried organic Red Baron onion is in agreement with their higher phenolic and flavonoid contents compared to all other samples.
... Colour is an important attribute of dried product from the consumer's acceptability view (Inchuen et al., 2010). It is also considered as an important quality indicator for acceptance of the final product in the market (Soysal, 2004).The results shows that drying temperature and time are the main factors affecting the colour of dried lemongrass leaves for tea. ...
Article
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The aim of this study was to investigate the effect of drying on quality and sensory attributes of lemon grass (Cymbopogon citratus) tea. Lemongrass (C. citratus) leaves were dried using four different drying methods: sun, solar, oven (40, 50, and 60°C), and microwave (50 W). Teas made from the grass were analyzed for colour, pH and sensory attribute. Data obtained were statistically analyzed using SPSS Version 23 one way analysis of variance and means were compared using Duncan multiple comparison test (p ˂ 0.05). Results obtained indicate that after drying the moisture content were significantly reduced. Ash content results showed no significant difference amongst lemongrass samples dried under difference drying methods. However, there was a significant difference (p < 0.05) in the pH of tea made from the lemongrass dried under different drying methods. Results indicate that drying temperature and time are the main factors affecting the colour of dried lemongrass leaves for tea. There was a significant difference (p < 0.05) in the colour profile of the dried leaves. Sensory evaluation results showed that the colour, aroma, taste, and overall acceptability scores of tea from lemongrass dried with oven at 40°C was highest. The study revealed that oven drying at 40°C for 15 hours was found to be most suitable for drying of lemongrass leaves for tea production in order to retain appreciable sensory attributes.
... The highest TPC was recorded at 500 W (48.44 mg GAE/g) while the lowest one was at 100 and 700 W (29.33 and 30.39 mg GAE/g). According to Inchuen et al. (2010), the highest TPC in microwave-dried sage plants could be explained by the fact that the intense heat generated from the microwaves creates a high vapour pressure and temperature inside plant tissue, resulting in the disruption of plant cell wall polymers thus causing more phenolics to be extracted. However, excessive output power (or temperature) led to the decrease of antioxidant compounds (Dong et al., 2011). ...
Article
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In the present study, the effects of two drying methods on antioxidant properties of coriander leaves were investigated. For the rate of drying, results showed that sample weight stability was reached faster in microwave (900 W/70 s) than in oven drying (120°C/290 s). Concerning antioxidants, results showed that the highest total polyphenols and total flavonoids contents were recorded by leaves dried in microwave (48.44 mg GAE/g and 20.28 mg RE/g, respectively) than those dried in oven (26.64 mg GAE/g and 19.60 mg RE/g, respectively). At the end, the assessment of radical scavenging activity against stable radical ABTS and DPPH showed an increase in scavenging effect particularly when microwave technology was used.
... This revelation suggests that phenolic compounds might contribute to the antioxidant capacity. Positive correlations between TPC and antioxidant capacity were also revealed by studies carried out on other foods [41,42]. Degradation of phenolic compounds or loss of antioxidant constituents of the kiwi samples may be the reason of the reduction in antioxidant capacity in consequence of drying treatment [41]. ...
Article
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This study analysed the convective (60, 70 and 80° C), microwave (120 and 350 W) and freeze drying methods in terms of their effects on the drying characteristics, colour, total phenolic content (TPC) and antioxidant capacity of kiwi slices. Nine different mathematical models were applied to experimental data to achieve the most accurate calculation for drying curves. The Midilli et al. and Wang and Singh models proved to be the most suitable at explaining the drying kinetics of kiwi samples as compared to other models according to the statistical tests. Each drying method was significantly affected by colour parameters (L*, a*, b*, C, α and ΔE). The dried samples exhibited respectively 5–49 % and 10–47 % less TPC and antioxidant capacity compared to the fresh sample. According to the correlation analysis conducted between TPC and antioxidant capacity for kiwi slices, there is a positive correlation (R2 = 0.7796). Microwave dried samples at 120 W particularly had the lowest TPC and antioxidant capacity. Freeze drying method yielded the closest values with respect to colour values, total phenol content and antioxidant capacity to those of fresh samples when compared to the other methods.
... The composition of Thai red curry powder reportedly consists of crude protein, crude fat, and crude fiber. [25] However, based on this result, approximately 88% of both Keang-hleung pastes (P1 and P2) would reach the colon if consumed, since some of the pastes were hydrolyzed by salivary α-amylase (3.38% and 3.41%), stomach acid (1.46% and 1.58%), and human pancreatic α-amylase (6.69% and 6.80%). Therefore, the totally and partially hydrolyzed material in the mouth, stomach, and small intestine was approximately 12%, indicating that the curry paste (P1 and P2) may contain non-digestible components other than carbohydrates. ...
Article
The prebiotic properties of sour curry paste in the upper gut and the gut microbiota were investigated in vivo during digestion. The effect of the addition of garcinia as souring agent in curry paste was studied. Curry paste without garcinia (P1) and curry paste with garcinia (P2) increased the number of beneficial bacteria in the gut microbiota, especially bifidobacteria and lactobacilli, and significantly (p<0.05) decreased the number of harmful bacteria (Clostridia). Fecal fermentation with P1 resulted in a prebiotic index (PI) of 1.19, whereas fermentation with P2 resulted in a PI of 2.75. The fermented metabolites produced were lactic acid; vitamins; and short-chain fatty acids (SCFAs) such as acetic acid, propionic acid and butyric acid. P1 produced metabolites including lactic acid, SCFAs and B vitamins in higher amounts than P2. After a 24 h fermentation period with colonic microbiota, P1 produced vitamins B1 (18.38 ± 0.10 µg/ml) and B2 (45.28 ± 2.02 µg/ml) but not folic acid, whereas P2 produced only vitamin B1 (5.99 ± 0.48 µg/ml).
... However, our findings were in agreement with a previous study on sage (Salvia officinalis L.) plants where microwave drying enhanced recovery of phenolic compounds in the dried sample [17] . Inchuen, et al. [43] attribute this to the intense heat generated from microwaves can create high vapour pressure inside the plant tissue, resulting in the disruption of plant cell wall polymers. Consequently, in certain cases, bonded phenolics could be released, resulting in increased quantities of phenolics being extracted. ...
Article
A significant amount of banana peels is generated as waste annually and shows great potential as a lead material for further utilisation in the nutraceutical industry. However, potentiality of banana peel utilization largely depends on the favourable drying condition of the material before it can be used for further processing. Therefore, it is necessary to identify the suitable drying conditions for banana peel. This study investigated the effect of six different drying methods on the quality of banana peels. The results showed that different drying conditions significantly affected the physical, chemical and antioxidant properties of dried peels. Microwave irradiation at the power level of 960 W for 6 min was the most suitable condition, as these dried peels had good physical properties, minimum loss of bioactive compounds and antioxidant properties. This was followed by freeze drying, vacuum oven at 60 °C, hot air oven at 120 °C, dehumidified air at 60 °C and sun drying. The peels dried by microwave possessed a total phenolics content of 25.26 mg GAE/g DM and potent antioxidant capacity (DPPH of 37.70; ABTS of 46.35; FRAP of 45.94, and CUPRAC 64.55 mg TE/g DM). Therefore, the study recommends the use microwave irradiation under the studied condition (power level of 960 W for 6 min) for further processing and utilisation.
... This showed that there is a good relationship between TPC and TAA. The reduction and a similar relationship between TPC and TAA were also observed in drying of Thai red curry powder (Inchuen, Narkrugsa, & Pornchaloempong, 2010), goldenberry (Izli, Yildiz, Unal, Isik, & Uylaser, 2014) and other fruits (Sultana, Anwar, Ashraf, & Saari, 2012). It can also be noted that the TAA of germinated red lentils was higher than green lentils at same processing conditions, except for runs 2, 4 and 6. ...
Article
The aim of this study was to optimize the processing parameters of pulse mode microwave-vacuum drying of germinated green and red lentils (CDC Greenland and CDC Maxim) and investigate the changes in their total phenolic content (TPC), total antioxidant activity (TAA) and In-vitro starch digestibility (SD). The lentils were germinated for 5 days and dried by a pulse mode microwave-vacuum method, using 2 s to 8 s out of 10 s pulsed mode at 2000W microwave power and varying the vacuum pressure level between 15 and 45 kPa. In-vitro starch digestibility increased significantly with increased microwave power level. The TPC and TAA appeared to vary distinctively in the two varieties of selected lentils. Vacuum pressure levels did not significantly (p > 0.05) affect any responses. Green lentils could be dried at 8 s microwave power and 45 kPa vacuum pressure and red lentils could be dried at 5.5 s microwave power and 42.19 kPa vacuum pressure. The microwave-vacuum drying showed great potential for the drying of germinated lentils.
... The attributes of three color parameters (L*, a*, b*) were found by Sudathip et al. [31] , who reported the values of (L*, a*, b*) of Thai red curry powder when using hot-air drying were higher than microwave drying. ...
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Four different fresh and dried herb species (sage, thyme, mint and lemonbalm) were evaluated to study the effect of drying process on the total phenolics, antioxidant activity, flavonoid contents and color properties. Fresh mint had the highest contents of total phenolics (335.4 mg GAE/100 g), whereas lower levels were respectively found in sage (316.4 mg GAE/100 g) followed by lemonbalm (303.2 mg GAE/100 g) and thyme (299.2 mg GAE/100 g). Dry processing significantly decreased the phytochemical contents of all investigated herbs. Compare to air drying, total phenolics, antioxidant activity and flavonoids content in herbs decreased apparently by oven dried. Fresh mint had the highest antioxidant activity (87.46%) and flavonoids content (298.51 mg CE/100 g), while the fresh sage, thyme and lemonbalm were found to have antioxidant activity values of 86.81%, 86.56% and 85.26%, respectively. Results showed that air drying herbs contained more total phenolics, antioxidant activity, and flavonoids than oven drying herbs.
... The intense heat generated from microwaves creates a high vapor pressure and temperature inside plant tissue, resulting in the disruption of plant cell wall polymers [20]. Consequently, cell wall phenolics or bond phenolics can be released, thus causing even more phenolics to be extracted [21]. However, more studies are needed to understand how structural modifications caused by microwaves influence the extraction of phenolic compounds. ...
Article
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The objective of this research was investigated the effect of polyphenol oxidase microwave treatment on phenolic composition, antioxidant activity and microstructure of loquat fruit. Phenolic profile of methanolic extracts prepared from fresh, and microwave-treated samples were analyzed. Antioxidant activity was also evaluated by 2,2’-azinobis (3-ethylbenzothiazoline-6-sulfonic acid) (ABTS •+ ) and 1,1-diphenyl-2-picrylhydrazyl (DPPH + ) methods. In addition, polyphenol oxidase inactivation was carried out using a response surface methodology to establish the optimal conditions of treatment. The phenolic content of fresh mesocarp was 311 ± 0.60 mg gallic acid equivalents (GAE)/100g dry weight (DW) and that of microwave-treated mesocarp was 1230 ± 0.36 mg GAE/100g DW. Total phenolic content of water/ methanol extract significantly increases after microwave treatment rather than methanolic extract of fresh loquat. Five glycoside phenolics were identified by HPLC-DAD-MS as 3-caffeoylquinic acid, 3-p-coumaroylquinic acid, 5-caffeoylquinic acid and quercetin-3-O-sambubioside. Methanolic extract of microwave-treated mesocarp showed higher antioxidant activity than that of fresh mesocarp. Thus, polyphenol oxidase inactivation by microwave energy preserved the integrity of phenolic compounds as well as antioxidant activity in mesocarp extracts prepared from loquat fruit. It was also noted that phenolics were more abundant in the microwaved samples than in the fresh samples.
... scorbic acid in TD sample was observed as compared to IR dried sample. In our study, ascorbic acid in jambhul and wood apple at 80 °C was high as compared to those sample dried at 60 °C in tray dried as well as in IR drying. Madrau et al. (2009) found that the ascorbic acid in apricot at 75 °C air flow cabinet dried highest to those dried at 55 °C. Gregory (2008) reported that the loss in vitamin C content during drying involves oxidation and hydrolysis. The ascorbic acid is oxidized to dehydroascorbic acid, followed by hydrolysis to 2, 3-diketogulonic acid and further oxidation and polymerization to form a wide range of other nutritionally inactive products. From Table 1 it can be seen that the ...
Article
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Jambhul and wood apple were subjected to two different drying methods to examine the effect of drying temperatures (80 °C and 60 °C) and influence of storage conditions viz., room temperature (25 °C) and refrigeration temperature (4 °C) on bioactive constituents of jambhul and wood apple powder for 90 days. Results showed that retention of phenolics, ascorbic acid and antioxidant capacity such as ABTS, DPPH and FRAP in jambhul and wood apple were high at 80 °C as compared to 60 °C in both tray and IR drying. Anthocyanin and flavonoid significantly (p<0.05) decreased at 80 °C. Jambhul showed retention of 30.83 %TPC, 10.40% TFC, 9.31 %, TMAC, 12.75 % ascorbic acid, 19.26 % ABTS activity, 98.71 % DPPH activity, and 27.78 % FRAP activitys in IR drying; whereas wood apple showed more retention of 25.74 % TPC, 61 % ascorbic acid, 10.31 % ABTS, 36.45 % DPPH and 0.27 % FRAP in tray drying (TD). During storage bioactive constituents in jambhul powder were preserved at refrigeration temperatures whereas in wood apple they were retained at room temperature.
... In this study, the antioxidant capacities of the samples are proportional to their total phenolic contents (Fig. 3). Positive correlations between total phenolic content and antioxidant capacity have also been reported for other foods (Inchuen et al., 2010;Sultana et al., 2012). The reduction in antioxidant capacity as a result of drying process might be caused by degradation of phenolic compounds or loss of antioxidant constituents of the goldenberry samples (Sultana et al., 2012). ...
Article
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In this study, the effects of convective, microwave and microwave–convective drying methods on the drying characteristics, colour, total phenolic content and antioxidant capacity of goldenberry fruits were investigated. To select the most appropriate thin-layer drying model for drying treatments, nine mathematical drying models were fitted to the experimental data. Based on the statistical tests used for evaluation, the Midilli et al. and Wang and Singh models were considered the best models to describe the drying behaviours of goldenberry fruits in all drying methods. The colour values (L*, a* and b*) of fresh fruit were decreased by drying. Compared with the fresh sample, the dried samples exhibited a 64–75% and 65–75% decrease in total phenolic content and antioxidant capacity, respectively. Among the different drying treatments, the values closest to those of fresh samples with respect to colour values, total phenolic content and antioxidant capacity were achieved with the 160 W microwave drying method.
... This heat resulted in disruption of the plant cell wall polymers due to the production of high vapor pressure and temperature inside the plant tissues. Therefore, more phenolic could be released [47]. Meanwhile, the heat from hot air oven drying resulted in the vaporization of volatile compound that causes the loss of compound in the water vapor [48]. ...
Article
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Objective: This study aimed to evaluate the effect of oven and microwave drying on total phenolic content (TPC), total flavonoid content (TFC), and antioxidant capacity of unfermented and fermented tea developed from Strobilanthes crispus leaves.Methods: TPC and TFC were estimated using a spectrophotometric method, while antioxidant capacity was determined using ferric reducing antioxidant power assay and 2,2-diphenyl-1-picrylhydrazyl radical scavenging assay. Camellia sinensis (tea plant), that is, used for the production of all varieties of commercial tea and fresh S. crispus leaves were served as controls in this study.Results: The highest antioxidant activity and TPC were observed in S. crispus tea developed from microwave-dried leaves, while the highest TFC was observed in oven-dried tea. Unfermented S. crispus tea showed significantly higher values (p<0.05) for antioxidant activity, TPC, and TFC as compared to fermented S. crispus tea. A strong and moderate correlation was observed between antioxidant activity and TPC as well as TFC values.Conclusion: The present work clearly showed that S. crispus tea developed from microwave-dried leaves able to preserve the polyphenols and hence contribute to excellent antioxidant capacity. Incorporation of unfermented S. crispus tea in the diet can be a good source of natural antioxidant.
... At least two methods should be employed to evaluate the total antioxidant capacity due to different mechanisms of antioxidants, such as free radical scavenging, reducing capacity, decomposition of peroxides, prevention of continued hydrogen abstraction, and binding of transition-metal ion catalysts [24,25]. Therefore, DPPH, FRAP, and ABTS assays were used to determine the antioxidant capacity of the beetroots under various intermittent microwave drying conditions. ...
Article
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The object of this research was the beetroots prepared by intermittent microwave drying at different conditions. The paper aimed to investigate the influence of intermittent microwave drying conditions (power density, microwave gap ratio and slice thickness) on the bioactive compounds and antioxidant capacity of beetroots. A microwave drying system SAM-255 (CEM Corporation, USA) was used to intermittent microwave drying of fresh beetroots. The effect of different power densities (1.0, 1.5, 2.0, and 2.5 W/g), microwave gap ratios (1, 2, 3, and 4) and slice thicknesses (2, 4, 6, and 8 mm) on the bioactive compounds and antioxidant capacity of beetroots were investigated. Colorimetric methods were used to determine contents of betalains, total phenolic and total flavonoid, and antioxidant capacity of dried beetroots. The ascorbic acid content was determined using 2,6-dichloroindophenol titration method. Results showed that power density, microwave gap ratio and slice thickness significantly affected the drying time, bioactive compounds and antioxidant capacity of beetroots. The drying time decreased with the increasing of power density, while increased significantly with the growth of slice thickness and microwave gap ratio. The shortest drying time (35.4±2.6 min) of beetroots was occurred at microwave gap ratio of 2. The content of betacyanins was found to be the highest in the dried beetroots with thickness of 2 mm. The beetroots with slice thickness of 2 and 4 mm showed the highest betacyanins content. Moreover, the highest content of ascorbic acid (240.00±2.32 mg/100 g) and total flavonoid (14.52±0.06 mg rutin equivalent (RE)/g) was appeared at power density of 2.0 W/g, while the content of total phenolic to be highest (12.54±0.13 mg gallic acid equivalent (GAE)/g) at slice thickness of 6 mm. For the antioxidant capacity of dried beetroots, the 1,1-diphenyl-1-picrylhydrazyl (DPPH) radical scavenging activity reached to the highest value of 6.43±0.03 mg trolox equivalent (TE)/g at power density of 2.5 W/g. While the highest values of ferric-reducing antioxidant power (FRAP) (15.47±0.10 mg TE/g) and 2,2′-azino-bis-(3-ethylbenzthiazoline-6-sulfonic acid) (ABTS) radical scavenging activity (25.31±0.30 mg TE/g) at microwave gap ratio of 2. It was found that ABTS radical scavenging ability and FRAP were related to the presence of reductions including betalains, ascorbic acid, and total flavonoid in beetroots. The most effective condition for intermittent microwave drying of beetroots were microwave gap ratio of 2, power density of 2.0 W/g, and slice thickness of 4 mm, leads to a better preservation of bioactive compounds and high antioxidant capacity.
... There are several evaluation methods for antioxidant activity. Antioxidants have different mechanisms, such as reducing capacity, decomposition of peroxides, free radical scavenging, and binding of transition metal ion catalysts [49,50]. Choosing different methods can be expected to obtain different antioxidant activity results, so as to better understand the wide variety and range of action of antioxidant compounds present in beetroots [51]. ...
Article
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The objective of this study was to investigate the effects of different microwave-assisted drying methods on the physical properties, bioactive compounds and antioxidant activity of beetroots. Beetroots were subjected to high-power microwave drying followed by low-power microwave drying (HMD+LMD), high-power microwave drying (HMD), low-power microwave drying (LMD), high-power microwave drying followed by hot air drying (HMD+HAD), hot air drying followed by low-power microwave dry�ing (HAD+LMD), high-power microwave drying followed by vacuum drying (HMD+VD), and vacu�um drying followed by low-power microwave drying (VD+LMD). The drying time, moisture content, hard�ness, color, microstructure, betalains, ascorbic acid, total flavonoids, 2,2′-azino-bis-(3-ethylbenzоthiazo�line-6-sulfonic acid) (ABTS) radical scavenging activ�ity and ferric reducing antioxidant power (FRAP) of beetroots were analyzed. The shortest drying time (67.0 min) was observed in HMD, while VD+LMD required the longest drying time of 308.0 min. There was no significant difference in the moisture content of dried beetroots prepared by different microwave-assisted drying methods. Beetroots dried by HMD+HAD showed the highest hardness of 1332.0 g, VD+LMD led to the most desirable color with the lowest total color change. Porous structures were found in beetroots pro�duced by HMD+LMD, HMD and LMD. Beetroots pre�pared by VD+LMD displayed the highest content of betacyanin, betaxanthin and total flavonoids. While beetroots dried by HMD illustrated the highest ascor�bic acid content of 272.3 mg/100 g dry weight (DW). In terms of antioxidant activity, the highest FRAP value of beetroots obtained using VD+LMD was 14.95 mg trolox equivalent (TE)/g DW. Meanwhile, beetroots dried by VD+LMD exhibited the largest ABTS radical scavenging activity (16.92 mg TE/g DW). Compared to other microwave-assisted drying methods, VD+LMD is a more promising method for drying beetroots
... Polyphenols can react with cell-wall polysaccharides and be oxidised by polyphenol oxidase (Renard, Watrelot, & Bourvellec, 2016). During the drying process, the decline in moisture content altered the three-dimensional structure of the cell-wall, decreasing the affinity constant of polyphenols to the cellwalls and destructing the noncovalent or covalent interactions between polyphenols and cell-wall matrices, resulting in the disruption of plant cell wall polymers (Inchuen, Narkrugsa, & Pornchaloempong, 2010;Le Bourvellec & Renard, 2005;Que, Mao, Fang, & Wu, 2008). Consequently, in certain cases, cell-wall phenolics or bond phenolics could be released, causing more phenolics to be extracted, except that further increasing the temperature might deactivate the enzyme and avoid the loss of phenolic acid caused by oxidisation, with the Maillard reaction products increasing. ...
... Beetroot contains a variety of phytochemicals with high antioxidant activity. At least two methods should be employed to evaluate the total antioxidant capacity due to different mechanisms of antioxidants, such as reducing capacity, decomposition of peroxides, free radical scavenging, and binding of transition-metal ion catalysts (Mao et al., 2006;Inchuen et al., 2010). In this study, the antioxidant activity of dried beetroots was evaluated by three methods: DPPH radical scavenging activity, ferric reducing antioxidant power (FRAP), and ABTS radical scavenging activity. ...
Article
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Introduction. The aim of the research is to investigate the influence of different drying methods, including freeze drying, vacuum drying, microwave drying and microwave vacuum drying, on the bioactive compounds and antioxidant activity of beetroots. Materials and methods. Bioactive compounds and antioxidant activity of dried beetroots prepared by freeze drying (FD), vacuum drying (VD), microwave drying (MD), and microwave vacuum drying (MVD) were investigated. Moisture analyzer was used to determine moisture content of beetroots. Beetroot powder was extracted three times with 50% ethanol (v/v). Colorimetric methods were used to determinate contents of betalain, ascorbic acid and total phenolic, and 1,1-diphenyl-1-picrylhydrazyl (DPPH) radical scavenging activity, ferric reducing antioxidant power (FRAP) and 2,2′-azino-bis-(3- ethylbenzthiazoline-6-sulfonic acid) (ABTS) radical scavenging activity of dried beetroots. Results and discussion. Drying methods significantly affected the drying time, bioactive compounds and antioxidant activity of beetroots. The shortest drying time (0.56±0.01 h) was occurred at MVD, while FD required the longest drying time of 29.67±0.58 h. There was no significant difference in the final moisture content of dried beetroots prepared by different drying methods. It was found that the dried beetroots prepared by VD showed the highest ascorbic acid content of 8.73±0.23 mg/g, and the beetroots dried by FD displayed the highest betaxanthin content of 2.57±0.01 mg/g, while the beetroots obtained by MD showed the lowest betacyanin content of 2.98±0.02 mg/g, and FD led to significantly lower total phenolic content of beetroots in comparison with other drying methods. In terms of antioxidant activity, the beetroots prepared by MD and MVD showed significantly higher DPPH radical scavenging activity than the beetroots prepared by VD and FD. Meanwhile, the beetroots obtained by VD exhibited the largestABTS radical scavenging activity of 17.22±0.35 mg trolox equivalent (TE)/g. Besides, the beetroots prepared by MVD displayed the highest FRAP value of 13.36±0.17 mg TE/g. Compared to beetroots prepared by other drying methods, the beetroots prepared by FD showed the lowest FRAP, DPPH and ABTS values, indicating the weakest antioxidant activity. Conclusions. Considering the drying time, bioactive compounds and antioxidant activity, MVD is recommended to prepare dehydrated beetroots, which can reduce drying time and better preserve bioactive compounds and antioxidant activity of beetroots.
... It is important to remind that the power used on microwave varies depending on the plant species used for drying, and may present variation on the phenolic content (Hihat et al., 2017;Khodja et al., 2020). Nonetheless, this high phenolic content may be related to the intense heat generated from this drying mechanism, creating intense vapour pressure and temperature in localized parts of the plant tissue, which could disrupts the plant cell wall leading to more phenolics being extracted (Inchuen et al., 2010). ...
Article
This work investigates the consumer's acceptance of hot and iced mate tea, bioactive compounds content and antioxidant capacity of toasted yerba mate leaves dried from various processes, aiming at presenting drying alternatives to the traditional, and mostly used, methods. Therefore, five drying methods were tested, traditional rotary dryer, conveyor dryer and three alternatives including microwave oven, over dryer at 40, 60, 80 °C and freeze-drying, which was followed by toasting. Overall, the microwave oven and freeze dryer were highly efficient and can be considered as drying alternatives with high values of total phenolic compounds (78.72 mg GAE.g-1), antioxidant capacity by DPPH/ABTS (376.6 TEAC µmol.g-1 /1062.04 TEAC µmol.g-1), caffeine (13.25 mg.g-1) and caffeoylquinic acids (69 mg.g-1). Using a reworked python script, the preference map of teas dried in microwave oven and freeze-drying resulted in similar sensory acceptance for hot tea, produced using traditional drying methods, with a slight decrease for the iced tea. Novelty Impact statement The tea industry can adopt microwave and freeze drying as alternative methods for drying mate leaves, this is followed by toast in order to obtain the commercial tea. These methodologies present smaller equipment sizes and removes the dangerous traditional process known as "zapeco". The microwave and freeze drying have a small decrease in sensory acceptance compared to traditional methods used in agri-food industry but with high content of total phenolic compounds, caffeoylquinic acids and high antioxidant activities; also, in the case of microwaves, this method has the advantage of reducing the drying time.
... The use of powers greater than 600W induces a reduction of phenolic compound content and antioxidant activity. According to Inchuen et al. [43], the intensity of heat generated by microwaves creates high pressures and temperatures inside the sample. The heat was generated inside particles and cells of the plant; then, a considerable pressure was formed that directed outside, causing the destroying of cell walls and thus releasing phenolic compounds to extraction solvent, which will increase yield. ...
Article
Background The laurel is a shrub native to the Mediterranean basin. It is too often wrongly relegated to the kitchen as a simple condiment while it possesses many therapeutic properties and virtues. The valorization of this plant in terms of bioactive compounds seems to be important. Objective The aim of the present study is to optimize total phenolic content (TPC) extraction and antioxidant activity from dried bay leaves using conventional process and response surface methodology (RSM). Method The study of optimization was firstly tested three extraction methods (maceration, ultrasonic-assisted extraction (UAE), and Microwave-assisted extraction (MAE)) then the best one was considered for RSM. Results The results for the sequential procedure indicated that MAE was the best method for TPC extraction and antioxidant activity of Laurus nobilis leaves. The mathematical modeling of MEA using response surface methodology showed that optimal conditions for phenolic compounds extraction were 57% methanol with microwaves power of 602W during 3.48 minutes. These conditions allowed TPC extraction of 83.53 mg/g and manifested an antioxidant activity of 32.51 mg EAG/g. Conclusion The validation of models indicated that experimental values were in accordance with predicted ones, demonstrating the suitability of developed models and the success of RSM in the optimization of antioxidants extraction from Laurus nobilis leaves. Therefore, the bay leaves could be considered as an interesting source of phenolic antioxidants.
... Indeed, Ince et al. (2013) demonstrated that microwave extraction of phenolic compounds is more efficient compared to maceration. According to Inchuen et al. (2010), the intense heat generated by microwaves creates high pressures and temperatures inside the sample. When plant cells are heated, high pressure is generated causing the destroying of cell walls. ...
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Laurus nobilis one of medicinal and aromatic plant endemic to the Mediter-ranean region. It is highly appreciated for the condiment benefits of its leaves. Due to its richness in bioactive compounds, the leaves are also used in traditional therapy to treat several infectious diseases. Phenolic com-pounds and alkaloids are particularly important because they are used in many pharmaceutical, food supplement, and cosmetic fields. The presence of phenolic compounds and alkaloids in L. nobilis leaves attracted our atten-tion due to their various functions such as antioxidant capacity and antibac-terial properties. The main objective of this study was to determine antioxi-dant and antibacterial activities of phenolic and alkaloid extracts of L. nobilis. The quantification of antioxidant substances allowed obtaining phenolic compounds content of 86.46 EAG mg/g and a total alkaloids yield of 700 μg/g. The results of antioxidant activity show that, although the alkaloid concen-trations are low, their antioxidant power is higher than phenolic compounds. The results of antibacterial activity of L. nobilis extracts revealed that the highest inhibition was recorded for alkaloid extract against staphylococcal strains responsible for food poisoning. However, L. nobilis phenolic com-pounds showed better activity against phytopathogenic strains associated particularly with potato rot.
... whereas the L � values were slightly different among samples. This finding was in accordance with Inchuen et al. [66] for microwave-dried red curry, Pereira et al. [67] for combined microwave/hot-air-dried banana, Soysal [68] for microwave-dried parsley, and Maskan [69] for microwave-dried banana. Browning effects are mainly contributed to the quality deterioration of dried food products caused by thermally induced browning reactions [70]. ...
Article
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The objective of this research was to comparatively investigate the effect of hot air drying (HA) and hybrid microwave-infrared drying (MI) on physico-chemical characteristics of Thai fermented fish viscera, Tai-Pla , curry powder (TCP). HA was carried out at 60°C, 70°C, and 80°C and MI was carried out at a microwave power of 740, 780, and 810 W with a constant infrared heating power (500 W) for different drying times to obtain the final moisture content ≤ 12.0% and the water activity (a w ) ≤ 0.6. The quality characteristics of TCP were governed by HA temperature and MI output power. TCP dried using HA and MI at all conditions had similar contents of protein, lipid, ash, fiber, and carbohydrate (p>0.05). The fastest drying rate was detected when MI at 810 W for 40 min was applied (p < 0.05). In this condition, TCP had the lowest browning index (A 294 and A 420 ) and the highest lightness ( L* value) (p < 0.05). TCP dried with MI at all powers had higher phenolic content and lower TBARS compared to HA (p < 0.05). However, no significant differences in DPPH • scavenging activity were observed among TPC made by HA and MI (p>0.05). Similar Fourier transform infrared (FTIR) spectra with different peak intensities were observed in all samples, indicating the same functional groups with different contents were found. The bulk density of all TCP ranged from 0.51 g/mL to 0.61 g/mL and the wettability ranged from 24.02% to 26.70%. MI at 810 W for 40 min effectively reduced the drying time (5-fold faster) and lowered the specific energy consumption (18-fold lower) compared to the HA at 60°C for 210 min. Therefore, MI is a promising drying technique to reduce the drying time and improve the overall quality of TCP.
... Indeed, Ince et al. (2013) demonstrated that microwave extraction of phenolic compounds is more efficient compared to maceration. According to Inchuen et al. (2010), the intense heat generated by microwaves creates high pressures and temperatures inside the sample. When plant cells are heated, high pressure is generated causing the destroying of cell walls. ...
Article
Full-text available
Laurus nobilis is one of medicinal and aromatic plant endemic to the Mediter-ranean region. It is highly appreciated for the condiment benefits of its leaves. Due to its richness in bioactive compounds, the leaves are also used in traditional therapy to treat several infectious diseases. Phenolic compounds and alkaloids are particularly important because they are used in many pharmaceutical, food supplement, and cosmetic fields. The presence of phenolic compounds and alkaloids in L. nobilis leaves attracted our attention due to their various functions such as antioxidant capacity and antibac-terial properties. The main objective of this study was to determine antioxi-dant and antibacterial activities of phenolic and alkaloid extracts of L. nobilis. The quantification of antioxidant substances allowed obtaining phenolic compounds content of 86.46 EAG mg/g and a total alkaloids yield of 700 µg/ g. The results of antioxidant activity show that, although the alkaloid concentrations are low, their antioxidant power is higher than phenolic compounds. The results of antibacterial activity of L. nobilis extracts revealed that the highest inhibition was recorded for alkaloid extract against staphylococcal strains responsible for food poisoning. However, L. nobilis phenolic compounds showed better activity against phytopathogenic strains associated particularly with potato rot.
... But were higher than S. aegyptiaca (Ben Farhat et al., 2013) The in vitro antioxidant ability of natural substances can be assessed by several analytical methods. Due to the high diversity in the phytochemicals composition and oxidative processes, this lead to evaluate the AA of plant extracts using a variety of methods (Inchuen, Narkrugsa, & Pornchaloempong, 2010). Different mechanisms can be involved in the AA, such as free radical scavenging, peroxide decomposition, chain initiation prevention, hydrogen abstraction, binding of transition metal ion catalysts, and reducing capacity (Mao, Pan, Que, & Fang, 2006). ...
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In this study, Salvia aegyptiaca and Salvia verbenaca aerial part decoction and methanol extracts (SAE DE, SAE ME, SVR DE, and SVR ME) were screened for their in vitro antioxidant, anti-Alzheimer, and antidiabetic enzymes inhibition activities. The antioxidant properties of Salvia extracts were determined using DPPH radical scavenging, ABTS radical scavenging, Alkaline DMSO superoxide radical scavenging, β-carotene bleaching, reducing power, and metal chelating activity assays. All extracts showed high antioxidant capacity and the antioxidant properties with the best performance were detected in the SAE ME and SVR ME. The extracts of S. aegyptiaca and S. verbenaca showed a low inhibitory activity of acetylcholinesterase (AChE), whereas, the methanol extract of S. aegyptiaca had the highest inhibitory activity on butyrylcholinesterase (BChE) (71.60 ± 4.33% for 100 µg/ml) compared to the other extracts. In vitro inhibitory effect on diabetic enzymes showed that the ME inhibited α-amylase enzyme with an IC50 86 and 101 µg/ml for SAE and SVR, respectively. Similarly, both extracts inhibited α-glucosidase with (IC50 97 and 150 µg/ ml, respectively). The decoction extracts exhibited lower activity on both enzymes
... The attributes of three color parameters (L*, a*, b*) were found by Sudathip et al. [31] , who reported the values of (L*, a*, b*) of Thai red curry powder when using hot-air drying were higher than microwave drying. ...
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Four different fresh and dried herb species (sage, thyme, mint and lemonbalm) were evaluated to study the effect of drying process on the total phenolics, antioxidant activity, flavonoid contents and color properties. Fresh mint had the highest contents of total phenolics (335.4 mg GAE/100 g), whereas lower levels were respectively found in sage (316.4 mg GAE/100 g) followed by lemonbalm (303.2 mg GAE/100 g) and thyme (299.2 mg GAE/100 g). Dry processing significantly decreased the phytochemical contents of all investigated herbs. Compare to air drying, total phenolics, antioxidant activity and flavonoids content in herbs decreased apparently by oven dried. Fresh mint had the highest antioxidant activity (87.46%) and flavonoids content (298.51 mg CE/100 g), while the fresh sage, thyme and lemonbalm were found to have antioxidant activity values of 86.81%, 86.56% and 85.26%, respectively. Results showed that air drying herbs contained more total phenolics, antioxidant activity, and flavonoids than oven drying herbs. Citation: Rababah T M, Al-u'datt M, Alhamad M, Al-Mahasneh M, Ereifej K, Andrade J, et al. The Effect of drying process on total phenolics, antioxidant activity, and flavonoid contents of common Mediterranean herbs. Int J Agric & Biol Eng, 2015; 8(2): 145-150.
... The attributes of three color parameters (L*, a*, b*) were found by Sudathip et al. [31] , who reported the values of (L*, a*, b*) of Thai red curry powder when using hot-air drying were higher than microwave drying. ...
Article
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Four different fresh and dried herb species (sage, thyme, mint and lemonbalm) were evaluated to study the effect of drying process on the total phenolics, antioxidant activity, flavonoid contents and color properties. Fresh mint had the highest contents of total phenolics (335.4 mg GAE/100 g), whereas lower levels were respectively found in sage (316.4 mg GAE/100 g) followed by lemonbalm (303.2 mg GAE/100 g) and thyme (299.2 mg GAE/100 g). Dry processing significantly decreased the phytochemical contents of all investigated herbs. Compare to air drying, total phenolics, antioxidant activity and flavonoids content in herbs decreased apparently by oven dried. Fresh mint had the highest antioxidant activity (87.46%) and flavonoids content (298.51 mg CE/100 g), while the fresh sage, thyme and lemonbalm were found to have antioxidant activity values of 86.81%, 86.56% and 85.26%, respectively. Results showed that air drying herbs contained more total phenolics, antioxidant activity, and flavonoids than oven drying herbs. Citation: Rababah T M, Al-u'datt M, Alhamad M, Al-Mahasneh M, Ereifej K, Andrade J, et al. The Effect of drying process on total phenolics, antioxidant activity, and flavonoid contents of common Mediterranean herbs. Int J Agric & Biol Eng, 2015; 8(2): 145-150.
... Hamrouni-Sellami et al. (2013), reportaron resultados similares en extractos metanólicos de plantas de salvia (Salvia officinalis L.) evaluadas en peso seco, donde, la presión de vapor y la alta temperatura a las cuales se sometió al material vegetal, ocasionó la interrupción de los polímeros de la pared celular. Adicionalmente, Inchuen et al. (2010), reportaron que a consecuencia de esto se podrían liberar polifenoles presentes en la pared celular, lo que provocaría un aumento de estos compuestos en los extractos de plantas sometidas a secado. Sin embargo, un proceso de desecación prolongado y excesivo puede desnaturalizar algunas enzimas y compuestos bioactivos (Cabrera et al., 2012). ...
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... Indeed,Sathishkumar, Lakshmi, and Annamalai (2009) reported a sharp decrease in the TPC of Enicostemma littorale as processed by microwave drying.Inchuen et al. (2010) have reported that increasing MP from 180 to 540 W resulted in an increase of the TPC of Thai red curry powder. KammounBejar et al. (2011) found that the drying method deeply affected qualitative phenolic composition by increasing contents of some compounds but decreasing those of others, as well as by the appearance of some other pheno ...
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The effects of microwave power (MP, 100–600 W) on the drying kinetics, as well as the physical and antioxidant properties of papaya seeds dried under microwave vacuum drying (MVD) were investigated. The results found that moisture diffusivity increased in the order of 10⁻⁸ with an increase in MP. Shrinkage increased from 1.2 to 4.9% and bulk density decreased from 3,441 to 1,091 kg/m³, respectively, while the moisture content decreased. The antioxidant contents of all of the MVD samples were higher than those of the samples dried under ambient air ventilation. An increase in MP decreased the total phenolic content from 14.69 to 10.66 mg gallic acid equivalent per gram dry weight (DW), increased both the β‐carotene and the total flavonoid content in the ranges of 0.2–0.35 mg β‐carotene equivalent per gram DW and 20.71 to 23.51 mg catechin equivalent per gram DW, respectively. Higher values of antioxidant activity were obtained at higher MP. The results have shown that the use of novel MVD technique in appropriate conditions can improve the overall drying efficiency and enhance the total yield of antioxidant content. Practical Applications Papaya seeds have great potential for use as a source of antioxidants. However, the best novel techniques for retaining high values of antioxidant compounds, and therefore recouping value from the wasted seeds, has not been widely reported on. This study has found that combined microwave vacuum drying (MVD) is a very beneficial drying method for the preservation of antioxidant content. A better antioxidant yield from dried papaya seeds was obtained using MVD at a higher MP of 600 W. Trolox equivalent antioxidant capacity of seeds dried using MVD was 27.62% higher than the samples dried using ambient air ventilation.
... TPC in the mixture was evaluated by using the Folin-Ciocalteau method [9]. 0.5 mL of diluted extract was mixed with 9.5 mL of distilled water and 0.5 mL of Folin-Ciocalteau reagent. ...
... The high temperature, 70 • C, did not negatively affect the antioxidant activity of pepper during oven drying. Similar results have been reported by various researchers such as Madrau (2009) who reported a significant increase in antioxidant activity of apricots from Cafona variety after air drying at 75 • C, Inchuen et al. (2010) who reported an improved antioxidant activity of the red curry powder and Oboh and Akindahunsi (2004) who reported that sun-drying cause significant increases in the antioxidant properties of the green leafy vegetables. In fact, less air circulation compared to sun drying and longer drying time required than drying at 70 • C, the oven drying at 50 • C did not reveal the desired result. ...
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The effect of thermal and non-thermal drying methods on hydrophilic and lipophilic antioxidant capacities of bitter gourd fruit was investigated in this study. The bitter gourd fruits were dried by following methods: (i) oven drying 40 degrees C, (ii) oven drying 50 degrees C, (iii) oven drying 60 degrees C, (iv) microwave drying (medium low power), (v) microwave drying (medium power) and (vi) freeze drying. Pure acetone and hexane were used to extract the hydrophilic and lipophilic antioxidant compounds from dried bitter gourd fruits. Freeze dried extracts reported to have highest values in DPPH scavenging activity (hydrophilic and lipophilic fractions), FRAP (lipophilic fraction) and TPC (hydrophilic and lipophilic fraction). Thermal drying slightly increased the values of DPPH scavenging activity, FRAP and TPC assays for hydrophilic extracts. Results concluded bitter gourd fruit is a good source of natural antioxidants and its total antioxidant quality was most preserved by freeze drying. Additionally, the higher value reported in DPPH scavenging activity, FRAP and TPC assays for lipophilic extracts than the hydrophilic extracts suggested that the lipophilic antioxidant compounds of bitter gourd fruit might possess stronger antioxidant power than its counterpart.
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The antioxidant activities and total phenolics of 28 plant products, including sunflower seeds, flaxseeds, wheat germ, buckwheat, and several fruits, vegetables, and medicinal plants were determined. The total phenolic content, determined according to the Folin−Ciocalteu method, varied from 169 to 10548 mg/100 g of dry product. Antioxidant activity of methanolic extract evaluated according to the β-carotene bleaching method expressed as AOX (Δ log A470/min), AA (percent inhibition relative to control), ORR (oxidation rate ratio), and AAC (antioxidant activity coefficient) ranged from 0.05, 53.7, 0.009, and 51.7 to 0.26, 99.1, 0.46, and 969.3, respectively. The correlation coefficient between total phenolics and antioxidative activities was statistically significant. Keywords: Antioxidant activity; phenolics; medicinal plants; oilseeds; buckwheat; vegetables; fruits; wheat products
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The effect of heat treatment on the antioxidant activity of extracts from Citrus unshiu peels was evaluated. Citrus peels (CP) (5 g) were placed in Pyrex Petri dishes (8.0 cm diameter) and heat-treated at 50, 100, or 150 degrees C for 10, 20, 30, 40, 50, and 60 min in an electric muffle furnace. After heat treatment, 70% ethanol extract (EE) and water extract (WE) (0.1 g/10 mL) of CP were prepared, and total phenol contents (TPC), radical scavenging activity (RSA), and reducing power of the extracts were determined. The antioxidant activities of CP extracts increased as heating temperature increased. For example, heat treatment of CP at 150 degrees C for 60 min increased the TPC, RSA, and reducing power of EE from 71.8 to 171.0 microM, from 29.64 to 64.25%, and from 0.45 to 0.82, respectively, compared to non-heat-treated control. In the case of WE from CP heat-treated at the same conditions (150 degrees C for 60 min), the TPC, RSA, and reducing power also increased from 84.4 to 204.9 microM, from 15.81 to 58.26%, and from 0.27 to 0.96, respectively. Several low molecular weight phenolic compounds such as 2,3-diacetyl-1-phenylnaphthalene, ferulic acid, p-hydroxybenzaldoxime, 5-hydroxyvaleric acid, 2,3-diacetyl-1-phenylnaphthalene, and vanillic acid were newly formed in the CP heated at 150 degrees C for 30 min. These results indicated that the antioxidant activity of CP extracts was significantly affected by heating temperature and duration of treatment on CP and that the heating process can be used as a tool for increasing the antioxidant activity of CP.
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Phenolic compounds in foods originate from one of the main classes of secondary metabolites in plants. They are essential for the growth and reproduction of plants, and are produced as a response for defending injured plants against pathogens. In recent years, there is a growing interest in phenolic compounds and their presumed role in the prevention of various degenerative diseases, such as cancer and cardiovascular diseases. The importance of antioxidant activities of phenolic compounds and their possible usage in processed foods as a natural antioxidant have reached a new high in recent years. The absorption and bioavailability of phenolics in humans are also controversial. Data on these aspects of phenolics are scarce and merely highlight the need for extensive investigations of the handling of phenolics by the gastrointestinal tract and their subsequent absorption and metabolism. In this article, absorption, metabolism, and the bioavailability of pheniolic compounds are reviewed.
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Parsley (Petroslinum crispum Mill.) leaves were dried in a domestic microwave oven to determine the effects of microwave output power on drying time, drying rate and the dried product quality in terms of colour. Seven different microwave output powers ranging from 360 to 900 W were used in the drying experiments. Drying took place mainly in constant rate and falling rate periods. After a short heating period a relatively long constant rate period was observed. Approximately 40·5% of the water was removed in this period. The rapidly decreasing falling rate period followed the constant rate period. As the drying progressed, the loss of moisture in the product caused a decrease in the absorption of microwave power and resulted in a fall in the drying rate. Increasing the microwave output power resulted in a considerable decrease in drying time (probability P<0·01). The semi-empirical Page's equation used to describe the drying kinetics of dried leaf materials gave an excellent fit for all data points with values for the coefficient of determination R2 of greater than 0·997 and for the standard error of estimates (SEE) of lower than 0·0188. The value of the drying constant increased with increased microwave output power. No significant differences were observed between the colour parameters of fresh and microwave-dried leaf materials, except for some decrease in whiteness L value (P>0·05). The change in colour values was not dependent on the microwave output power. Although some darkening occurred, microwave drying maintained a good green colour close to that of the original fresh parsley leaves. By working at 900 W instead of 360 W, the drying time could be reduced by 64% with a good quality product.
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The effects of independent variables (ethanol:water ratio, temperature and time) on the extraction yield and antioxidant properties of phenolic extracts from lemon grass, galangal, holy basil and rosemary were studied. The extraction solvent ratio of ethanol to water was found to have a significant (P < 0.05) influence on extraction yield, reducing power and total phenolic content, but not on the antioxidant activity of all herb and spice samples, while extraction temperature had only minor effects. Extraction time had a significant (P < 0.05) effect only on the reducing power of holy basil extracts. The optimum extraction conditions, i.e. extraction solvent ratio of ethanol to water, extraction temperature and extraction time for maximum total phenolic content, were 3:1 at 25 °C for 30 min for lemon grass, 3:1 at 75 °C for 90 min for galangal and holy basil and 3:1 at 75 °C for 30 min for rosemary.
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The total phenolic content (TPC) and antioxidant activity of fresh and dried Phyllanthus amarus plant materials were evaluated using the Folin-Ciocalteau method, 2,2-diphenyl-1-picrylhydrazyl (DPPH) free radical scavenging activity and ferric reducing antioxidant power (FRAP) assays. Different drying treatments led to significant reduction (P<0.05) in antioxidant properties of P. amarus methanolic extracts, with microwave drying causing the highest decrease in TPC and antioxidant activity exhibited by the reduction in both radical scavenging activity and FRAP. On the other hand, boiling water extracts appeared to exhibit significantly stronger antioxidant potentials (P<0.05) even in dried plant materials due to greater solubility of compounds, breakdown of cellular constituents as well as hydrolysis of tannins. Its strong free radical scavenging activity suggests that it has great potential in the food industry as functional food ingredient.
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Pectin-sugar gels were dehydrated with four different drying methods: freeze, microwave, vacuum and conventional drying to a moisture content of about 5%. The effect of the drying method on the water sorption properties of dehydrated products was evaluated at 25 °C. Freeze-dried gel adsorbed more water vapour than microwave-dried gel, which had a higher sorption capacity than vacuum- and conventional-dried product. The sorption isotherms were in agreement with the reported shape for high sugar foodstuffs. Three different equations proposed in the literature (GAB, Oswin, Hasley) were used to fit the sorption data. The GAB equation gave the best fit to the experimental data. The porosity of the dehydrated products depended on the drying method, ranging between 0.2 and 0.5. Freeze- and vacuum-dried pectin developed the highest porosity, whereas the lowest porosity was obtained using conventional and microwave drying. Hunter colour parameters (L, a, b) also depended on the drying method. The colour of freeze- and vacuum-dried pectin was close to that of commercial pectin, while the colour of the conventional- and microwave-dried product changed significantly.
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Nutritional factors are widely considered to be critical for human health. Overwhelming evidence from epidemiological studies indicate that diets rich in fruit and vegetables are associated with a lower risk of several degenerative diseases. These results have created a new perspective concerning the potential of diet in preventing serious diseases in the future. However, the health-promoting capacity of fruit and vegetables strictly depends on their processing history. This aspect has been generally neglected or scarcely considered in present nutritional and epidemiological studies. Processing is expected to affect content, activity and bioavailability of bioactive compounds.The aim of this article, therefore, is to review the effects of processing on the antioxidant properties of foods by means of a multidisciplinary approach. It is believed that the implications of this challenging and rapidly advancing area may contribute to enhanced industrial competitiveness as well as consumer health and well-being.
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Carrot slices were dried by using microwave, halogen lamp–microwave combination and hot-air drying. Microwave and halogen lamp–microwave combination drying were applied after carrots were dried to 0.47 kg moisture/kg dry solid by hot-air drying. Drying time, rehydration capacity and colour of the carrots dried by different methods were compared. The increase in microwave oven power level decreased the drying time. Microwave drying at the highest power and halogen lamp–microwave combination drying reduced the drying time to an extend of 98% in comparison to conventional hot-air drying and a high-quality dried product was obtained. Moreover, in the case of halogen lamp–microwave combination drying, moisture level was reduced to a level, which is lower than the one achieved by other methods. Less colour change occurred when microwave and halogen lamp–microwave combination drying were applied. Carrots dried in microwave and halogen lamp–microwave combination oven had lower L*, higher a* and b* values and had higher rehydration capacity as compared to hot-air drying.
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Garlic cloves were dried with hot air and combined microwave–hot air drying methods in an experimental dryer. The combined microwave–hot air drying experiments were carried out with 100 g sample sizes at temperatures of 40°C, 50°C, 60°C and 70°C at air velocities of 1.0 and 2.0 m/s, using continuous microwave power of 40 W. For comparison of hot air drying, the same sample sizes were taken for experiments and the drying air temperatures and air velocity were 60°C and 70°C, and 2.0 m/s respectively. The total drying time, the color and flavor strength of dried garlic cloves were used to evaluate the performance of the combined microwave–hot air drying and the conventional hot air drying processes. Combined microwave–hot air drying resulted in a reduction in the drying time to an extent of 80–90% in comparison to conventional hot air drying and a superior quality final product.
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The thermal modelling of foods in a microwave field was investigated. The purpose of this work was to simplify the complex thermal modelling necessary for the drying calculations. The calorimetric technique was used to model the power absorbed with respect to sample size and oven loading. A linear relationship between power absorbed and sample diameter was obtained, while a non-linear behaviour was observed between the power absorbed by samples of various diameters and oven loading.
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This paper reports on a study of the final stage of microwave-hot air drying of osmotically dehydrated bananas, focusing on the effects of microwave power, air temperature and air velocity on drying kinetics and product quality, evaluated in terms of colour, apparent volume and porosity. The drying process was divided into three periods: phase I (760 W; 2 kgmoisture/kgdry matter); phase II (380 W; 0.67 kgmoisture/kgdry matter); and phase III (0 W, 76 W, 150 W or 230 W up to the final sample moisture of 0.17 kgwater/kgd m). Three conditions for the hot air were tested: 50 °C and 3.3 m/s; 70 °C and 3.3 m/s; 70 °C and 5.7 m/s. The results show that increasing the microwave power in phase III increased the drying rate, thus making the drying time shorter. However, higher microwave power also caused temperature runaway leading to charring on the dried product. Air flow cools the product surface and improves product quality by reducing charring.
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Microwave (MW)-related (MW-assisted or MW-enhanced) combination drying is a rapid dehydration technique that can be applied to specific foods, particularly to fruits and vegetables. Increasing concerns over product quality and production costs have motivated the researchers to investigate and the industry to adopt combination drying technologies. The advantages of MW-related combination drying include the following: shorter drying time, improved product quality, and flexibility in producing a wide variety of dried products. But current applications are limited to small categories of fruits and vegetables due to high start-up costs and relatively complicated technology as compared to conventional convection drying. MW-related combination drying takes advantages of conventional drying methods and microwave heating, leading to better processes than MW drying alone. This paper presents a comprehensive review of recent progresses in MW-related combined drying research and recommendations for future research to bridge the gap between laboratory research and industrial applications.
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Yams (the tubers of the Dioscorea spp.), consumed and regarded as medicinal food in traditional Chinese herbal medicine, are seasonal foods and easily deteriorate during storage. It is of great importance to prolong the storage of yams for supplying in the off-season and without losing nutritional functionality. Three varieties of yams, Dioscorea alata (cultivars of Tai-Nung no. 2 and Ta-Shan) and D. purpurea (cultivar of Ming-Chien), were made into flours by freeze-drying, hot air-drying, and drum-drying in this report. The proximate compositions and physical properties, as well as antioxidant activities, of yam flours were determined. While drying methods showed significant effects on the moisture contents of yam flours, they had no marked effects on other components of yam flours. Colour attributes and physical properties were all affected by drying methods to different extents. While freeze-drying usually preserved more antioxidant activity of the yam flours, yam flours made of different yam varieties showed different antioxidant mechanisms.
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The antioxidant activities of peanut (Arachis hypogaea L.) hull extracts were evaluated after far-infrared (FIR) radiation or heat treatment. Peanut hulls in petri dishes were FIR-irradiated or heat-treated (150 °C) for 5, 10, 15, 20, 40 or 60 min. The water extracts (300 mg/10 mL) of peanut hulls (WEPH) were prepared and their total phenol contents (TPC), radical scavenging activity (RSA), and reducing power were determined. The antioxidant activities of WEPH increased as the time of heating or FIR-radiation increased. When peanut hulls were FIR-irradiated at 150 °C for 60 min, the values of TPC, RSA, and reducing power of WEPH increased from 72.9 to 141.6 μM, 2.34% to 48.83%, and 0.473 to 0.910, respectively, compared to the untreated controls. Heat treatment of peanut hull under the same conditions (150 °C for 60 min) also increased the TPC, RSA, and reducing power of WEPH from 72.9 to 90.3 μM, 1.90% to 23.69%, and from 0.471 to 0.718, respectively. The result indicated that FIR-radiation or heat treatment on peanut hulls increased the antioxidant activities of WEPH.
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The antioxidant properties of 25 edible tropical plants, expressed as Trolox equivalent antioxidant capacity (TEAC), were studied using DPPH (1,1-diphenyl-2-picrylhydrazyl free radical) scavenging and reducing ferric ion antioxidant potential (FRAP) assays. Their cupric ion chelating activities (CCA) and total polyphenol contents (TPC) were also determined. A strong correlation between TEAC values obtained for the DPPH assay (TEACDPPH) and those for the FRAP assay (TEACFRAP) implied that compounds in the extracts were capable of scavenging the DPPH free radical and reducing ferric ions. A satisfactory correlation of TPC with TEACDPPH and TEACFRAP suggested that polyphenols in the extracts were partly responsible for the antioxidant activities while its correlation with CCA was poor, indicating that polyphenols might not be the main cupric ion chelators. Principal component analysis (PCA) indicated that TEACDPPH, TEACFRAP and TPC contributed to the total variation in the antioxidant activities of the plants.
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The effect of microwave pretreatment of fruit raw material on some physical properties of the orange tissue was investigated. Scanning electron micrographs showed that microwave heating led to destruction of the parenchymal cells. It was also found that specific surface and the water absorption capacity of the orange tissue, and the endogenous enzymes of the peels were inactivated. As a result of this pectin extraction was facilitated. Considerable increasing in pectin yield and was attained (190% from oranges from crop of 1996 and over 250% for oranges of crop 1997 as compared with control). The quality of the pectin was also improved.
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Food dehydration is still one of the most relevant and challenging unit operations in food processing, although the art of food preservation through the partial removal of water content dates back several centuries. This article provides essential information on the fundamental, including psychrometry, and applied engineering aspects of food dehydration with up-to-date available commercial applications. The evolution of drying technology, divided into four generations, is thoroughly reviewed, from tray drying to the combination of some drying technologies (the hurdle technology approach in drying) in order to optimize the process in terms of final food quality and energy consumption. The study of each generation covered numerous examples of different dryers, including their principles of operation, basic configurations and most common applications, as well as their main advantages and disadvantages.
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Dehydration promoted important modifications affecting both the physico-chemical properties of dietary fibre (DF) and the antioxidant capacity of orange by-products (peel and pulp remaining after juice extraction). The significance of such changes was largely dependent on the air-drying temperature used (from 30 °C to 90 °C). The major modifications on the DF components were observed when either extended drying periods, i.e. at lower temperatures, or elevated drying temperatures were applied. Dehydration around 50–60 °C apparently promoted the minor disruption of cell wall polymers, in particular of pectic substances. Pulp samples exhibited higher values of swelling (SW) and fat adsorption capacity (FAC) than those derived from orange peel. Although, significant decreases in water retention capacity (WRC), FAC and solubility values were detected for both by-products as the air-drying temperature increased. The antioxidant capacity associated to dehydrated citrus by-products was significantly higher for orange peel than for pulp samples. In general, the by-products studied proved to be quite resistant to the different heat treatments applied within the range of 40–70 °C. In overall, the study shows that, in order to preserve either the DF quality and/or the antioxidant capacity, air-drying temperature should be controlled since both types of compounds, DF components and antioxidants, might be degraded or modified either when extended drying periods and/or high drying temperatures are applied.
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The kinetics of degradation of color was evaluated using a fraction conversion model during thermal treatment of red chilli puree at 60, 70, 80 and 90°C (up to 20 min) and storage of red chilli paste at 5, 25 and 37°C (up to 6 mo). Red chilli puree was subjected to heat treatment at different temperatures in a well-stirred water bath. Test samples were removed from the bath at selected time intervals (0–20 min after come-up), cooled immediately and analysed for color using a Hunterlab colorimeter. Chilli paste was prepared by a standard formulation by adding common salt (8%) and the required volume of citric acid to bring the pH to 4.0. The paste was thermally processed at 85°C for 15 min, filled into glass bottles and stored at selected temperatures for 6 mo. Red chilli color was expressed as a tristimulus combination value (L·a·b) as well as the total color difference (ΔE). The fraction conversion model adequately described the kinetic changes in both color values during thermal treatment of puree and storage of puree. The process activation energies were 24.2 and 24.8 kJ/mol, respectively, for ΔE and L·a·b during the thermal treatment, and during the storage the respective values were 24.1 and 25.0 18;kJ/mol. Up to the end of the 6-mo storage, the paste was microbiologically stable with no major changes in other physico-chemical characteristics.
Article
Thai red curry paste was dried with two different drying methods: microwave and hot-air drying. The microwave drying was carried out in a microwave oven with output power of 180, 360 and 540 W, while the hot-air drying was carried out at drying air temperatures of 60, 70 and 80 C. The drying time of microwave drying process to reduce the moisture content of red curry paste from 2.58 to 0.08 g water/g dry matter was much shorter than that of the hot-air drying process. An increase in the microwave power significantly decreased the drying time. In the hot-air drying, increasing the drying air temperature also significantly decreased the drying time. Microwave drying process of red curry paste consisted of three drying periods, i.e. heating up, constant rate and falling rate periods, while hot-air drying process consisted of two drying periods, i.e. heating up and falling rate periods. To describe the effect of microwave power and drying air temperature on drying kinetics of red curry paste, three different mathematical thin-layer equations, i.e. Lewis, Page and Henderson-Pabis models, were used to fit the drying data. The fitness by these models was evaluated using the coefficient of determination (R2), the reduced chi-square (2) and the root mean square error (RMSE). The Page model provided the best fit to both microwave and hot-air drying experimental data.
Article
The antioxidant capacities (oxygen radical absorbance capacity, ORAC) and total phenolic contents in extracts of 27 culinary herbs and 12 medicinal herbs were determined. The ORAC values and total phenolic contents for the medicinal herbs ranged from 1.88 to 22.30 micromol of Trolox equivalents (TE)/g of fresh weight and 0.23 to 2.85 mg of gallic acid equivalents (GAE)/g of fresh weight, respectively. Origanum x majoricum, O. vulgare ssp. hirtum, and Poliomintha longiflora have higher ORAC and phenolic contents as compared to other culinary herbs. The ORAC values and total phenolic content for the culinary herbs ranged from 2.35 to 92.18 micromol of TE/g of fresh weight and 0.26 to 17.51 mg of GAE/g of fresh weight, respectively. These also were much higher than values found in the medicinal herbs. The medicinal herbs with the highest ORAC values were Catharanthus roseus, Thymus vulgaris, Hypericum perforatum, and Artemisia annua. A linear relationship existed between ORAC values and total phenolic contents of the medicinal herbs (R = 0.919) and culinary herbs (R = 0.986). High-performance liquid chromatography (HPLC) coupled with diode-array detection was used to identify and quantify the phenolic compounds in selected herbs. Among the identified phenolic compounds, rosmarinic acid was the predominant phenolic compound in Salvia officinalis, Thymus vulgaris, Origanum x majoricum, and P. longiflora, whereas quercetin-3-O-rhamnosyl-(1 --> 2)-rhamnosyl-(1 --> 6)-glucoside and kaempferol-3-O-rhamnosyl-(1 --> 2)-rhamnosyl-(1 --> 6)-glucoside were predominant phenolic compounds in Ginkgo biloba leaves.
Article
Four cultivars (Bronowicka Ostra, Cyklon, Tornado, and Tajfun) of pepper fruit Capsicum annuum L. were studied for phenolics contents and antioxidant activity. Two fractions of phenolics, flavonoids (with phenolic acids) and capsaicinoids, were isolated from the pericarp of pepper fruit at two growth stages (green and red) and were studied for their antioxidant capacity. Both fractions from red fruits had higher activities than those from green fruits. A comparison of the capsaicinoid fraction with the flavonoid and phenolic acid fraction from red fruit with respect to their antioxidant activity gave similar results. Phenolic compounds were separated and quantified by LC and HPLC. Contents of nine compounds were determined in the flavonoid and phenolic acid fraction: trans-p-feruloyl-beta-d-glucopyranoside, trans-p-sinapoyl-beta-d-glucopyranoside, quercetin 3-O-alpha-l-rhamnopyranoside-7-O-beta-d-glucopyranoside, trans-p-ferulyl alcohol-4-O-[6-(2-methyl-3-hydroxypropionyl] glucopyranoside, luteolin 6-C-beta-d-glucopyranoside-8-C-alpha-l-arabinopyranoside, apigenin 6-C-beta-d-glucopyranoside-8-C-alpha-l-arabinopyranoside, lutoeolin 7-O-[2-(beta-d-apiofuranosyl)-beta-d-glucopyranoside], quercetin 3-O-alpha-l-rhamnopyranoside, and luteolin 7-O-[2-(beta-d-apiofuranosyl)-4-(beta-d-glucopyranosyl)-6-malonyl]-beta-d-glucopyranoside. The main compounds of this fraction isolated from red pepper were sinapoyl and feruloyl glycosides, and the main compound from green pepper was quercetin-3-O-l-rhamnoside. Capsaicin and dihydrocapsaicin were the main components of the capsaicinoid fraction. A high correlation was found between the content of these compounds and the antioxidant activity of both fractions. Their antioxidant activities were elucidated by heat-induced oxidation in the beta-carotene-linoleic acid system and the antiradical activity by the 1,1-diphenyl-2-picrylhydrazyl (DPPH) decoloration test. The highest antioxidant activity in the beta-carotene-linoleic acid system was found for trans-p-sinapoyl-beta-d-glucopyranoside, which was lower than the activity of free sinapic acid. Quercetin 3-O-alpha-l-rhamnopyranoside had the highest antiradical activity in the DPPH system, which was comparable to the activity of quercetin. The activities of capsaicin and dihydrocapsaicin were similar to that of trans-p-feruloyl-beta-d-glucopyranoside in the DPPH model system.
Effect of method drying on sorption characteristics of model fruit powders
  • E Tsami
  • M K Krokida
  • A E Drouzas
Tsami, E., M.K. Krokida and A.E. Drouzas. 1999. Effect of method drying on sorption characteristics of model fruit powders. J. Food Eng. 38: 381-392.