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Low Temperature Superplasticity of Submicrocrystalline Titanium Alloys

Trans Tech Publications Ltd
Materials Science Forum
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Abstract

Severe plastic deformation at temperatures below 0.4...0.5Tm was used to obtain submicrocrystalline (SMC) structure in pure titanium and titanium alloys Ti-6.7Al-4.7Mo and Ti-11Mo-5.5Sn-4.2Zr. The structural studies showed that the density of titanium and its alloys in the SMC condition was less that in the coarse grained (CG) one. This change is connected with the presence of less-density intercrystalline regions. Low temperature superplasticity was studied in the temperature range 450...575°C. A considerable dependence of ductility on alloy composition was shown. The calculated value of apparent activation energy of the Ti-6.7Al-4.7Mo was equal to 315 kJ/mol at n=2.3, that being higher than during superplastic (SP) deformation of the alloy with usual microstructure.
Materials Science Forum Vols. 243-245 (1997) pp 585-590
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© (1997) Trans Tech Publications, Switzerland
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publisher: Trans Tech Publications Ltd, Switzerland, www.ttp.net. (ID: 212.193.134.82-15/12/08,13:07:52)
2 Superplasticity in Advanced Materials - ICSAM-97
Materials Science Forum Vols. 243-245 3
4 Superplasticity in Advanced Materials - ICSAM-97
Materials Science Forum Vols. 243-245 5
6 Superplasticity in Advanced Materials - ICSAM-97
Superplasticity in Advanced Materials - ICSAM-97
doi:10.4028/0-87849-759-5
Low Temperature Superplasticity of Submicrocrystalline Titanium Alloys
doi:10.4028/0-87849-759-5.585
Materials Science Forum Vols. 243-245 7
... Ti-6Al-4V alloy with an ultrafine grain microstructure obtained via severe plastic deformation techniques can achieve excellent elongation at a lower temperature of 600 • C [36,37], which limits the wide application. These limitations can be short-came by reformulating the alloy chemistry, such as ATI425 and Ti54M alloy that can obtain a lower optimum forming temperature below 900 • C [38][39][40][41]. ...
Article
Full-text available
The superplastic tensile test was carried out on SP700 (Ti-4.5Al-3V-2Mo-2Fe) titanium alloy sheet at 760 °C by the method of maximum m value, and the microstructure characteristics were investigated to understand the deformation mechanism. The results indicated that the examined alloy showed an extremely fine grain size of ~1.3 μm and an excellent superplasticity with fracture elongation of up to 3000%. The grain size and the volume fraction of the β phase increased as the strain increased, accompanied by the elements’ diffusion. The β-stabilizing elements (Mo, Fe, and V) were mainly dissolved within the β phase and diffused from α to β phase furthermore during deformation. The increase in strain leads to the accumulation of dislocations, which results in the increase in the proportion of low angle grain boundaries by 15%. As the deformation process, the crystal of α grains rotated, and the texture changed, accompanied by the accumulation of dislocations. The phase boundary (α/β) sliding accommodated by dislocation slip was the predominant mechanism for SP700 alloy during superplastic deformation.
... Moreover, processing of the alloy by high-pressure torsion decreases the temperature by 200 K and increases the strain rate of superplastic deformation by two orders of magnitude [2]. The same effect is found in ultrafine-grained alloy processed by equal channel angular pressing (ECAP) and multiaxial forging [3,4]. Thus, the formation of the ultrafine-grained structure in Ti-based alloys using severe plastic deformation is a promising way to improve their mechanical and physical chemical properties. ...
Conference Paper
The comparative TEM investigation of the structure of Ti-6Al-4V alloy processed by equal channel angular pressing at 973 K and helical rolling followed by groove rolling in the temperature interval 1123–923 K is carried out. It is found that the ultrafine-grained state with the grain size less than 1 µm and numerous high-angle grain boundaries is not formed by these methods at indicated temperatures. It is assumed that the reasons for the negative result are the high deformation temperature resulting in partial recrystallization of the alloy in the former case and the insufficient strain degree in the latter case.
... For example, the alloy Ti-6Al-3.2Mo with the grain size of 60 nm showed high superplastic properties at 575ºC and strain rate of 2×10 -4 s -1 : the total elongation of 1200%, strain rate sensitivity m=0.45 and flow stress σ=165 MPa were achieved [13]. ...
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Volume 22A provides a thorough review of computational modeling and its application in the development of alloys and associated processing techniques. It describes the basic concepts of modeling and simulation and accepted practices in the use of finite elements, computational fluid dynamics, mechanistic and phenomenological modeling, and statistical approaches. It addresses a wide range of processes, including deformation and solidification transformations, recrystallization, grain growth, precipitation, strengthening, and the evolution of microstructure and surface texture. It offers insight on damage evolution processes as well, examining cavitation, fracture, hot tearing, creep, crack growth, and fatigue. It also discusses phase equilibria and phase field modeling, state variable and constitutive modeling, electronic structure modeling, and density functional theory. It explains how use models to simulate and control mechanical properties and minimize defects in specific steels, aluminum, titanium, and superalloys. The volume also includes physical data, mathematical reference information, and a discussion on length scales and relevant effects. For information on the print version of Volume 22A, ISBN 978-1-61503-001-9, follow this link.
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Chapter
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