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Publications (37)
Iron (Fe)-incorporated zinc oxide (ZnO) nanoparticles (NPs) were synthesized via chemical precipitation technique and studied using powder X-ray diffraction (PXRD), field emission scanning electron microscopy (FESEM), and UV–vis diffuse reflectance spectroscopy. PXRD analysis reveals a hexagonal wurtzite structure for all the synthesized samples. U...
The structural, optical, morphological, and electrical properties of polycrystalline copper-doped tin sulfide (Cu-Sn2S3) thin films with different concentrations of Cu dopants were synthesized using the spray pyrolysis method. Structural characterizations (powder XRD) revealed orthorhombic Sn2S3 crystal structure with Pmma space group. The XRD spec...
The present investigation reports the successful incorporation of Graphite into the PPy matrix via a chemical in-situ polymerization technique. Obtained composites were thoroughly studied by using powder X-ray diffraction (PXRD), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FT-IR). The corrosion inhibition respons...
Organic effluents—the gift of industrial development is a critical menace to environs as well as raising a question mark toward the sustainability of humans. In such a scenario, achieving consistent sunlight-driven photocatalytic degradation gains widespread attention due to its eco-friendly low-cost approach with high efficiency. Herein, the CdS-c...
Semiorganic crystals are hybrid materials that have captured the interest of researchers due to their improved material characteristics and applications. In the current work, single crystals of oxalic acid dihydrate (OAD), Ammonium oxalate hydrate (AHO), and Ammonium hydrogen oxalate oxalic acid dihydrate (AHOOD) were grown using a slow evaporation...
The structural, optical, mechanical and electrical properties of pure and 5—20-kGy gamma-irradiated semi-organic single crystals of ammonium hydrogen oxalate oxalic acid dihydrate (NH4H3(C4O8).2H2O) are presented. The crystals were synthesized at room temperature using facile solvent evaporation technique. Powder XRD measurements indicate gradual e...
A metal–organic hybrid compound named potassium hydrogen oxalate oxalic acid dihydrate (KH3(C4O8)·2H2O) single crystal (KHOOD) is synthesized using a facile and different approach. The obtained crystals are thoroughly investigated using single crystal XRD (SCXRD), powder XRD (PXRD), UV–Vis absorption, photoluminescence, TGA-DTA and dielectric measu...
The viability of tellurium (Te)-based Te90Si5Sn5 alloy synthesized using the facile melt-cooling method is explored in the photocatalytic degradation of methylene blue (MB) and crystal violet (CV) dye molecules. The Te90Si5Sn5 alloy catalyst synthesized by doping Te host dually with Si and Sn dopants exhibits absorption in the visible region, favor...
The article focuses on the suitability of electrically characterized polypyrrole-banana carbon (PPy-BC) nanocomposites for broadband electromagnetic interference (EMI) shielding application. The environmental-friendly polypyrrole (PPy)-banana carbon (BC) nanocomposites were synthesized via in situ chemical polymerization technique and were characte...
The quick responsive and durable supercapacitive performance was achieved from reduced graphene oxide/zinc hydroxide/polyaniline (rGO5.88%/Zn(OH)211.77%/PANI82.35%) (GZnP82) nanocomposite, synthesized by in-situ single step. The GZnP82 provided a specific capacitance (Cs) of 173.60 F g‒1, a specific capacity (Q) of 208.32 C g‒1, a specific energy o...
A different approach used in the synthesis of ammonium hydrogen oxalate oxalic acid dihydrate (NH4H3(C4O8)·2H2O) single crystals is presented. The crystals are synthesized using solvent evaporation technique. The analysis of the synthesized NH4H3(C4O8)·2H2O single crystals has been carried out through measurements such as single-crystal X-ray diffr...
The structural, optical, mechanical, electrical and nonlinear properties of standard Ammonium Dihydrogen Phosphate (NH4H2PO4, ADP) single crystals incorporating organic Erioglaucine dye dopant are presented. The effect of Erioglaucine dye dopant at varied concentration on these properties has been investigated through measurement of powder X-Ray Di...
Synthesis of polypyrrole (PPy) / graphite (G) composites via chemical oxidation polymerization method is reported. Synthesized composites were studied for its structural, optical and electrical properties. Structural and morphological studies were performed using powder X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron m...
In the present investigation, synthesis of pristine and methyl orange dye-doped potassium hydrogen oxalate oxalic acid dihydrate (KHOOD) single crystals are reported. In this study, the structural properties of the crystals were investigated using powder XRD and the effect of dye incorporation on the KHOOD crystal was explored in detail. The effect...
The potassium hydrogen oxalate oxalic acid dihydrate (KHOOD) single crystals were grown using solvent evaporation technique. The mechanical hardness of grown KHOOD single crystal was performed using Vickers microhardness tester and investigated for different loads starting from 10 g to 100 g and it was decided to include under hard material categor...
Influence of amaranth dye on the potassium hydrogen oxalate oxalic acid dihydrate (KHOOD) single crystal is investigated. The structural studies were carried out to understand the crystal behavior after dye incorporation. Optical studies were performed to investigate the photon absorption of the crystal with or without the presence of dye molecule....
Single crystals of Oxalic acid dihydrate (OAD), Potassium oxalate hydrate (KOH), Potassium hydrogen oxalate oxalic acid dihydrate (KHOOD) were grown using solvent evaporation technique. Unit cell parameters of the crystals were studied using single crystal XRD (SCXRD) and the crystal parameters were found to match with the reported values. Structur...
Semiorganic crystals play vital role in the design and development of optical devices. In this context, we report the synthesis of metalorganic potassium hydrogen oxalate oxalic acid dihydrate (KHO) single crystals using slow solvent evaporation technique. Further, Co(OH)2 nanoparticles pre-synthesized using hydrothermal method are doped to KHO sin...
The pristine and AgNP-doped TGS crystals are studied using powder X-ray diffraction, density measurements, solubility studies, UV–Vis analysis, photoluminescence spectroscopic analysis, thermal gravimetric analysis, differential thermal analysis, differential scanning calorimetry, Vicker’s hardness measurements, I–V and impedance measurements. From...
Potassium oxalate oxalic acid dihydrate (KHO) single crystals were grown from solvent evaporation technique at room temperature. Crystals were optically characterized using UV–Vis and photoluminescence analysis. The gamma irradiation effects on KHO crystals were also studied optically and the results were analyzed to compare the effect of irradiati...
In the present work, a synthesis and comparative study on the effect of Zinc (Zn) on thiourea barium chloride (TBC) single crystals has been reported. Crystals of thiourea barium chloride and Zn-doped thiourea barium chloride crystals are prepared using slow evaporation from the saturated solution. The samples were subjected to single crystal and p...
In the present study, TBC single crystals were synthesized using solution evaporation method. The structural analysis of TBC crystal was studied using Powder X-ray diffraction. Optical properties of TBC crystals were carried out using UV-Vis, FTIR, Raman and photoluminescence (PL) spectra. The crystal shows absorbance maxima at 209 nm and transpare...
