Juliana Azevedo Lima PalloneState University of Campinas (UNICAMP) | UNICAMP · Departamento de Ciência de Alimentos (DCA)
Juliana Azevedo Lima Pallone
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Publications (109)
Rice is considered a staple food in Asia, Africa, and Latin American countries. As interest in healthier lifestyles
increases, the market for organic brown rice is growing. Concurrently, there is a rising concern about developing
fast and environmentally friendly analytical monitoring tools that can ensure the quality of brown rice by dis
tinguishi...
This review explores the historical, botanical, sensory, and quality aspects of Coffea canephora, with a focus on Brazil’s rise as a producer of specialty canephora coffees in the Amazon region, Espírito Santo, and Bahia. Brazil has gained global recognition through the first geographical indications for canephora: Matas de Rondônia for robusta ama...
Purslane (Portulaca oleracea) and spinach (Spinacea oleracea) are species with elevated levels of oxalic acid, an antinutrient that interferes in the bioaccessibility of minerals such as calcium and iron. Evaluating methods to determine oxalic acid content with reduced matrix interference, such as employing Flame Atomic Absorption Spectrometry (FAA...
The nutritional quality of 132 plant-based meat alternatives (PBMAs) and 242 plant-based dairy alternatives (PBDAs) in the Brazilian market was evaluated for nutritional content reported in the labeling. Added sugar, saturated fat, and sodium limits were also observed according to the new Brazilian front-of-pack labeling (FOPL). In general, PBMAs h...
Integration of first- and second-generation ethanol production is a strategy to strengthen the economic viability of individual processes and the overall viability of biorefineries. The sharing of storage, fermentation, distillation, and energy infrastructure is an important advantage of process integration. Furthermore, integration contributes to...
The use of microencapsulated ferrous-sulfate is among the various options recommended for food fortification, as the protective wall material surrounding the compound can preserve it from undesirable alterations and also protect the food. Microencapsulated iron can be produced using different wall materials and encapsulation methods. Thus, a microp...
The study estimated the bioaccessibility of calcium, phosphorus and magnesium in organic milk (ORG), compared to conventional (CNV) by the INFOGEST in vitro protocol. Total proteins, lipids and lactose were evaluated, the determination of essential minerals was performed by FAAS and phosphorus by colorimetric method. All ORG samples showed protein...
New Brazilian Canephora coffees (Conilon and Robusta) of high added value from specific origins have been protected by geographical indication to guarantee their origin and quality. Recently, benchtop near-infrared (NIR) spectroscopy combined with chemometrics has demonstrated its usefulness to discriminate them. It was the first study, however, an...
Robusta Amazônico is the name given to the Amazonian coffee that has been becoming popular and has recently been registered as a geographical indication in Brazil. It is produced by indigenous and non-indigenous coffee producers in regions that are geographically very close to one another. There is a need to authenticate whether coffee is truly pro...
Plant-based beverages could contain iron but also phenolic compounds (PC) and ascorbic acid, which are considered modulators of iron uptake. We investigated whether iron from almond and coconut beverages can be taken up by Caco-2 cells. The iron content in almond and coconut beverages was 19.20 and 19.34 mg kg ⁻¹ dry weight (dw), respectively; PC w...
Rice beverages are commonly fortified with minerals to improve their nutritional value. However, the effect of fortification on mineral bioaccessibility is poorly understood. Thus, the effects of fortification of a rice beverage on mineral concentration and bioaccessibility using calcium carbonate (CaCO3), tricalcium phosphate (Ca3(PO4)2), sodium i...
This study aimed at reducing the amount of salt added to potato chips by decreasing the size of salt particles. First, a selected panel ( n = 15 assessors) evaluated the saltiness of potato chips added with refined and microparticulated salt using the magnitude estimation. The amount of 1.6% of refined salt, previously determined as just‐about‐righ...
Barley is an important crop worldwide, and it can be affected by various fungi, among them Fusarium is one of the most relevant due to the economic losses caused by mycotoxin contamination. Enniantins (ENNs) are one of the emergent group of mycotoxins that have been found in grains around the world. Nowadays, the main analytical tools available to...
This study aimed to validate an alternative analytical method of samples preparation to evaluate the content of essential elements (Ca, Mg, Fe, Zn, Cu, Mn, Na, and K) in plant-based burgers (PBBs) marketed in Brazil, formulated with mushroom, pea, chickpea, and soybean. Samples are prepared by wet mineralization in the open system in digester block...
Goat cheeses have important nutritional properties, with an emphasis on proteins, lipids (high digestibility), and essential minerals. This study analyzes the bioavailability of Ca, Mg, and Zn in Brazilian cheeses using an in vitro dynamic digestion method. Two self-produced fresh cheeses, cow and goat Minas frescal cheese, and two commercial matur...
The objective of this work was to investigate and characterize new rice cultivars still little explored and never reported in the literature but of nutritional and economic potential. For this, the Brazilian cultivars IAC 500 (aromatic) and IAC 2157 (non-aromatic) were analyzed and compared regarding their proximate composition, amylose content, fa...
The buritirana is a little-explored species of the Arecaceae family. The biometric and physicochemical characteristics, nutritional and chemical composition and antioxidant and antibacterial potential of the buritirana fruit fractions were evaluated here for the first time. The fruits presented an oblong shape. The pulp represented 16.58% of the wh...
Bovine cheese whey presents physico-chemical similarity with goat cheese whey, making the occurrence of adulteration of goat dairy beverage by addition of bovine whey possible. This study aimed to develop a green analytical method, using NIR spectroscopy and Data Driven–Soft Independent Modelling of Class Analogies (DD-SIMCA), to verify the authent...
The consumption of processed meat products has increased due to its convenient preparation and characteristics related to taste and consumer acceptance. In this study, we evaluated the content and bioaccessibility of iron (Fe), zinc (Zn), calcium (Ca) and magnesium (Mg) in processed pork and beef products by dialysis assay. In addition, different a...
The nutritional quality and bioactive potential of breads made with partial replacement of refined wheat flour (RWF) with 30% or 45% refined buckwheat flour (RBF) or whole buckwheat flour (WGBF) was assessed through mineral bioaccessibility, starch digestibility, dietary fiber content and bioactive potential by determining rutin and quercetin level...
Rapadura is an artisanal candy obtained from concentrated sugarcane juice. In this study, a differentiation between South American rapadura producers has been tried using a Kurtosis-based projection pursuit analysis (kPPA) concerning essential minerals, acrylamide, moisture contents, pH, and color. These parameters revealed significant inter- and i...
The study evaluated the effect of goat and cow milk processing on the bioaccessibility of calcium, magnesium and zinc using different methods following the static in vitro simulation of gastrointestinal digestion: solubility and dialysis models. Raw goat and cow milks were processed to obtain pasteurized milk, yogurt and cheese. In general, goat mi...
Cheese has important nutritional properties as a result of their protein, lipid and essential minerals content. This study analyzed the bioavailability of Ca, Mg and Zn in Brazilian cheeses, using the in vitro INFOGEST digestion method coupled with assays in Caco-2 cells. Furosine content (marker of the early Maillard reaction) was also evaluated....
Exclusive breastfeeding is recommended for newborns until at least the sixth month. However, in some cases, the use of infant formulas as breast milk replacement has been used to provide the nutritional needs of infants. For children over six months baby foods can often be incorporated into the diet. Aluminium (Al) could be present in baby foods an...
Regarding mycotoxin exposure, weaned infants and young children are a particular vulnerable subgroup when compared to adults, due to their distinct metabolic rates and lower body weight. In this review, the occurrence and co-occurrence of mycotoxins in baby food and values of daily intakes are presented. Since not all mycotoxin content described by...
Peruvian Andean maize (PAM) has been commonly used as an ingredient that confers color, flavor, and texture in culinary. Nevertheless, no studies are focusing on agro-industrial interest characteristics to develop new products. This study aimed to evaluate the physicochemical, nutritional, and technological characteristics of kernels and the starch...
Goat dairy products are the target of fraudulent practices due to their high commercial value. This study evaluated the capacity of vibrational spectroscopy Near Infrared (FT-NIR) coupled with chemometric tools to detect goat’s yogurt and cheese adulterated with cow milk. Principal Component Analysis (PCA), Q-control chart and Partial Least Squares...
The development of green analytical techniques for food industry quality control has become an important issue in the context of the fourth industrial revolution. In this sense, near infrared spectroscopy (NIR) and smartphonebased imaging (SBI) were applied to evaluate the bioactive potential of freeze-dried açai pulps. For this purpose, reference...
Deoxynivalenol (DON) is one of the mycotoxins produced mainly by the Fusarium graminearum species complex in small grain cereals, including barley. This toxin can cause alimentary disorders, immune function depression and gastroenteritis. The negative health effects associated with DON coupled to the increasing concern about green and rapid methods...
Goat milk has a potential target of fraud. In this sense, Near Infrared Spectroscopy (NIRS) have been successfully used to detect food fraud. This study aimed to develop multivariate classification models using NIRS to detect adulterants in goat milk. Principal Component Analysis (PCA), control chart, k-Nearest Neighbor (k-NN), Part Least Square-Di...
Consumption of plant-based beverages (PBB) is a growing trend; and have been used as viable substitutes for dairy based products. To date, no study has comparatively analyzed mineral composition and effect of in vitro digestion on the bioaccessibility of different PBB. The aim of this research was to investigate the content of essential minerals (c...
The aim of this study was to investigate the feasibility of applying near infrared spectroscopy (NIR), associated with multivariate calibration, which is characterized as a fast and green technique, to evaluate Fe, Ca, K and Na in commercial hamburger samples and for sodium control, according to the law. PLS models obtained by NIR to predict the es...
Fruta-do-lobo (Solanum lycocarpum St. Hill) is a native fruit commonly used in Brazilian folk medicine as a hypoglycemic agent. These properties are attributed to their starch, mainly its resistant fraction. Resistant starch has shown to increases the growth of Bifidobacterium and Lactobacillus in the gut, even though not being selective for these...
Powdered soft drinks (PSDs), fortified with antioxidants such as ascorbic acid (AA), are normally controlled by titration or chromatographic methods. This study evaluated the feasibility of using near-infrared spectroscopy (NIRS) and multivariate analysis to predict AA contents in PSDs as an alternative not-destructive method. The AA content of six...
Excessive sodium (Na) consumption can lead to serious health problems such as hypertension, and cardiovascular and renal diseases. Therefore, the food industry in worldwide has been trying to reduce sodium levels in processed products. The aim of this study was to validate a method and quantify sodium in processed and packaged foods and to estimate...
The United Nations Organization predicts a scenario where the world population will be up to 10 billion people by 2050. As the population grows the demand for food will increase. For this reason, insect consumption by humans has been encouraged as an alternative to the conventional protein sources. Insect consumption is highly sustainable if compar...
A análise de selênio em alimentos pode ser realizada por diversas técnicas, entre elas a Espectrometria de Absorção atômica com gerador de hidretos, a qual se apresenta como uma técnica sensível e de baixo custo. Para tanto, é necessário um preparo prévio de amostras de alimentos, conhecido como processo de mineralização, em que há a decomposição d...
O trabalho teve como estudo o impacto do probiótico (Lactobacillus acidophilus) e adição de resíduo agroindustrial (Farinha de bagaço de Laranja) na bioacessibilidade do cálcio em leites fermentados.
Jambu (Acmella oleracea (L.) R.K. Jansen) is a neglected plant native to the Amazon Biome. Although it is very consumed in the north of Brazil, little is known about its chemical and nutritional composition. Thus, this study aimed to characterize jambu and to evaluate the effects of the boiling process on its chemical composition. The proximate com...
In this study we evaluated the proximate composition of two Solanaceae fruits from Brazilian Cerrado, their mineral content, volatile organic compounds (VOCs), phenolic compounds profile, and antioxidant capacity employing Oxygen Radical Absorbance Capacity (ORAC) assay, for each part of the fruits (pulp, peel and seeds). Our results showed that th...
The aim of this study was to evaluate the effects of fortification of whole wheat flour with different iron compounds, such as ferrous sulfate (FS), ferrous fumarate (FF), reduced iron (RI), ferric sodium ethylenediaminetetraacetate (NaFeEDTA), microencapsulated ferrous sulfate (FSm) and microencapsulated ferrous fumarate (FFm), on quality paramete...
The characterization of the modifications that may occur during the storage of iron-fortified wheat flour is an important tool for understanding the variations in the product quality, since iron may present pro-oxidant activity. Therefore, the aim of this study was to evaluate the effect of refined wheat flour fortification with different iron comp...
The objective of this study was to evaluate in vitro bioaccessibility of calcium (Ca), iron (Fe) and zinc (Zn) in soy drink after phytase treatment and correlate it with the content of myo-inositol phosphates. Samples of commercial soy drink products and one sample produced in the laboratory by maceration were evaluated. Phytase was applied using 3...
The aim of this work was to develop a method for the determination of antimony (Sb) in polyethylene terephthalate (PET) bottles and to evaluate its migration into soft drink and simulant. In this context, a new procedure for PET sample preparation, using a high pressure asher (HPA), is presented for the determination of Sb by inductively coupled pl...
Açai pulp suffers adulteration by the addition of less expensive materials with the objective to increase yield and consequently the profit margin. Near-infrared spectroscopy has been used in the present work to detect adulteration of freeze-dried açai pulp samples. Adulterants used included cornstarch, beet pulp, grape juice, cassava starch, and m...
The aim of this study was to optimize and validate a simple method for determination of the potential of important minerals for health (calcium, iron, zinc, and magnesium) in residue from orange and lemon juice industries and determine whether there are differences concerning these nutrients during the months when these fruits were harvested. The m...
The aim of this study was to estimate bioaccessibility of Ca, Fe and Mg in residues of orange, lime, and their mixture, in order to evaluate the effects of cooking in water on mineral bioaccessibility and also to determine the composition of macronutrients and myo-inositol phosphate content. The citrus samples contained on average 9.53 g/100 g mois...
This study aimed at investigating the effect of iron compounds used in whole wheat flour (WWF) fortification, both on rheological properties of the dough and on bread technological quality. Furthermore, bioaccessibility of iron (Fe), zinc (Zn) and calcium (Ca) in the final breads was determined. Rheological properties (mainly dough development time...
This study shows the use of time-domain (TD)-NMR transverse relaxation ( T <sub>2</sub>) data and chemometrics in the nondestructive determination of fat content for powdered food samples such as commercial dried milk products. Most proposed NMR spectroscopy methods for measuring fat content correlate free induction decay or echo intensities with t...
Iron deficiency is one of the most important nutritional problems in theworld. The aims of this studywere to determine the total concentration of iron in order to evaluate its bioaccessibility in biscuits produced with fortified flour, check the importance of its contribution to the iron intake and monitor physicochemical parameters such as moistur...
The aim of this study was to propose a method for analysis of lead (Pb), cadmium (Cd), mercury (Hg) and arsenic (As) in polypropylene packaging intended for contact with ice cream and migration of these elements using the food itself and 3 % acetic acid as food simulant. Ten commercial samples of ice cream marketed in Campinas-São Paulo (Brazil) we...
Nowadays, most analytical methods used in the quality control of food products are based on wet chemical methods, which are destructive and generate toxic chemical waste. Therefore, in this study, we are proposing a nondestructive, noninvasive, wasteless method for quality control of mustard sauces, in sealed packets, using time-domain nuclear magn...
The aim of the present work was to evaluate molar ratio iron: zinc and the levels of folic acid in biscuit and snacks commercialized in Brazil, prepared with folic acid and iron fortified flours. These nutrients are important for human nutrition; however, iron can have a negative effect on zinc absorption. Molar ratio iron:zinc can indicate if ther...
The purpose of this paper was to assess the concentration of lead (Pb), cadmium (Cd), mercury (Hg) and arsenic (As) in high-density polyethylene (HDPE) packaging intended for contact with yoghurt and the migration of these elements using the food itself and 3% acetic acid as a food simulant in accordance to ANVISA, the Brazilian Health Surveillance...
This study examined the ability of near-infrared reflectance spectroscopy method (FT-NIRS) and multivariate calibration to estimate the concentration of moisture, protein, lipid, ash and carbohydrate of Brazilian soybeans. The spectra obtained in the range of 4000 to 10,000 cm− 1 were preprocessed by several combinations of mathematical treatments:...
The effect of the addition of glucose oxidase as a technological option todecrease the oxidative stress in a stirred yogurt during 15 days of refrigerated storage was investigated. A significant increase in the viable population of Bifidobacteria longum (6.9–8.7 log CFU g−1) was observed in all yogurts added with glucose oxidase and glucose. Additi...
Soybean based fruit juices and soymilk has been constantly increasing their market share among non-alcoholic beverages in the Brazilian market. Besides, companies adding some essential minerals like iron and zinc to these products, aiming to produce healthier beverages, are more appealing to their consumers. Although according to the Brazilian regu...
IntroductionMetabolic fingerprint is a high-throughput screening to provide a sample classification.Objectives
Herein, we describe a metabolic fingerpint strategy for proof of authenticity and possible adulteration of natural products. This strategy provides useful and complementary information to food science for content analysis.Methods
Twelve sa...
Multivariate statistical design modeling and the Derringer-Suich desirability function analysis were applied to micellar electrokinetic chromatography (MEKC) results with anionic surfactant to separate carbohydrates (CHOs) in different food matrices. This strategy has been studied with success to analyze compounds of difficult separation, but has n...
Cited By (since 1996):4, Export Date: 26 October 2013, Source: Scopus
Some countries, including Brazil (resolution - RDC # 344, 2004), have issued a regulation stipulating that corn and wheat flours have to be fortified with folic acid and iron. The main objective of this work was to investigate some enriched flour characteristics using Principal Component Analysis (PCA). Wheat and corn flours presented, on average,...
In 2002, Brazil issued a regulation requiring that corn and wheat flours be fortified by the addition of folic acid and iron. The aim of the present work was to evaluate the levels of folic acid, iron, and zinc in macaroni. pizza, and bread prepared with fortified flour. The methodologies used for the mineral (FAAS) and vitamin (HPLC) determination...