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Introduction
Publications
Publications (23)
In this paper, we present indirect methods to define the change in the rates of hydrolysis and condensation reactions of a silica oxide network formed of (3-glycidoxypropyl)methyltriethoxysilane (GPTMS) and (3-aminopropyl)triethoxysilane (ApTEOS), which was strongly dependent upon the nature of the solvent used in the reaction environment, such as...
The study investigated the effect of aging time on the protective properties of submicron thickness sol-gel coatings. Coatings were based on zirconia and silica modified with fluoroalkyl substituents that were deposited on P265GH steel and were aged for 3 years. The corrosion tests were carried out in sodium chloride solution and liquid caprolactam...
Development of silica aerogels for real applications requires control of their mechanical properties. Based on the sol-gel procedure and using the alkoxide precursor of silica (TMOS), native silica aerogels were synthesized. This work explores the influence of three synthesis parameters, namely, TMOS concentration, catalyst concentration, and solve...
During the manufacturing of composite pressure vessels, the fiber tension of the filament winding process has an important influence on the mechanical properties as well as on the gravimetric efficiency of the structure and is therefore investigated within this paper. Three series of samples were manufactured and tested: A) steel liners as referenc...
Material as well as process variations in the composites industry are reasons to develop methods for in-line monitoring, which would increase reproducibility of the manufacturing process and the final composite products. Fiber Bragg Gratings (FBGs) have shown to be useful for monitoring liquid-composite molding processes, e.g., in terms of online g...
In this paper, we present indirect methods to define the change in the rates of hydrolysis and condensation reactions of a silica oxide network formed of (3-glycidoxypropyl)methyltriethoxysilane (GPTMS) and (3-aminopropyl)triethoxysilane (ApTEOS), which was strongly dependent upon the nature of the solvent used in the reaction environment, such as...
Automated tape layup (ATL) has been used extensively for manufacturing composites laminates using unidirectional prepregs for high-performance industries like aerospace. Residual stress is one of the defects that adversely affect the layup quality. These stresses affect geometrical tolerances in the form of distortion of the final product and are f...
In this paper, the application of a fiber Bragg grating written in a highly birefringent side-hole elliptical core optical fiber for two-axial strain measurement is presented. Hybrid optical fiber structures achieved by combining large side-holes and elliptical core result in a very high birefringence of 1 × 10−3 and thus high initial Bragg peak sp...
This paper analyses the issues relative to the modelling of tubular (cylindrical) composite structures. This paper aims to describe the design of a multi-layer structure of filament-wound composite pipes where, after loading, the hoop-stress distribution would be as uniform as possible. That would allow the mass of the composite to decrease while m...
A polyethylene (PE) liner is the basic element in high-pressure type 4 composite vessels designed for hydrogen or compressed natural gas (CNG) storage systems. Liner defects may result in the elimination of the whole vessel from use, which is very expensive, both at the manufacturing and exploitation stage. The goal is, therefore, the development o...
This paper presents the result of the investigation of organically modified silica (ORMOSIL)-zirconia coatings used to enhance their protective properties, namely corrosion and scratch resistance. Two different materials, i.e., SiO2/ZrO2 and SiO2/GPTMS/ZrO2, were synthesized, measured, and analyzed to find the difference in the used organosilane pr...
In this study, a novel approach of silica-PVA hybrid aerogel synthesis is presented based on the simultaneous sol-gel reaction of the silica precursor tertramethoxysilane (TMOS) and thermally impacted non-solvent induced phase separation of polyvinyl alcohol (PVA). The method based on: (1) water from PVA solution is required for hydrolysis of TMOS;...
The detailed information about the growth of organically modified silica networks regarded as useful for barrier coatings and membrane coatings preparation are the subject of this paper. The networks obtained using different precursors containing non-hydrolysable organic groups: dimethyldiethoxysilane – dMdEOS, ethyltriethoxysilane – EtEOS, n-propy...
In the present work silica (SiO2) coatings as interlayer and silica-titania (SiO2/TiO2) hybrid coatings as top layers, obtained by the sol-gel method and successfully applied on the polymeric substrate, were investigated as a sealing coatings. Materials were newly obtained and the morphological and structural investigations were performed. The stud...
The main purpose of the work was development of high-pressure composite vessel for hydrogen storage (type IV, CFRC) with an integrated Structural Health Monitoring (SHM) system, based on optical fiber sensors. It has been assumed that this NDE system should provide for continuous and reliable monitoring of the structure during its long operation an...
The work presents the methodology of displacement and strain measurements (in type IV composite high pressure hydrogen and methane storage vessels in areas of the gaseous fuel cell vehicle. The research was conducted in vessels with so called programmed defects in the form of notches and delamination. The complementary optical methods, namely: opti...
The modification of carbon fibers for improving adhesion between fibers and an epoxy resin in composite materials has become the focus of attention. In this work the carbon fiber coating process has been devised in a way preventing the stiffening and clumping of fibers. To improve interactions between coated fibers and a resin in composites, four t...
This article describes the dynamic mechanical analysis of the behaviour of magnetorheological composites consisting of a magnetically active filler (carbonyl iron powder) and a soft thermoplastic elastomer matrix (styrene-ethylene-butylene-styrene). The carbonyl iron particle surface was coated by a sol–gel silica layer to improve the adhesion betw...
This article presents a method for modification of carbonyl iron particles’ surface (CIP), (d50=4-9 µm) by silica coatings obtained using the sol-gel method. Reaction parameters were determined to obtain dry magnetic powder with homogeneous silica coatings without further processing and without any by-product in the solid or liquid phase. This appr...
Many production processes in chemical industry generates hydrogen as a by-product. Part of this is reused in the other production process, however significant amount that is wasted can be used for energy production in stationary application. The goal of the project was development of the technology for safe exploitation of by-product hydrogen in ch...
Real-time monitoring of lightweight composite components by embedding additional sensors in the structure of composites becomes more and more popular in nowadays aerospace and automotive industry. However, polymer composites due to their low thermal stability are incapable of working at higher temperatures. Therefore the development of multifunctio...
In this paper a study of damage accumulation evaluation of highly stressed composite layer using acoustic emission method and local strain measurements by optical fiber based sensors in form of Fiber Bragg Grating (FBG) is presented. The study was carried out using composite NOL-ring specimens. These kind of specimens can simulate behavior of the c...