Synthesis of complex 1.

Synthesis of complex 1.

Source publication
Article
Full-text available
The 18e saturated rhodium(III) species [Rh(H)(X)(κ²‐NSitBu2)(bipyMe2)] (NSitBu2={4‐methylpyridine‐2‐yloxy}ditertbutylsilyl; bipyMe2=4,4'‐dimethylbipyridine) (X=Cl, 1; OTf, 2) have been prepared and characterized by NMR spectroscopy and in the case of 2 it has been possible to determine its solid‐state structure by X‐ray diffraction. Complex 1 has p...