Publications (9)3.28 Total impact
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Dataset: 00397911.2011
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Article: Solvent-free microwave-assisted synthesis of oxadiazoles containing imidazole moiety
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ABSTRACT: Microwave-assisted as well as conventional synthesis of 5-substituted-2-(2-methyl-4-nitro-1-imidazomethyl)-1,3,4-oxadiazoles containing the nitroimidazole moiety is carried out and their antibacterial, antifungal and anti-inflammatory activity is reported.Journal of Chemical Sciences 04/2012; 119(1):41-46. · 1.18 Impact Factor -
Article: Novel One-Pot Synthesis of Aziridines Carrying Sydnone Moiety and Their Biological Studies
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ABSTRACT: doi: 10.1080/00397911.2011.599102Synthetic Communications 02/2012; 43(2):301-308. · 1.06 Impact Factor -
Article: Ethyl 6-(4-chloro-phen-yl)-4-(4-methoxy-phen-yl)-2-oxocyclo-hex-3-ene-1-carboxyl-ate.
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ABSTRACT: In the title compound, C(22)H(21)ClO(4), the cyclo-hex-3-ene unit adopts an envelope conformation in both independent mol-ecules comprising the asymmetric unit. The two benzene rings are inclined to each other at a dihedral angle of 82.03 (5)° [86.37 (5)°]. In the crystal, the molecules interact via C-H⋯O, C-H⋯Cl and C-H⋯π interactions.Acta Crystallographica Section E Structure Reports Online 01/2009; 65(Pt 6):o1235. · 0.35 Impact Factor -
Article: 4-[(5-Hydroxy-3-methyl-1-phenyl-1H-pyrazol-4-yl)phenylmethyl]-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one ethanol hemisolvate
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ABSTRACT: The asymmetric unit of the title compound, C27H24N4O2·0.5C2H6O, comprises two crystallographically independent molecules (A and B) with slightly different conformations, and one ethanol molecule of crystallization. Intramolecular C—H...O and O—H...O hydrogen bonds generate six- and eight-membered rings, producing S(6) and S(8) ring motifs, respectively. In molecule A, one of the benzene rings is disordered over two positions, with site-occupancy factors of 0.542 (11) and 0.458 (11). The dihedral angles between the central benzene ring and the two outer benzene rings are 73.88 (9) and 82.6 (2)/88.9 (2)° in molecule A, and 80.81 (8) and 79.38 (8)° in molecule B. In the crystal structure, molecules form infinite one-dimensional chains in the (101) plane. The crystal structure is stabilized by intermolecular O—H...N, N—H...N, N—H...O and C—H...O hydrogen bonds, weak C—H...π and π–π [centroid–centroid = 3.5496 (1) Å] interactions.Acta Crystallographica Section E. 01/2009; -
Article: Ethyl 6-(4-chlorophenyl)-4-(4-methoxyphenyl)-2-oxocyclohex-3-ene-1-carboxylate
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ABSTRACT: In the title compound, C22H21ClO4, the cyclohex-3-ene unit adopts an envelope conformation in both independent molecules comprising the asymmetric unit. The two benzene rings are inclined to each other at a dihedral angle of 82.03 (5)° [86.37 (5)°]. In the crystal, the molecules interact via C—H...O, C—H...Cl and C—H...π interactions.Acta Crystallographica Section E. 01/2009; -
Article: 4-[(4-Chloro-phen-yl)(5-hydr-oxy-3-methyl-1-phenyl-1H-pyrazol-4-yl)meth-yl]-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one.
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ABSTRACT: In the the title compound, C(27)H(23)ClN(4)O(2), the chloro-phenyl ring forms dihedral angles of 77.70 (9) and 86.65 (9)°, respectively, with the pyrazol-3-one and pyrazole rings. The phenyl rings attached to the pyrazole rings are twisted away from them [dihedral angles 33.80 (9) and 40.34 (10)°]. An intramolecular O-H⋯O hydrogen bond generates an S(8) ring motif. The mol-ecules are linked into chains running along the c axis by N-H⋯N hydrogen bonds, and the chains are cross-linked via C-H⋯O hydrogen bonds and C-H⋯π inter-actions involving the chloro-phenyl ring.Acta Crystallographica Section E Structure Reports Online 01/2008; 64(Pt 12):o2301-2. · 0.35 Impact Factor -
Article: 4-[(5-Hydr-oxy-3-methyl-1-phenyl-1H-pyrazol-4-yl)phenyl-meth-yl]-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one ethanol hemisolvate.
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ABSTRACT: The asymmetric unit of the title compound, C(27)H(24)N(4)O(2)·0.5C(2)H(6)O, comprises two crystallographically independent mol-ecules (A and B) with slightly different conformations, and one ethanol mol-ecule of crystallization. Intra-molecular C-H⋯O and O-H⋯O hydrogen bonds generate six- and eight-membered rings, producing S(6) and S(8) ring motifs, respectively. In mol-ecule A, one of the benzene rings is disordered over two positions, with site-occupancy factors of 0.542 (11) and 0.458 (11). The dihedral angles between the central benzene ring and the two outer benzene rings are 73.88 (9) and 82.6 (2)/88.9 (2)° in mol-ecule A, and 80.81 (8) and 79.38 (8)° in mol-ecule B. In the crystal structure, mol-ecules form infinite one-dimensional chains in the (101) plane. The crystal structure is stabilized by inter-molecular O-H⋯N, N-H⋯N, N-H⋯O and C-H⋯O hydrogen bonds, weak C-H⋯π and π-π [centroid-centroid = 3.5496 (1) Å] inter-actions.Acta Crystallographica Section E Structure Reports Online 01/2008; 65(Pt 1):o66-7. · 0.35 Impact Factor -
Article: 4-[(4-Chlorophenyl)(5-hydroxy-3-methyl-1-phenyl-1H-pyrazol-4-yl)methyl]-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one
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ABSTRACT: In the the title compound, C27H23ClN4O2, the chlorophenyl ring forms dihedral angles of 77.70 (9) and 86.65 (9)°, respectively, with the pyrazol-3-one and pyrazole rings. The phenyl rings attached to the pyrazole rings are twisted away from them [dihedral angles 33.80 (9) and 40.34 (10)°]. An intramolecular O—H...O hydrogen bond generates an S(8) ring motif. The molecules are linked into chains running along the c axis by N—H...N hydrogen bonds, and the chains are cross-linked via C—H...O hydrogen bonds and C—H...π interactions involving the chlorophenyl ring.Acta Crystallographica Section E. 01/2008;
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Institutions
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2012
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Mangalore university
Mangalore, State of Karnataka, India
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