Ismail Murat Palabiyik |
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Dr.
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Ankara University
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Division of Analytical Chemistry
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19.27
Skills (6)
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379 Questions27054 Followers
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240 Questions11218 Followers
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7 Questions741 Followers
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51 Questions4719 Followers
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38 Questions172 Followers
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322 Questions34607 Followers
Awards & achievements
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Sep 2009Award: PhD Thesis Award, University of Ankara
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Sep 2003Scholarship: TÜBİTAK – BİDEB, The Scientific Research and Technological Council of Turkey, Ph.D. Fellowship
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Sep 2000Scholarship: TÜBİTAK – BİDEB, The Scientific Research and Technological Council of Turkey, MSc. Fellowship
Other
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LanguagesTurkish,English,German
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Scientific MembershipsFABAD
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Journal Referees1. Journal of Pharmaceutical and Biomedical Analysis, Journal of AOAC International, Journal of chromatographic science, Chemical Industry and Chemical Engineering Quarterly, Journal of Liquid Chromatography & Related Technologies, Bulletin of the Chemical Society of Ethiopia, AFRICAN JOURNAL OF BIOTECHNOLOGY, 8. African Journal of Pharmacy and Pharmacology
Questions and Answers (4) View all
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Answer added in Optimization Methods9 Optimization toolBy Sachin Ghalme · SCSM COE,AhmednagarIsmail Palabiyik · Ankara UniversityYou should use simplex centroid design for that. This design technique is very useful especially for these kind of mixtures.You should use simplex centroid design for that. This design technique is very useful especially for these kind of mixtures.Following
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Answer added in Multidimensional analysis17 How to minimize a set of fitted multidimensional data?By Anna Obertacke · Bergische Universität WuppertalIsmail Palabiyik · Ankara UniversityYou should use response surface methodology with different design chart like central composite, box behnken etc. You should reach any software program... [more]You should use response surface methodology with different design chart like central composite, box behnken etc. You should reach any software program easily for that.Following
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Answer added in Chromatography127 How to determine if two HPLC chromatograms are different?By Special Smyth · University of Western AustraliaIsmail Palabiyik · Ankara UniversityI think that, the difference between two chromatograms with two different treatments is ok and a statistical test is not needed. You could change the... [more]I think that, the difference between two chromatograms with two different treatments is ok and a statistical test is not needed. You could change the detector and MS dedector is very useful about that.Following
Publications (20) View all
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Article: Simultaneous spectrophotometric and liquid chromatographic determination of dextromethorphan hydrobromide, phenylephrine hydrochloride and carbinoxamine maleate in pharmaceutical preparations
I. Murat PALABIYIK, Feyyaz ONURJournal of Analytical Chemistry. 01/2012; 67(1):56-63. -
Article: Stability-Indicating Micellar Electrokinetic Chromatography Method for Determination of Finasteride in Pharmaceutical Preparations
M. Gökhan ÇAĞLAYAN, İsmail Murat PALABIYIK, Feyyaz ONURJournal of Liquid Chromatography & Related Technologies 02/2013; 36(6):781-791. · 0.71 Impact Factor -
Article: Hypochlorous acid: Analytical Methods and Antimicrobial Activity
Müjde ERYILMAZ, İsmail Murat PALABIYIKTropical Journal of Pharmaceutical Research 02/2013; 12(1):123-126. · 0.82 Impact Factor -
Article: Using Derivative and Ratio Spectra Derivative Spectrophotometry as a New Data Pre-Processing Method in Partial Least Squares Technique for Resolving Ovelapped Spectra of Montelukast Sodium, Desloratadine and Levocetirizine Dihydrochloride
İsmail Murat PALABIYIK, M. Gökhan ÇAĞLAYAN, Feyyaz ONURReviews in analytical chemistry 06/2012; 31(2):107-112. · 0.36 Impact Factor -
Article: Multivariate optimization and validation of a capillary electrophoresis method for the simultaneous determination of dextromethorphan hydrobromur, phenylephrine hydrochloride, paracetamol and chlorpheniramine maleate in a pharmaceutical preparation using response surface methodology.
I Murat Palabiyik, Feyyaz Onur[show abstract] [hide abstract]
ABSTRACT: A fast, accurate, precise and sensitive capillary electrophoresis method for the simultaneous determination of dextromethorphan hydrobromide, phenylephrine hydrochloride, paracetamol and chlorpheniramine maleate has been developed. Response surface methodology with a central composite design was used for optimization of the concentration of the buffer, pH of the buffer and applied voltage. Therefore, working with Na(2)HPO(4) buffer (pH 8.00, 0.01 M) at 20 kV as an applied voltage in the capillary electrophoresis method were found to be suitable; under these optimal conditions, these four active ingredients were separated in about 7 min. This developed method was validated and successfully applied to a pharmaceutical preparation, sugar-coated tablet, and the results were compared with a high-performance liquid chromatographic method developed by us.Analytical Sciences 01/2010; 26(8):853-9. · 1.25 Impact Factor